Determination of Carbamate Pesticide Residues in Vegetables and Fruits by Liquid Chromatography-Atmospheric Pressure Photoionization-Mass Spectrometry and Atmospheric Pressure Chemical Ionization-Mass Spectrometry

Journal of Agricultural and Food Chemistry

Volumn 52, Issue 4, 2004, Pages 727-735

  Takino, Masahiko ^a   Yamaguchi, Kenji ^a   Nakahara, Taketoshi ^a  

^a YOKOGAWA ANALYTICAL SYSTEMS INC   (Japan)

Author keywords

APPI; Carbamates; Fruits; LC MS; Pesticides; Vegetables

Indexed keywords

ALDICARB; CARBAMATE PESTICIDE; PESTICIDE RESIDUE;

ARTICLE; ATMOSPHERIC PRESSURE PHOTOIONIZATION MASS SPECTROMETRY; FOOD ANALYSIS; FOOD CONTAMINATION; FRUIT; GRAPE; IONIZATION; LIQUID CHROMATOGRAPHY; MASS SPECTROMETRY; ONION; VEGETABLE;

ATMOSPHERIC PRESSURE; CARBAMATES; CHROMATOGRAPHY, LIQUID; ELECTROCHEMISTRY; FRUIT; INSECTICIDES; MASS SPECTROMETRY; PESTICIDE RESIDUES; QUATERNARY AMMONIUM COMPOUNDS; SENSITIVITY AND SPECIFICITY; TEMPERATURE; VEGETABLES;

ALLIUM CEPA; VITIS SP.;

EID: 1242336774     PISSN: 00218561     EISSN: None     Source Type: Journal    
DOI: 10.1021/jf0343377     Document Type: Article

References (15)

1. Saunders, D. S.; Harper, C. In Principles and Methods of Toxicology; Hyes, A. W., Ed.; Raven Press: New York, 1994; Chapter 11, p 389.
2. Ting, K. C.; Kho, P. GC MIP AED method for pesticide-residue determination in fruits and vegetables. J. Assoc. Off Anal. Chem. 1991, 74, 991-998.
3. Moye, H. A.; Scherer, S. J.; St. John, P. A. Dynamic fluorogenic labeling of pesticides for HPLC: detection of N-methylcarbamates with o-phthalaldehyde. Anal. Lett. 1977, 10, 1049-1055.
4. De Kok, A.; Hiemstra, M.; Vreeker, C. P. Improved cleanup method for the multiresidue analysis of N-methylcarbamates in grains, fruits, and vegetables by means of HPLC with postcolumn reaction and fluorescence detection. Chromatographia 1987, 24, 469-476.
5. Page, J. M.; French, M. Determination of N-methylcarbamate insecticides in vegetables, fruits and feeds using solid-phase extraction cleanup in the normal phase. J. Assoc. Off. Anal. Chem. 1992, 75, 1073-1083.
6. Di Corcia, A.; Creszenci, C.; Lagana, A.; Sebastiani, E. Evaluation of a method based on liquid chromatography/electrospray/ mass spectrometry for analyzing carbamate insecticides in fruits and vegetables. J. Agric. Food Chem. 1996, 44, 1930-1938.
7. Chiron, S.; Valverde, A.; Fernandez-Alba, A.; Barcelo, D. Automated sample preparation for monitoring groundwater pollution by carbamate insecticides and their transformation products. J. AOAC Int. 1995, 78, 1346-1352.
8. Honing, M.; Rui, J.; Barcelo, D.; van Baar, B. M. L.; Brinkman, U. A. Th. Determination of ten carbamate pesticides in aquatic and sediment samples by liquid chromatography-ion spray and thermospray mass spectrometry. J. Chromatogr. A 1996, 733, 283-294.
9. Salau, J. S.; Honing, M.; Tauler, R.; Balcelo, D. Resolution and quantitative determination of coeluted pesticide mixtures in liquid chromatography-thermospray mass spectrometry by multivariate curve resolution. J. Chromatogr. A 1998, 79.5, 3-12.
10. Takino, M.; Yamagami, T.; Daishima, S. Simultaneous determination of N-methylcarbamate pesticides by LC/atmospheric pressure-ionization MS. Bunseki Kagaku 1997, 46, 555-561.
11. Fernandez, M.; Pico, Y.; Manes, J. Determination of carbamate residues in fruits and vegetables by matrix solid-phase dispersion and liquid chromatography-mass spectrometry. J. Chromatogr. A 2000, 871, 43-56.
12. Robb, D. B.; Covey, T. R.; Bruins, A. P. Atmospheric pressure photoionization: an ionization method for liquid chromatography-mass spectrometry. Anal. Chem. 2000, 72, 3653-3659.
13. Syage, J. A.; Evans, M. D.; Hanold, K. A. Photoionization mass spectrometry. Am. Lab. 2000, 32, 24-29.
14. Takino, M.; Daishima, S.; Yamaguchi, K. Determination of diquat and paraquat in water by liquid chromatography/electrospray-mass spectrometry using volatile ion-pairing reagents. Anal. Sci. 2000, 16, 707-711.
15. Takino, M.; Daishima, S.; Yamaguchi, K.; Nakahara, T. Determination of polycyclic aromatic hydrocarbons by liquid chromatography-electrospray ionization mass spectrometry using silver nitrate as a post-column reagent. J. Chromatogr. A 2000, 928, 53-61.