The Synthesis of Novel Polycyclic Heterocyclic Ring Systems. 3. Synthesis and NMR Spectroscopy of 15-Chloro[1]benzothieno[2″,3″:3′,4′]naphtho[1′, 2′:4,5]thieno[2,3-c]quinoline

Journal of Heterocyclic Chemistry

Volumn 34, Issue 6, 1997, Pages 1829-1832

  Sasaki, Kenji ^a   Tokuda, Osamu ^a   Hirota, Takashi ^a   Luo, Jiann Kuan ^b   Federspiel, Ronald R ^b   Castle, Raymond N ^b  

^a OKAYAMA UNIVERSITY   (Japan)

^b UNIVERSITY OF SOUTH FLORIDA   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 1542421246     PISSN: 0022152X     EISSN: None     Source Type: Journal    
DOI: 10.1002/jhet.5570340632     Document Type: Article

References (22)

1. J.-K. Luo, R. F. Federspiel and R. N. Castle, J. Heterocyclic Chem., 33, 185 (1996) and references cited therein.
2. J.-K. Luo and R. N. Castle, J. Heterocyclic Chem., 27, 1031 (1990).
3. [5a] S. L. Castle, J.-K. Luo, H. Kudo and R. N. Castle, J. Hetero-cyclic Chem., 25, 1363 (1988);
4. [b] J.-K. Luo, R. F. Federspiel and R. N. Castle, J. Heterocyclic Chem., 32, 659 (1995);
5. [c] A. F. Halverson, L. W. Castle and R. N. Castle, J. Heterocyclic Chem., 33, 119 (1996).
6. A. Bax and R. J. Freeman, J. Magn. Reson., 44, 542 (1981).
7. J. Jeener, B. Meier, P. Bachmann and R. R. Ernst, J. Chem. Phys., 71, 4546 (1979).
8. The nOe between H10 and H11 was not observable because their chemical shifts are too close to each other.
9. A. Bax and S. Subramanian, J. Magn. Reson., 67, 565 (1986)
10. A. Bax and F. Summers, J. Am. Chem. Soc., 108, 2093 (1986).
11. M. J. Musmar and R. N. Castle, J. Heterocyclic Chem., 28, 1533 (1991).
12. [12a] J.-K. Luo, A. S. Zektzer and R. N. Castle, J. Heterocyclic Chem., 28, 737 (1991);
13. [b] J.-K. Luo and R. N. Castle, J. Heterocyclic Chem., 28, 1825 (1991);
14. [c] J. P. Shockcor, R. C. Crouch, G. E. Martin, A. Cherif, J.-K. Luo and R. N. Castle, J. Heterocyclic Chem., 28, 2035 (1991);
15. [d] L. W. Castle, M. D. Johnston, Jr., Ch. L. Camoutsis and R. N. Castle, J. Heterocyclic Chem., 29, 1805 (1992);
16. [e] J.-K. Luo, A. S. Zektzer, R. N. Castle, R. C. Crouch, J. P. Shockcor and G. E. Martin, J. Heterocyclic Chem., 30, 453 (1993);
17. [f] M. J. Musmar, A. S. Zektzer, R. N. Castle and N. K. Dally, J. Heterocyclic Chem., 30, 487 (1993);
18. [g] J.-K. Luo, S. L. Castle and R. N. Castle, J. Heterocyclic Chem., 30, 653 (1993);
19. [h] J.-K. Luo and R. N. Castle, J. Heterocyclic Chem., 30, 1167 (1993);
20. [i] J.-K. Luo, R. F. Federspiel and R. N. Castle, J. Heterocyclic Chem., 32, 317 (1995);
21. [j] K. Sasaki, O. Tokuda, T. Hirota, J.-K. Luo and R. N. Castle, J. Heterocyclic Chem., 32, 1735 (1995).
22. Because of solubility problems, an elemental analysis was not possible.