Athena MIMOS II Mössbauer spectrometer investigation

Journal of Geophysical Research: Planets

Volumn 108, Issue 12, 2003, Pages

  Klingelhofer G ^a   Morris, R V ^b   Bernhardt, B ^a   Rodionov, D ^a,c   de Souza, P A ^a,d   Squyres, S W ^e   Foh, J ^a   Kankeleit, E ^f   Bonnes, U ^f   Gellert, R ^a   Schroder C ^a   Linkin, S ^c   Evlanov, E ^c   Zubkov, B ^c   Prilutski, O ^c  

^a JOHANNES GUTENBERG UNIVERSITY   (Germany)

^b NASA JOHNSON SPACE CENTER   (United States)

^c Space Research Institute IKI ^*  (Russian Federation)

^d VALE S A   (Brazil)

^e Department of Obstetrics Gynecology   (United States)

^f DARMSTADT UNIVERSITY OF TECHNOLOGY   (Germany)

Author keywords

Instrumentation; Iron mineralogy; Mars; MIMOS II; M ssbauer spectroscopy; Weathering

Indexed keywords

EXPLORATION; MARS; MOSSBAUER SPECTROSCOPY;

EID: 1542289010     PISSN: 01480227     EISSN: None     Source Type: Journal    
DOI: 10.1029/2003je002138     Document Type: Article

References (90)

