Analytical and semipreparative supercritical fluid chromatography in drug discovery

Supercritical Fluid Technology for Drug Product Development

Volumn , Issue , 2004, Pages 497-538

  Berger, Terry A ^a  

^a Berger Instruments   (United States)

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EID: 15744374650     PISSN: None     EISSN: None     Source Type: Book    
DOI: None     Document Type: Chapter

References (53)

1. Berger TA. Separation of polar solutes by packed column SFC. J Chromatogr A 1997; 785:3-33.
2. Gyllenhaal O, Karlsson A, Vessman J. Applications of packed column SFC in the development of drugs. In: Anton K, Berger C, eds. Supercritical Fluid Chromatography with Packed Columns. Chromatographic Science Series. Vol. 75. New York: Marcel Dekker, 1984, Chap 9.
3. Bargmann N, Caude M. SFC of drugs and related compounds. In: Caude M, Thiebaut D, eds. Practical Supercritical Fluid Chromatography and Extraction. Amsterdam: Harwood Academic Publishers, 1999, Chap 8.
4. Berger TA. Practical advantages of packed column SFC in supporting combinatorial chemistry. In: Unified Chromatography, Parcher JF. Chester TL, eds. ACS Symposium Series. Vol. 748. Washington, DC: American Chemical Society, 2000. Chap 12.
5. Berry AJ. Ramsey ED, Newby M, Games DE. Applications of packed column SFC using light-scattering detection. J Chromatogr Sci 1996; 34:245-253.
6. Herbreteau B, LaFosse M, Morin-Allory L, Dreux M. Analysis of sugars by supercritical fluid chromatography using polar packed columns and light-scattering detection. J Chromatogr 1990; 505:299 305.
7. Camel V, Thiebaut D, Caude M, Dreux M. Packed column subcritical fluid chromatography of underivatized amino acids. J Chromatogr 1992; 605:95-101.
8. Anton K, Bach M, Geiser A. Supercritical fluid chromatography in the routine stability control of antipruritic preparations. J Chromatogr 1991; 553:71-79.
9. Giddings JC. Meyers M, Wahrhaftig AL. Int J Mass Spectrom Ion Physi 1970: 4:9-20.
10. Randal LG. Wahrhaftig AL. Anal Chem 1978; 50:1703-1705.
11. Voorhees KJ, Zaugg SD, DeLuca SJ. Supercritical Fluid Chromatography/Mass Spectrometry. In: White CM, ed. Modern Supercritical Fluid Chromatography. New York: Huthig, 1988, Chap 4.
12. Games DE, Berry AJ, Mylcreest IC, Perkins JR, Pleasance S. Supercritical Fluid Chromatography-Mass Spectrometry. In: Smith RM, ed. Supercritical Fluid Chromatography. RSC Monograph Series. London: Royal Society of Chemistry, 1988. Chap 6.
13. Lane SJ. SFC-MS in the pharmaceutical industry. In: Smith RM, ed. Supercritical Fluid Chromatography. RSC Monograph Series. London: Royal Society of Chemistry. 1988, Chap 7.
14. Matsumoto K, Nagata S, Hattori H, Tsuge S. Development of directly coupled supercritical fluid chromatography with packed capillary-mass spectrometry with atmospheric pressure chemical ionization. J Chromatogr 1992; 605:87-94.
15. Morgan DG, Norwood DL, Fisher DL. Moseley MA III. Directly coupled packed column SFC with APCI/MS. Poster and abstract presented at American Society for Mass Spectrometry. Portland, OR, 1996
16. Pinkston JD. Supercritical fluid chromatography/mass spectrometry. In: Caude M, Thiebaut D, eds. Practical Supercritical Fluid Chromatography and Extraction. Amsterdam: Harwood Academic. 1999, Chap 5b.
17. Harrasch PB, Bente PF, Berger T. Combining mass spectrometry with supercritical fluid chromatography for high-speed pharmaceutical analysis. Business Briefing. Life Sci Technol Spring, 2003.
18. Ventura MC, Farrell WP, Aurigemma CM, Greig MJ. Packed column supercritical fluid chromatography/mass spectrometry for high throughput analysis. Anal Chem 1999; 71:2410-2416.
19. HokeSH II, Tomlinson JA II, Bolden RD, Morand KL, Pinkston JD, Wehmeyer K.R. Increasing bioanalytical throughput using pcSFC-MS/MS: 10 minutes per 96-well plate. Anal Chem 2001; 73:3083-3088.
20. Blum AM. Lynam KG, Nicolas EC. Use of a new Pirkle-typc chiral stationary phase in analytical and preparative subcritical fluid chromatography of pharmaceutical compounds. Chirality 1994; 6:302-313.
21. Jusforgues P, Shaimi M, Barth D. Preparative supercritical fluid chromatography: grams, kilograms, tons. In: Anton K. Berger C, eds. Supercritical Fluid Chromatography with Packed Columns. Chromatographic Science Series. Vol. 75. New York: Marcel Dekker, 1998, Chap 14.
22. Coleman K, Boutant R, Verillon F. Practical aspects of preparative supercritical fluid chromatography. Isol Purif 1999; 3:9-19.
23. Lembke P. Production of high purity n-3 fatty acid -ethyl esters by process scale supercritical fluid chromatography. In: Anton K, Berger C, eds. Supercritical Fluid Chromatography with Packed Columns. Chromatographic Science Series. Vol. 75. New York: Marcel Dekker, 1998. Chap 15.
