Crystallographic study of manganese(III) acetylacetonate: An advanced undergraduate project with unexpected challenges

Journal of Chemical Education

Volumn 82, Issue 3, 2005, Pages 460-465

  Geremia, Silvano ^a   Demitri, Nicola ^a  

^a UNIVERSITY OF TRIESTE   (Italy)

Author keywords

[No Author keywords available]

Indexed keywords

CHEMISTRY; CRYSTAL STRUCTURE; CRYSTALLIZATION; CRYSTALLOGRAPHY; EXPERIMENTS; LOW TEMPERATURE PROPERTIES; PHASE TRANSITIONS; STUDENTS; SYNTHESIS (CHEMICAL); X RAY DIFFRACTION ANALYSIS;

LABORATORY EXPERIMENT; MANGANESE ACETYLACETONATE; SOLID-SOLID PHASE TRANSITIONS; UNDERGRADUATE STUDENTS;

MANGANESE COMPOUNDS;

EID: 15044363748     PISSN: 00219584     EISSN: None     Source Type: Journal    
DOI: 10.1021/ed082p460     Document Type: Article

References (17)

1. Ruttledge, T. R. J. Chem. Educ. 1998, 75, 1575.
2. Woolins, J. D. Inorganic Experiments; VCH: Weinheim, Germany, 1994; p 117.
3. Szafran, Z.; Pike, R. M.; Singh, M. M. Microscale Inorganic Chemistry - A Comprehensive Laboratory Experience; Wiley: New York, 1991; p 224
4. Morosin, B.; Brathovde, J. R. Acta Crystallogr. 1964, 17 705.
5. Cotton, F. A.; Wilkinson, G. Advanced Inorganic Chemistry, 3rd ed.; Interscience: New York, 1972; p 851.
6. Hon, P. K.; Pfluger, C. E. J. Coord. Chem. 1973, 3, 67.
7. Fackler, J. P.; Avdeef, A. Inorg. Chem. 1974, 13, 1864.
8. Fackler, J. P. Inorg. Chem. 2002, 41, 6959.
9. Stults, B. R.; Marianelli, R. S.; Day, V. W. Inorg. Chem. 1979 18, 1853.
10. Hoggard, P. E. J. Chem. Educ. 2002, 79, 420.
11. Hunter, A. D. J. Chem. Educ. 1998, 75, 1297.
12. Crundwell, G.; Phan, J.; Kantardjieff, K. A. J. Chem. Educ. 1999, 76, 1242.
13. Collaborative Computational Project, Number 4. Acta Crystallogr. D Biol Crystallogr. 1994,50, 760.
14. Robinson, W. T.; Sheldrick, G. M. Crystallographic Computing 4. Techniques and New Technologies; Isaacs, N. W., Taylor, M. R., Eds.; International Union of Crystallography; Oxford University Press: Cambridge, 1988; p 366.
15. Sheldrick, G. M.; Schneider, T. R. Macromolecular Crystallography, Pt B 1997, 277, 319.
16. Lis, T.; Matuszewski, J.; Jezowska-Trzebiatowska, B. Acta Crystallogr., Sect. B 1977, 33, 1943.
17. Avdeef, A.; Fackler, J. P.; Costamagna, J. H. Inorg. Chem. 1974 13, 1854.