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Hyla-Kryspin, I.8
Gleiter, R.9
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6
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13244275518
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note
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max = 28.3°) collected, 5778 unique reflections [R(int) = 0.0391]. R1 = 0.0401 (I > 2σ(I)), wR2 = 0.0926 (all data). CCDC-244072 (1a), CCDC-244073 (4a), CCDC-244074 (4b) contains the supplementary crystallographic data for this paper. These data can be obtained free of charge via www.ccdc.cam.ac.uk/conts/retrieving.html (or from the Cambridge Crystallographic Data Centre, 12 Union Road, Cambridge CB21EZ, UK; fax: (+44)1223-336-033; or deposit@ccdc.cam.ac.uk).
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9
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0004150157
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Bruker Analytical X-ray Systems, Inc., Madison, WI
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c) G. M. Sheldrick, SHELXTL, Version 5.1, Program Package for Structure Solution and Refinement, Bruker Analytical X-ray Systems, Inc., Madison, WI, 1998.
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(1998)
SHELXTL, Version 5.1, Program Package for Structure Solution and Refinement
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Sheldrick, G.M.1
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10
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13244279980
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note
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2 is folded by 40.7° along the B⋯B vector, very similar to its green iron analogue.[2] The Ru-C2 bond length [2.029, cf. Fe-C 1.899 Å] is markedly shorter than the other Ru-C bond lengths of the heterocycle.
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11
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13244278554
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note
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102Ru: 550.2344, found: 550.2338, Δ = -0.7 mmu.
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13
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84982066667
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Koch, W.5
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14
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33748215301
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33748215301
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and references therein
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b) A. J. Ashe III, J. W. Kamp, W. Klein, R. Rousseau, Angew. Chem. 1993, 105, 1112; Angew. Chem. Int. Ed. Engl. 1993, 32, 1065-1066, and references therein.
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13244286853
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0142245926
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E. O. Fischer, S. Breitschaft, Angew. Chem. 1963, 75, 94-95; Angew. Chem. Int. Ed. Engl. 1963, 2, 44.
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A. J. Ashe III, S. Al-Ahmad, J. W. Kamp, V. G. Young, Jr., Angew. Chem. 1997, 109, 2104-2106; Angew. Chem. Int. Ed. Engl. 1997, 36, 2014-2016.
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Fang, X.1
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Bu, X.3
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0141670329
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X. Fang, D. Woodmansee, X. Bu, G. C. Bazan, Angew. Chem. 2003, 115, 4648-4652; Angew. Chem. Int. Ed. 2003, 42, 4510-4514.
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23
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13244295972
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University of Münster, Germany
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MO calculations for 1 and 4 are in progress (Dr. I. Hyla-Kryspin, University of Münster, Germany).
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Hyla-Kryspin, I.1
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