1. Agresti, D. G., R. V. Morris, E. L. Wills, T. D. Shelfer, M. M. Pimperl, M. Shen. B. C. Clark, and B. D. Ramsey, Extraterrestrial Mössbauer spectrometry. Hyperfine Interact., 72, 285-298, 1992.
2. Aramu, F., and V. Maxia, Shift and broadening of Mössbauer peaks by lack of collimation, Nucl. Instrum. Methods. 80, 35-39, 1970.
3. Arvidson, R. E., et al., Rocky 7 prototype Mars rover field geology experiments: 1. Lavic Lake and Sunshine Volcanic Field, California, J. Geophys. Res., 103, 22,671-22,688, 1998.
4. Arvidson, R. E., et al., Physical properties and localization investigations associated with the 2003 Mars Exploration rovers, J. Geophys. Res., 108(E12), 8070, doi: 10.1029/2002JE002041, 2003.
5. Bancroft, G. M., Mössbauer Spectroscopy: An Introduction for Inorganic Chemists and Geochemists. McGraw-Hill, New York, 1973.
6. Bell, J. F., III, R. V. Morris, and J. B. Adams, Thermally altered palagonitic tephra: A spectral and process analog to the soil and dust of Mars, J. Geophys. Res., 98, 3373-3385, 1993.
7. Bell, J. F., III, et al., Mars Exploration Rover Athena Panoramic Camera (Pancam) investigation, J. Geophys. Res, 108(E12), 8063, doi:10.1029/2003JE002070, 2003.
8. Bishop, J. L., and E. Murad, Schwertmannite on Mars? Spectroscopic analyses of schwertmannite, its relationship to other ferric minerals, and its possible presence in the surface material on Mars, in Mineral Spectroscopy: A Tribute to Roger G. Burns, edited by M. D. Dyar, C. McCammon, and M. W. Schaefer, Spec. Publ, Geochem. Soc., 5, 337-358, 1996.
9. Bishop, J. L., C. M. Pieters, and R. G. Burns, Reflectance and Mössbauer spectroscopy of ferrihydrite-montmorillonite assemblages as Mars soil analog materials, Geochim. Cosmochim. Acta, 57, 4583-4595, 1993.
10. Bishop, J. L., C. M. Pieters, R. G. Burns, J. O. Edwards, R. L. Mancinelli, and H. Froschel, Reflectance spectroscopy of ferric suflate-bearing montmorillonites as Mars soil analogue materials, Icarus, 117, 101-119, 1995.
11. Burns, R. G., Mössbauer spectral characterization of iron in planetary surface materials, in Remote Geochemical Analysis: Elemental and Mineralogical Composition, edited by C. M. Pieters and P. A. J. Englert, pp. 539-556, Cambridge Univ. Press, New York, 1993.
12. Burns, R. G., and D. S. Fisher, Iron-sulfur mineralogy of Mars: Magmatic evolution and chemical weathering products, J. Geophys. Res., 95, 14,415-14,421, 1990.
13. Burns, R. G., and S. L. Martinez, Mössbauer spectra of olivine-rich achondrites: Evidence for preterrestrial redox reactions, Proc. Lunar Planet. Sci. Conf. 21st, 331-340, 1991.
14. 57Fe-bearing oxide, silicate, and aluminosilicate minerals: Crystal structure trends in Mössbauer spectra, in Spectroscopic Characterization of Minerals and Their Surfaces, pp. 262-283, Am. Chem. Soc., Washington. D. C., 1990.
15. Christensen, P. R., et al., Detection of crystalline hematite mineralization on Mars by the Thermal Emission Spectrometer, J. Geophys. Res., 105, 9623-9642, 2000.
16. Christensen, P. R., R. V. Morris, M. D. Lane, J. L. Bandfield, and M. C. Malin, Global mapping of Martian hematite mineral deposits: Remnants of water-driven processes on early Mars, J. Geophys. Res., 106, 23,873-23,885, 2001.
17. Christensen, P. R., et al., Miniature Thermal Emission Spectrometer for the Mars Exploration Rovers, J. Geophys. Res., 108(E12), 8064, doi:10.1029/2003JE002117, in press, 2003.
18. De Grave, E., and A. Van Alboom, Evaluation of ferrous and ferric Mössbauer fractions, Phys. Chem. Miner., 18, 337-342, 1991.
19. de Souza, P. A., Jr., Automation in Mössbauer spectroscopy analysis, Lab. Robot. Automation, 11(1), 13-23, 1999.
20. de Souza, P. A., Jr., and G. Klingelhöfer, Mars-analogue minerals, soils, and rocks studied by Mössbauer spectroscopy, Meteorit. Planet. Sci., 36A, 139, 2001.
21. Evlanov, E. N., V. A. Frolov, O. F. Prilutski, A. M. Rodin, G. V Veselova, and G. Klingelhöfer, Mössbauer spectrometer for mineralogical analysis of the Mars surface: Mössbauer source considerations. Lunar Planet. Sci., 459-460, 1993.
22. Fegley, B., Jr., G. Klingelhöfer, R. A. Brackett, N. Izenberg. D. T. Kremser, and K. Lodders, Basalt oxidation and the formation of hematite on the surface of Venus, Icarus, 118, 373-383, 1995.
