A Novel and Convenient Synthetic Route to a 9-Phosphatriptycene and Systematic Comparisons of 9-Phosphatriptycene Derivatives

Chemistry Letters

Volumn 32, Issue 12, 2003, Pages 1144-1145

  Kobayashi, Junji ^a   Agou, Tomohiro ^a   Kawashima, Takayuki ^a  

^a UNIVERSITY OF TOKYO   (Japan)

Author keywords

[No Author keywords available]

Indexed keywords

9 PHOSPHATRIPTYCENE; 9 PHOSPHATRIPTYCENE DERIVATIVE; CHALCOGEN; PHOSPHINE DERIVATIVE; PHOSPHORUS DERIVATIVE; TRIPTYCENE DERIVATIVE; UNCLASSIFIED DRUG;

ARTICLE; CHEMICAL BOND; LITHIATION; NUCLEAR MAGNETIC RESONANCE; SYNTHESIS;

EID: 1442288760     PISSN: 03667022     EISSN: None     Source Type: Journal    
DOI: 10.1246/cl.2003.1144     Document Type: Article

References (9)

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5. +).
6. 2 (all data) = 0.1463 GOF = 1.105. Crystallographic data reported in this paper have been deposited with Cambridge Crystallographic Data Centre as supplementary publication no. CCDC-221540. Copies of the data can be obtained free of charge via www.ccdc.cam.ac.uk/conts/retrieving.html (or from the Cambridge Crystallographic Data Centre, 12, Union Road, Cambridge CB2 1EZ, UK; fax: +44 1223 336033; or deposit@ccdc.cam. ac.uk). Instruction for depositing the crystallographic data is available on the Web at http://www.ccdc.cam.ac.uk/conts/ depositing.html.
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9. 3) δ 601.3 (d, J = 827 Hz).; The signals of the bridgehead carbons of 4 and 6 were not observed.