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2 (SHELXL97) using the SHELXTL program package. CCDC reference numbers 221325-221326. See http://www.rsc.org/suppdata/ce/b3/b312553j/ for crystallographic data in CIF or other electronic format. G. M. Sheldrick, SADABS, Program for area detector adsorption correction, Institute for Inorganic Chemistry, University of Göttingen, Germany, 1996; G. M. Sheldrick, SHELXS-97, Program for solution of crystal structures, University of Göttingen, Germany, 1997; G. M. Sheldrick, SHELXL-97, Program for refinement of crystal structures, University of Göttingen, Germany, 1997.
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0004150157
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