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2 and BaO. Such a sample was used for the synchrotron experiment.[17] After barium metal was purified by heating in a closed Ta ampoule at 1173 K for 12 h in dynamic vacuum, followed by distillation at 1100 K, a hydrogen free product was obtained. The hydrogen analysis yielded 0.03(2) wt% of H, which is on the detection limit.
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28
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