A New Synthesis of 3-Methylidenetetrahydrofurans

Synlett

Volumn 1996, Issue 12, 1996, Pages 1201-1202

  Gordaliza, M ^a   Del Corral, J M Miguel ^a   Castro, M A ^a   Salinero, M A ^a   San Feliciano, A ^a   Dorado, J M ^a   Valle, F ^a  

^a UNIVERSITY OF SALAMANCA   (Spain)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 1542499541     PISSN: 09365214     EISSN: None     Source Type: Journal    
DOI: 10.1055/s-1996-5712     Document Type: Article

References (16)

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14. 2U or THF. The mixture was stirred under argon atmosphere for 1 to 4 h after which wet ether was added. Acidification to pH 2 with 2N HCl, extraction with EtOAc was followed by flash chromatography (hexene-EtOAc).
15. 3 requires C, 70.57; H, 5.92; found: C, 70.53; H, 5.98.
16. Hobbs J.B. "Purine and Pyrimidine Targets" in Comprehensive Medicinal Chemistry Vol. 2. Pergamon Press, Oxford, 1990; pp 299-332.