Synthesis and Structure of a New Lithium Amide Ligand Precursor: A Tridentate Nitrogen-Based Donor Set of the Formula N(SiMe2CH2NMe2)2. Synthesis and Structure of the Group 4 Amides MCl3[N(SiMe2CH2NMe2)2] (M = Ti, Zr, Hf)

Inorganic Chemistry

Volumn 36, Issue 16, 1997, Pages 3480-3484

  Fryzuk, Michael D ^a   Huffman, Vera ^a   Kickham, James E ^a   Rettig, Steven J ^a   Gambarotta, Sandro ^b  

^a UNIVERSITY OF BRITISH COLUMBIA   (Canada)

^b UNIVERSITY OF OTTAWA   (Canada)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 1542684013     PISSN: 00201669     EISSN: None     Source Type: Journal    
DOI: 10.1021/ic970168u     Document Type: Article

References (33)

1. Pauer, F.; Power, P. P. Lithium Chemistry; Sapse, A.-M., Schleyer, P. v. R., Eds.; John Wiley and Sons; New York, 1995; p 295.
2. Gregory, K.; Schleyer, P. v. R.; Snaith, R. Adv. Inorg. Chem. 1991, 37, 47.
3. Lucht, B. L.; Collum, D. B. J. Am. Chem. Soc. 1994, 116, 6009.
4. Lucht, B. L.; Collum, D. B. J. Am. Chem. Soc. 1993, 117, 9863.
5. Lucht, B. L.; Collum, D. B. J. Am. Chem. Soc. 1996, 118, 2217.
6. Galiano-Roth, A. S.; Collum, D. B. J. Am. Chem. Soc. 1989, 111, 6772.
7. Collum, D. B. Acc. Chem. Res. 1993, 26, 227.
8. DePue, J. S.; Collum, D. B. J. Am. Chem. Soc. 1988, 110, 5518.
9. Barnett, N. D. R.; Mulvey, R. D.; Clegg, W.; O'Neil, P. A. J. Am. Chem. Soc. 1991, 113, 8187.
10. Bernstein, M. P.; Romesberg, F. E.; Fuller, D. J.; Harrison, A. T.; Collum, D. B.; Liu, Q. Y.; Williard, P. G. J. Am. Chem. Soc. 1992, 114, 5100.
11. Mair, F. S.; Clegg, W.; O'Neil, P. A. J. Am. Chem. Soc. 1993, 115, 3388.
12. Romesberg, F. L.; Collum, D. B. J. Am. Chem. Soc 1994, 116, 9198.
13. Nichols, M. A.; Waldmuller, D.; Williard, P. G. J. Am. Chem. Soc. 1994, 116, 1153.
14. Rogers, R. D.; Atwood, J. L.; Gruning, R. J. Organomet. Chem. 1978, 157, 229.
15. Lappert, M. F.; Power, P. P.; Sanger, A. R.; Srivastava, R. C. Metal and Metalloid Amides; Ellis Horwood: Chichester, U.K.,1980.
16. Fryzuk, M. D.; Montgomery, C. D. Coord. Chem. Rev. 1989, 95, 1.
17. Fryzuk, M. D.; Haddad, T. S.; Berg, D. J.; Retting, S. J. Pure App. Chem. 1991, 63, 845.
18. Fryzuk, M. D. Can. J. Chem. 1992, 70, 2849.
19. Fryzuk, M, D.; Haddad, T. S.; Rettig, S. J. Organometallics 1992, 11, 2967.
20. Fryzuk, M. D.; Huang, L.; McManus, N. T.; Paglia, P.; Rettig, S. J.; White, G. S. Organometallics 1992, 11, 2979.
21. Fryzuk, M. D.; Mylvaganam, M.; Zaworotko, M. J.; MacGillivray, L. R. Polyhedron 1995, 15, 689.
22. Fryzuk, M. D.; Leznoff, D. B.; Rettig, S. J. Organometallics 1995, 14, 5193.
23. Bangerter, B. W.; Beatty, R. P.; Kouba, J. K.; Wreford, S. S. J. Org. Chem. 1977, 42, 3247.
24. Grobe, J.; Heyer, G. J. Organomet. Chem. 1973, 61, 133.
25. Grobe, J.; Scheuer, G. F. Z. Anorg. Allg. Chem 1977, 433, 157.
26. Engelhardt, L. M.; May, A. S.; Raston, C. L.; White, A. H. J. Chem. Soc. Dalton Trans. 1983, 1671.
27. van der Zeijden, A. A. H.; van Koten, G. Recl. Trav. Chim. Pays-Bas 1988, 107, 431.
28. Moene, W.; Vos, M.; deKanter, F. J. J.; Klumpp, G. W.; Spek, A. L. J. Am. Chem. Soc. 1989, 111, 3463.
29. Jastrzebski, J. T. B. H.; van Koten, G.; Konijn, M.; Stam, C. H. J. Am. Chem. Soc. 1982, 104, 5490.
30. Fryzuk, M. D.; Carter, A.; Rettig, S. J. Organometallics 1992, 11, 469.
31. teXsan: Crystal Structure Analysis Package; Molecular Structure Corp.: The Woodlands, TX, 1995.
32. (a) International Tables for X-Ray Crystallography; Kynoch Press: Birmingham, U.K. (present distributor Kluwer Academic Publishers: Boston, MA), 1974; Vol. IV, pp 99-102.
33. (b) International Tables for Crystallography; Kluwer Academic Publishers: Boston, MA, 1992; Vol. C, pp 200-206.