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Volumn 44, Issue 8, 2005, Pages 1251-1254

Solid-state structure and temperature/evacuation-induced dehydration of sodium saccharinate 1.875 hydrate

Author keywords

Artifical sweeteners; Hydrates; IR spectroscopy; Structure elucidation; X ray diffraction

Indexed keywords

ADDITIVES; DEHYDRATION; MOLECULAR STRUCTURE; SODIUM COMPOUNDS; SOLUTIONS; THERMAL EFFECTS;

EID: 15444379969     PISSN: 14337851     EISSN: None     Source Type: Journal    
DOI: 10.1002/anie.200461043     Document Type: Article
Times cited : (25)

References (29)
  • 14
    • 15444376368 scopus 로고
    • PhD thesis, University of Zagreb
    • G Jovanovski, PhD thesis, University of Zagreb, 1981.
    • (1981)
    • Jovanovski, G.1
  • 18
    • 15444369787 scopus 로고    scopus 로고
    • note
    • 2O which splits into a doublet was found to be very sensitive to dehydration.
  • 19
    • 0001120357 scopus 로고    scopus 로고
    • As the pronounced structural disorder precludes accurate location of the hydrogen atoms by X-ray diffraction, the structure of the stoichiometric water was additionally investigated with the isotopic matrix-isolation method (examples: a) G. Jovanovski, P. Naumov, O. Grupče, B. Kaitner, Eur. J. Solid State Inorg. Chem. 1998, 35, 231-242;
    • (1998) Eur. J. Solid State Inorg. Chem. , vol.35 , pp. 231-242
    • Jovanovski, G.1    Naumov, P.2    Grupče, O.3    Kaitner, B.4
  • 20
    • 0033826150 scopus 로고    scopus 로고
    • -1 region (see the Supporting Information), to which 30 mixed Gaussian-Lorentzian component ν(OD) bands with different intensities were fitted. This result indicates the structural dissimilarity of at least 30 structurally different water OH groups.
    • (2000) Solid State Sci. , vol.2 , pp. 249-256
    • Naumov, P.1    Jovanovski, G.2
  • 27
    • 84944640969 scopus 로고
    • The use of refinable coordinates defined relative to local orthonormal axial systems (a) A. D. Rae, Acta Crystallogr. C 1975, 31, 560-570;
    • (1975) Acta Crystallogr. C , vol.31 , pp. 560-570
    • Rae, A.D.1
  • 28
    • 0000234616 scopus 로고
    • -1. The errors quoted for bond lengths and angles are conditional on the appropriateness of the various constraints and restraints.
    • (1975) Acta Crystallogr. C , vol.31 , pp. 570-574
    • Rae, A.D.1
  • 29
    • 0003992987 scopus 로고
    • Oak Ridge National Laboratory, Oak Ridge, Tennessee, USA
    • C. K. Johnson, ORTEP. Oak Ridge National Laboratory, Oak Ridge, Tennessee, USA, 1976.
    • (1976) ORTEP
    • Johnson, C.K.1


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.