23. Fernandez-Moran, H., S. S. Hafner, M. Ohtsuki, and D. Virgo, Mössbauer effect and high-voltage electron microscopy of pyroxenes in Type B samples, Science, 167, 686-688, 1970.
24. Galazkha-Friedman, J., and J. Juchniewicz, Martian Mössbauer Spectrometer MarMös, project proposal, Space Res. Cent., Polish Acad. of Sci., Warsaw, Feb. 1989.
25. Gay, P., G. M. Bancroft, and M. G. Bown, Diffraction and Mössbauer studies of minerals from lunar soils and rocks, Science, 167, 626-628, 1970.
26. Golden, D. C., R. V. Morris, H. V. Lauer Jr., and S. R. Yang, Mineralogy of three slightly palagonitized tephra samples from the summit of Mauna Kea, Hawaii, J. Geophys. Res., 98, 3401-3411, 1993.
27. Gonser, U., Mössbauer spectroscopy, in Microscopic Methods in Metals, edited by U. Gonser, chap. 13, pp. 409-448, Springer-Verlag, New York, 1986.
28. Gonser, U., F. Aubertin, S. Stenger, H. Fischer, G. Smirnov, and G. Klingelhöfer, Polarization and thickness effects in Mössbauer spectroscopy, Hyperfine Interact., 67, 701-710, 1991.
29. Gorevan, S., et al., Rock Abrasion Tool Mars Exploration Rover Mission, J. Geophys. Res., 108(E12), 8068, doi: 10.1029/2003JE002061, in press, 2003.
30. Graff T. G., R. V. Morris, and P. R. Christensen, Lunar mare basalts as analogues for Martian volcanic compositions: Evidence from visible, near-IR, and thermal emission spectroscopy, Lunar Planet. Sci. [CDROM], XXXIV, 1632, 2003.
31. Greenwood, N. N., and T. C. Gibb, Mössbauer Spectroscopy, Chapman and Hall, New York, 1971.
32. Gummer, A. W., Effect of accumulated decay product on the Mösssbauer emission spectrum, Nucl. Instrum. Methods Phys. Res., Sect. B, 34, 224-227, 1988.
33. Hargraves, R. B., D. W. Collinson, R. E. Arvidson, and P. M. Cates, Viking magnetic properties experiment: Extended mission results, J Geophys. Res., 84, 8379-8384, 1979.
34. Hawthorne, F. C., Mössbauer spectroscopy, in Spectroscopic Methods in Mineralogy and Geology, Rev. Mineral., vol. 18, edited by F. C. Hawthorne, pp. 255-340, Mineral. Soc. Am., Washington, D. C., 1988.
35. Held, P., PIN-Photodioden als Detektoren für das Mössbauerspektrometer MIMOS zur Untersuchung der Marsoberfläche, diploma thesis, Inst. for Nucl. Phys., Univ, Darmstadt, Darmstadt, Germany, 1993.
36. Held, P., MIMOS II: Ein miniaturisiertes Möβauerspektrometer in Rückstreugeometrie zur mineralogischen Analyse der Marsoberfläche, Ph.D. thesis, Inst. for Nucl. Phys., Univ. Darmstadt, Darmstadt, Germany, 1997.
37. Held, P., R. Teacher, G. Klingelhöfer, J. Foh, H. Jäger, and E. Kankeleit, Mössbauer Spectrometer for mineralogical analysis of the Mars surface: First temperature dependent tests of the detector and drive system, Lunar Planet. Sci., XXIV. 633-634, 1993.
38. Herkenhoff, K., et al., Athena Microscopic Imager investigation, J. Geophys. Res., 108(E12), 8065, doi:10.1029/2003JE002076, 2003.
39. Herzenberg, C. L., and D. L. Riley, Analysis of first returned lunar samples by Mossbauer spectrometry, Proc. Lunar Sci. Conf. 1st, 2221-2241, 1970.
40. Herzenberg, C. L., R. B. Moler, and D. L. Riley, Mossbauer instrumental analysis of Apollo 12 lunar rock and soil samples, Proc. Lunar Sci. Conf. 2nd, 2103-2123, 1971.
41. Housley, R. M., M. Blander, M. Abdel-Gawad, R. W. Grant, and A. H. Muir Jr,, Mossbauer spectroscopy of Apollo 11 samples, Proc. Lunar Sci. Conf. 1st, 2251-2268, 1970.
42. Housley, R. M., R. W. Grant, A. H. Muir Jr., M. Blander, and M. Abdel-Gawad, Mossbauer studies of Apollo 12 samples, Proc. Lunar Sci. Conf. 2nd, 2125-2136, 1971.
43. Housley, R. M., E. H. Cirlin, and R. W. Grant, Characterization of fines from the Apollo 16 site, Proc. Lunar Sci. Conf. 4th, 2729-2735, 1973.
44. Huffman, G. P., F. C. Schwerer, and R. M. Fisher, Iron distributions and metallic-ferrous ratios for Apollo lunar samples: Mossbauer and magnetic analyses, Proc. Lunar Sci. Conf. 5th. 2779-2794, 1974.
45. Hviid, S. F., et al., Magnetic properties experiments on the Mars Pathfinder Lander: Preliminary results, Science, 278, 1768-1770, 1997.
46. Johnson, G. R., and G. R. Olhoeft, Densities of rocks and minerals, in CRC Handbook of Physical Properties of Rocks, vol. III, edited by R. S. Carmichael, pp, 1-38, CRC Press, Boca Raton, Fla., 1984.
