Improved Procedure for the Selective N-Debenzylation of Benzylamines by Diisopropyl Azodicarboxylate

Synthesis

Volumn , Issue 3, 2004, Pages 446-450

  Kroutil, Jiří ^a   Trnka, Tomáš ^a   Černý, Miloslav ^a  

^a CHARLES UNIVERSITY   (Czech Republic)

Author keywords

Amines; Azides; Cleavage; Debenzylation; Protecting groups

Indexed keywords

REACTION KINETICS; SOLVENTS;

REACTION INTERMEDIATES; SELECTIVE DEPROTECTION;

AROMATIC COMPOUNDS;

1,6 ANHYDRO BETA DEXTRO GLUCOPYRANOSE; BENZYLAMINE DERIVATIVE; CARBOXYLIC ACID DERIVATIVE; DIISOPROPYL AZODICARBOXYLATE; PYRAN DERIVATIVE; SOLVENT; UNCLASSIFIED DRUG;

ARTICLE; CHEMICAL ANALYSIS; CHEMICAL STRUCTURE; DEBENZYLATION; DEPROTECTION REACTION; REACTION ANALYSIS; STRUCTURE ANALYSIS; TECHNIQUE;

EID: 1442286423     PISSN: 00397881     EISSN: None     Source Type: Journal    
DOI: 10.1055/s-2004-815937     Document Type: Article

References (8)

1. Kroutil, J.; Trnka, T.; Cerný, M. Org. Lett. 2000, 2, 1681.
2. Colonna, M.; Marchetti, L. Gazz. Chim. Ital. 1969, 99, 14.
3. Egger, N.; Hoesch, L.; Dreiding, A. S. Helv. Chim. Acta 1983, 66.
4. Linke, K. H.; Göhausen, H. J. Chem. Ber. 1971, 104, 301.
5. Kenner, G. W.; Stedman, R. J. J. Chem. Soc. 1952, 2089.
6. Kroutil, J.; Trnka, T.; Buděšínský, M.; Černý, M. Collect. Czech. Chem. Commun. 1998, 63, 813.
7. Kroutil, J.; Karban, J.; Trnka, T.; Buděší nský, M.; Černý, M. Collect. Czech. Chem. Commun. 2002, 67, 1805.
8. Kroutil, J.; Trnka, T.; Buděšínský, M.; Černý, M. Eur. J. Org. Chem. 2002, 2449.