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2O (111 mg, 0.584 mmol) was gently blended in an agate mortar. The resulting homogeneous mixture was then ground for 10 min. The formation of acetic acid and wetting of the reaction mixture was observed. The solid residue was washed with diethyl ether (5 mL) and dried under high vacuum to afford 3a (218 mg, 97%), mp 134-136°C.
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