47. Kankeleit, E., Velocity spectrometer for Mössbauer experiments, Rev. Sci. Instrum. 35, 194-197, 1964.
48. Kankeleit, E., Some technical developments in Mössbauer spectroscopy, paper presented at International Conference on Mössbauer Spectroscopy, Univ. of Krakow, Krakow, Poland, 1975.
49. Klingelhöfer, G., The miniaturized spectrometer MIMOS II, in Mössbauer Spectroscopy in Materials Science, edited by M. Miglierini and D. Petridis, pp. 413-426. Kluwer Acad., Norwell, Mass., 1999.
50. Klingelhöfer. G., U. Imkeller, E. Karkeleit, and B. Stahl, Remarks on depth selective CEMS -backscattering measurements, Hyperfine Interact., 71, 1445-1448, 1992.
51. Klingelhöfer, G., B. Fegley Jr., R. V. Morris, E. Kankeleit, P. Held, and E. P. O. Evlanov, Mineralogical analysis of Martian soil and rock by a miniaturized backscattering Mössbauer spectrometer, Planet. Space Sci, 44, 1277-1288, 1996.
52. Klingelhöfer, G., P. Held, B. Bernhardt, J. Foh, R. Teucher, and E. Kankeleit, In-situ phase analysis by a versatile miniaturized Mössbauer spectrometer. Hyperfine Interact., 111, 331-334, 1998.
53. 57Fe and the evolution of the solar system, Hyperfine Interact. 47, 3-31, 1989.
54. Knudsen, J. M., S. Moerup, and J. Galazkha-Friedman, Mössbauer spectroscopy and the iron on Mars, Hyperfine Interact., 57, 2231-2234, 1990.
55. Knudsen, J. M., et al., Mössbauer spectroscopy on the surface of the planet Mars. Why?, Hyperfine Interact., 68, 83-94, 1992.
56. Lane, M. D., R. V. Morris, S. A. Mertzman, and P. R. Christensen, Evidence for platy hematite grains in Sinus Meridiani Mars, J. Geophys. Res., 107(E12), 5126, doi:10.1029/2001JE001832, 2002.
57. Madsen, M. B., S. Morup, T. V. V. Costa, J. M. Knudsen, and M. Olsen, Superparamagnetic component in the Orgueil meteorite and Mossbauer spectroscopy studies in applied magnetic fields, Nature, 29, 501-503, 1986.
58. Madsen, M. B., S. F. Hviid, H. P. Gunnlaugsson, J. M. Knudsen, W. Goetz, C. T. Pedersen, A. R. Dinesen, C. T. Morgensen, M. Olsen, and R. B. Hargraves, The magnetic properties experiments on Mars Pathfinder, J. Geophys. Res., 104, 8761-8779, 1999.
59. Madsen, M., et al., Magnetic Properties Experiments on the Mars Exploration Rover mission, J. Geophys. Res., 108(E12), 8069, doi:10.1029/2002JE002029, in press, 2003.
60. Maki. J. N., et al., Mars Exploration Rover engineering cameras, J. Geophys. Res., 108(E12), 8071, doi:10.1029/2003JE002077, in press, 2003.
61. McCammon, C., Mössbauer spectroscopy of minerals, in Mineral Physics and Crystallography: A Handbook of Physical Constants, AGU Ref. Shelf. vol. 2, edited by T. J. Ahrens, pp. 332-347, AGU, Washington, D. C., 1995.
62. 3O4), goethite (α-FeOOH), and lepidocrocite (γ-FeOOH), J. Geophys. Res., 90, 3126-3144, 1985.
63. Morris, R. V., D. G. Agresti, T. D. Shelfer, and T. J. Wdowiak, Mössbauer spectroscopy for mineralogical analysis on planetary surfaces paper presented at SAAP Instrument Technology Workshop, Sample Acquisition and Anal. Program, Houston, Tex., 14-16 Nov. 1988.
64. Morris, R. V., D. G. Agresti, H. V. Lauer Jr., J. A. Newcomb, T. D. Shelfer, and A. V. Murali, Evidence for pigmentary hematite on Mars based on optical magnetic and Mössbauer studies of superparamagnetic (nanocrystalline) hematite, J. Geophys. Res., 94, 2760-2778, 1989.
65. Morris, R. V., J. J. Gooding, H. V. Lauer Jr., and R. B. Singer, Origins of Marslike spectral and magnetic properties of a Hawaiian palagonitic soil, J. Geophys. Res., 95, 14,427-14,434, 1990.
66. Morris, R. V., D. C. Golden, J. F. Bell III, H. V. Lauer Jr., and J. B. Adams, Pigmenting agents in Martian soils: Inferences from spectral, Mössbauer, and magnetic properties of nanophase and other iron oxides in Hawaiian palagonitic soil PN-9. Geochim. Cosmochim. Acta, 57, 4597-4609, 1993.
67. Morris, R. V., D. C. Golden, J. F. Bell III, and H. V. Lauer Jr., Hematite, pyroxene, and phyllosilicates on Mars: Implications from oxidized impact melt rocks from Manicouagan Crater Quebec, Canada, J. Geophys. Res., 100, 5319-5328, 1995.
68. Morris, R. V., D. W. Ming, D. C. Golden, and J. F. Bell III, An occurrence of jarositic tephra on Mauna Kea, Hawaii: Implications for the ferric mineralogy of the Martian surface, in Mineral Spectroscopy: A Tribute to Roger G. Burns, edited by M. D. Dyar, C. McCammon, and M. W. Schaefer. Spec. Publ. Geochem. Soc., 5, 327-336, 1996.
