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23
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-
85039571135
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-
note
-
16 To the solution was added 3 g of 1,3-butadiene, and the reaction mixture was stirred further for 2 h at 40°C. However, no polymerization was induced from the two reactions.
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-
-
-
24
-
-
85039570802
-
-
note
-
The oxidation state of complexes 2 and 4 is 0. Nonetheless, only complex 2 gave catalytic activity. This shows that the important factor inducing polymerization in the absence of metal alkyl compound is the easiness of the ligand exchange reaction between the ligand in metal complex and 1,3-butadiene rather than the oxidation state of metal. Both carboxylate and diimine ligands in complexes 1 (Ni(II)) and 3 (Ni(II)), respectively, would be hardly displaced by 1,3-butadiene due to their stronger coordination with Ni.
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-
-
-
26
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-
85039581297
-
-
note
-
3 to come around it.
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-
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27
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0037065857
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Jang, Y; Kim, P.; Lee, H. Macromolecules 2002, 35, 1477.
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-
Jang, Y.1
Kim, P.2
Lee, H.3
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28
-
-
85039564549
-
-
note
-
19F NMR spectra of these materials did not give significant information on the catalytic complexes due to the poor resolution and the complexity of the absorption peaks, respectively.
-
-
-
-
29
-
-
85039567841
-
-
note
-
-4 mol) in 5 mL of toluene was added to the solution, and the reaction mixture was stirred further for l h at 0°C. Evaporation of solvent at reduced pressure provided crude products, which were washed several times with dried-pentane under nitrogen atmosphere before analysis. For the details, see ref. 21.
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-
-
-
30
-
-
85039569429
-
-
note
-
2. For the details, see ref. 22.
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-
-
-
31
-
-
85039566014
-
-
note
-
On the other hand, the polymerization performed at [MAO]/[Ni] = 3 did not give any catalytic activity.
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-
-
-
32
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-
6544241298
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Johnson, L. K.; Killian, C. M.; Brookhart, M. J Am Chem Soc 1995, 117, 6414.
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J Am Chem Soc
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-
Johnson, L.K.1
Killian, C.M.2
Brookhart, M.3
-
34
-
-
85039573524
-
-
note
-
The π-electrons from the aromatic solvent can be donated into the vacant d orbital of the Ni atom, which contributes to stabilize Ni complex against decomposition, thus enhancing catalytic activity.
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