24. Nicoud R-M. Clavier J-Y, Perrut M. Preparative SFC: basics and applications. In: Caude M, Thiebaut D. eds. Practical Supercritical Fluid Chromatography and Extraction. Amsterdam: Harwood Academic, 1999, Chap 10.
25. Depta A, Giese T, Johannsen M, Brunner G. Separation of sterioisomers in a simulated moving bed-supercritical fluid chromatography plant. J Chromatogr A 1999; 865:175-186.
26. Berger TA. Packed Column SFC. London: Royal Society, 1995.
27. Berger TA, Wilson WH. High-speed screening of combinitorial libraries by gradient packed-column SFC. J Biochem Biophys Methods 2000; 43:77-85.
28. Stringham RW, Lynam KG, Grasso CC. Application of SFC to rapid method development. Anal Chem 1994; 66:1949-1954.
29. Lynam KG, Nicolas EC. Chiral HPLC vs. chiral SFC: evaluation of long term stability and selectivity of Chiracel OD using various eluents. J Pharma Biomed Anal 1993; 11:1197-1206.
30. Gere DR. Supercritical fluid chromatography. Science 1983; 222:253-259.
31. Lapinski CA, Lombardo F, Dominy BW, Feeney PJ. Experimental and computational approaches to estimate solubility and permeability in drug discovery and development settings. Adv Drug Deliv Rev 1997; 23:4-25; 2001; 46:326.
32. Berger TA, Smith J, Fogelman K, Kruluts K. Am Lab News October, 2002.
33. Berger TA. Packed Column SFC. London: Royal Society. 1995:56.
34. Berger TA, Wilson WH. Separation of drugs by packed column supercritical fluid chromatography. J Pharm Sci 1994; 83:281.
35. Berger TA, Fogelman K, Staats T, Bente P, Crocket I, Farrel W, Osonubi M. The development of a semi-preparatory scale supercritical-fluid chromatograph for high throughput purification of 'combi-chem' libraries. J Biochem Biophys Methods 2000; 43:87-111.
36. Standard Guide for Purity of Carbon Dioxide Used in Supercritical Fluid Application. ASTM Designation: E 1747–95. West Conshohocken, PA: American Society of Testing Materials, 1995.
37. Strubinger JR, Song H, Parcher JF. High pressure phase distribution isotherms for supercritical fluid chromatographic systems. 2. Binary isotherms of carbon dioxide and methanol. Anal Chem 1991; 63:104-108.
38. Mourier PA, Eliot E, Caude M, Rosset R. Anal Chem 1985; 57:2819.
39. Macaudiere P, Tambute A, Caude M, Rosset R, Alembik MA, Wainer IW.Resolution of enantiomeric amides on a Pirkle-type chiral stationary phase. J Chromatogr 1986; 371:159.
40. Wolf C, Pirkle WH. LC-GC 1997; 15:352-363.
41. Wolf C, Pirkle WH. Enantiomer separation by sub- and supercritical fluid chromatography on rationally designed chiral stationary phases. In: Anton K, Berger C, eds. Supercritical Fluid Chromatography with Packed Columns. Chromatographic Science Series. Vol 75. New York: Marcel Dekker, 1998, Chap 9.
42. Liu Y, Berthod A, Mitchell CR. Xiao TL, Zhang B, Armstrong DW. Super/subcritical fluid chromatography chiral separations with macrocyclic glycopep- tide stationary phases. J Chromatogr A 2002; 978:185-204.
43. Sandra P. Medvedovici A, Kot A, David F. Selectivity tuning in packed column SFC. In: Anton K, Berger C, eds. Supercritical Fluid Chromatography with Packed Columns. Chromatographic Science Series. Vol. 75. New York: Marcel Dekker, 1998, Chap 6.
44. Anton K, Eppinger J, Frederiksen L, Francotte E, Berger TA, Wilson WH. J Chromatogr A 1994; 666:395-01.
45. Phinney KW. SFC of drug enantiomers. Anal Chem 2000; 72:A204-A211.
46. Bargmann-Leyder N, Tambute A, Caude M. A comparison of LC and SFC for cellulose- and amylose-derived chiral stationary phases. Chirality 1995; 7:311325.
47. Biermanns P, Miller C. Lyon V, Wilson WH. Chiral resolution of β-blockers by packed column SFC. LC-GC 1993; 11(10):744—747.
48. Villeneuve MS, Anderegg RJ. Analytical supercritical fluid chromatography using fully automated column and modifier selection valves for the rapid development of chiral separations. J Chromatogr A 1998; 826:217-225.
49. Harrasch PB, Bente PF, Berger T. Combining mass spectrometry with supercritical fluid chromatography for high-speed pharmaceutical analysis. Business Briefing Life Sci Technol, Spring 2003.
50. Olson J, Pan J, Hochlowski J, Searle P, Blanchard D. Customization of a commercially available prep scale SFC system to provide enhanced capabilities. 2002.
51. Hochlowski J, Sauer D, Sowin T. Preparative scale supercritical fluid chromatography in support of HTOS. Presented at High Throughput Organic Synthesis. San Diego, CA, February 2002.
52. Hochlowski J, Searle P, Gunawardana G, Sowin T, Pan J, Olson J, Trumbull J. Development and application of a preparative scale supercritical fluid chromatography system for high throughput purification. Presented at Prep 2001. Washington, DC, 2001.
53. Xu R, Cai Z, Fogelman K, Wikfors R, Worle V, Stublen N, Kassel DB. Mass- directed purification of compound libraries by automated semi-preparative SFC/MS. Oral presentation and poster. American Society for Mass Spectrometry. Orlando, FL. 2002.