69. Morris, R. V., D. C. Golden, and J. F. Bell III, Low-temperature reflectivity spectra of red hematite and the color of Mars, J. Geophys. Res., 102, 9125-9133, 1997.
70. Morris, R. V., G. Klingelhöfer R. L. Korotev, and T. D. Shelter. Mössbauer mineralogy on the Moon: The lunar regolith, Hyperfine Interact., 117, 405-432, 1998a.
71. Morris, R. V., S. W. Squyres, J. F. Bell III, T. Economou, G. Klingelhoefer, P. Held, L. A. Haskin, A. Wang, B. L. Jolliff, and R. Rieder, Analysis of Martian surface materials during the Mars Surveyor 001 mission by the Athena instrument payload (abstract), Lunar Planet. Sci. [CD-ROM], XXIX, abstract 1326, 1998b.
72. Morris, R. V., et al., Mineralogy, composition, and alteration of Mars Pathfinder rocks and soils: Evidence from multispectral, elemental, and magnetic data on terrestrial analogue, SNC meteorite, and Pathfinder samples, J. Geophys. Res., 105, 1757-1817, 2000.
73. Morris, R. V., D. C. Golden, D. W. Ming T. D. Shelfer, L. C. Jorgensen, J. F. Bell III, T. G. Graff, and S. A. Mertzman, Phyllosilicate-poor palagonitic dust from Mauna Kea Volcano (Hawaii): A mineralogical analogue for magnetic Martian dust?, J. Geophys. Res., 106, 5057-5083, 2001a.
74. Morris, R. V., T. G. Graff, T. D. Shelfer, and J. F. Bell III, Effect of palagonitic dust coatings on visible, near-IR and Mössbauer spectra of rocks and minerals: Implications for mineralogical remote sensing of Mars (abstract), Lunar Planet. Sci. [CD-ROM]. XXXII, abstract 1912, 2001b.
75. Prilutskii, O., Internal report from Minsk, Space Res. Inst. (IKI), Moscow, 1990.
76. Rieder, R., R. Gellert, J. Brückner, G. Klingelhöfer, G. Dreibus, A. Yen, and S. W. Squyres, The new Athena alpha particle X-ray spectrometer for the Mars Exploration Rovers, J. Geophys. Res., 108(E12), 8066, doi:10.1029/2003JE002150, 2003.
77. Riesenman, R., J. Steger, and E. Kostiner, Cosine effect in Mössbauer spectroscopy involving a source of non-zero radius, Nucl. Instrum. Methods, 72, 109-110, 1969.
78. Schröder, C., Optimierung der Nachweiseigenschaften des miniaturisierten Mössbauer-Spektrometers MIMOS II und Messungen an Mars-Analog-Proben, diploma thesis, Johannes Gutenberg Univ., Mainz, Germany, 2001.
79. Sims, M. R., et al., Performance characteristics of the PAW instrumentation on Beagle 2 (the astrobiology lander on ESA's Mars Express Mission), Proc. SPIE Int. Soc. Opt. Eng., 4859, 32-44, 2002.
80. Solberg, T. C., and R. G. Burns, Iron Mossbauer spectral study of weathered Antarctic and SNC meteorites, Proc. Lunar Planet. Sci. Conf., 19th, 313-322, 1989.
81. Squyres, S. W., et al., Athena Mars Rover science investigation, J. Geophys. Res., 108(E12), 8062, doi:10.1029/2003JE002121, in press, 2003.
82. Stevens, J. G., A. M. Khasanov, J. W. Miller, H. Pollak, and Z. Li (Eds.), Mössbauer Mineral Handbook, 527 pp., Biltmore, Ashville, N. C., 1998.
83. Straub, D. W., R. G. Burns, and S. F. Pratt, Spectral signature of oxidized pyroxenes: Implications to remote sensing of terrestrial planets, J. Geophys. Res., 96, 18,819-18,830, 1991.
84. Teucher, R., Miniaturisierter Mössbauerantrieb, diploma thesis, Inst. for Nucl. Phys., Univ. Darmstadt, Darmstadt, Germany, 1994.
85. Vieira, V. W. A., T. V. V. Costa, H. G. Jensen, J. M. Knudsen, and M. Olsen, Oxidation state of iron in SNC meteorites as studied by Mössbauer spectroscopy, Phys. Scr., 33, 180-186, 1986.
86. Wade, M. L., D. G. Agresti, T. J. Wdowiak, and L. P. Armendarez, A Mössbauer investigation of iron-rich terrestrial hydrothermal vent systems: Lessons for Mars exploration, J. Geophys. Res., 104, 8489-8507, 1999.
87. Wdowiak, T. J., and D. G. Agresti, Presence of a superparamagnetic component in the Orgueil meteorite, Nature, 311, 140-142, 1984.
88. Wegener, H., Der Mössbauer-Effect und Seine Anwendungen in Physik und Chemie, 2nd ed., Bibliogr Inst., Mannheim, Germany, 1966.
89. Weinheimer, C., M. Schrader. J. Bonn, T. Loeken, and H. Backe, Measurement of energy resolution and dead layer thickness of LN2-cooled PIN photodiodes, Nucl. Instrum. Methods, Sect, A, 311, 273-279, 1992.
90. Wertheim, G. K., Mössbauer Effect: Principles and Applications, Academic, San Diego, Calif., 1964.