Primary and secondary coordination of crown ethers to scandium(III). Synthesis, properties and structures of the reaction products of ScCl 3(thf)3, ScCl3·6H2O and Sc(NO3)3·5H2O with crown ethers

Dalton Transactions

Volumn , Issue 5, 2003, Pages 857-865

  Brown, Michael D ^a   Levason, William ^a   Murray, David C ^a   Popham, Michael C ^a   Reid, Gillian ^a   Webster, Michael ^a  

^a UNIVERSITY OF SOUTHAMPTON   (United Kingdom)

Author keywords

[No Author keywords available]

Indexed keywords

CHLORINE; CROWN ETHERS; CRYSTAL STRUCTURE; DIMERS; ETHANE; ETHANOL; HYDROGEN BONDS; HYDROLYSIS; NUCLEAR MAGNETIC RESONANCE; SCANDIUM; SPECTROSCOPIC ANALYSIS; SYNTHESIS (CHEMICAL);

LATTICE WATER; LEWIS ACIDS; X-RAY CRYSTAL STRUCTURES;

COORDINATION REACTIONS;

EID: 12344276730     PISSN: 14779226     EISSN: None     Source Type: Journal    
DOI: 10.1039/b210458j     Document Type: Article

References (34)

1. (a) D. E. Fenton, in Comprehensive Coordination Chemistry, ed. G. Wilkinson, J. A. McCleverty and R. D. Gillard, Pergamon, Oxford, 1987, vol. 3, eh. 23;
2. (b) J. W. Steed and J. L. Atwood, Supramolecular Chemistry, Wiley, New York. 2000, eh. 3.
3. (a) For recent reviews see: S. A. Cotton, Polyhedron, 1999, 18, 1691;
4. (b) P. R. Meehan, D. A. Aris and G. R. Willey, Coord. Chem. Rev., 1999, 181, 121.
5. G. R. Willey, M. T. Lakin and N. W. Alcock, Chem. Commun., 1992, 1619;
6. G. R. Willey, M. T. Lakin and N. W. Alcock, J. Chem. Soc., Dalton Trans., 1993, 3407.
7. G. R. Willey, P. R. Meehan, M. D. Rudd and M. G. B. Drew, J. Chem. Soc., Dalton Trans., 1995, 811.
8. N. R. Strel'sova, V. K. Bel'ski, B. M. Bulychev and O. K. Kireeva, Zh. Neorg. Khim., 1992, 37, 1822.
9. W. Levason, M. C. Popham, G. Reid and M. Webster, Dalton Trans., 2003, 291.
10. (a) For lead references see: R. D. Rogers and A. N. Rollins, Inorg. Chim. Acta, 1995, 230, 177;
11. (b) R. D. Rogers and A. N. Rollins, J. Chem. Crystallogr., 1994, 24, 531;
12. (c) R. D. Rogers and A. N. Rollins, J. Chem. Crystallogr., 1994, 24, 321;
13. (d) R. D. Rogers, Inorg. Chim. Acta, 1988, 149, 307;
14. (e) R. D. Rogers and E. J. Voss, J. Coord Chem., 1988, 16, 405.
15. L. Deakin, W. Levason, M. C. Popham, G. Reid and M. Webster, J. Chem. Soc., Dalton Trans., 2000, 2439.
16. N. J. Hill, W. Levason, M. C. Popham, G. Reid and M. Webster, Polyhedron, 2002, 21, 1579.
17. L. E. Manzer, Inorg. Synth., 1982, 21, 135.
18. J. S. Bradshaw, G. Y. Hui, B. L. Haymore and J. J. Christensen, J. Heterocycl. Chem., 1973, 10, 1.
19. R. H. Blessing, J. Appl. Crystallogr., 1997, 30, 421.
20. G. M. Sheldrick, SHELXS 97, Program for crystal structure solution, University of Göttingen, Germany, 1997.
21. PATTY, The DIRDIF Program System P. T. Beurskens, G. Admiraal, G. Beurskens, W. P. Bosman, S. Garcia-Granda, R. O. Gould, J. M. M. Smits and C. Smykalla, Technical Report of the Crystallographic Laboratory, University of Nijmegen, The Netherlands, 1992.
22. G. M. Sheldrick, SHELXL 97, Program for crystal structure refinement, University of Göttingen, Germany, 1997.
23. P. R. Meehan and G. R. Willey, Inorg. Chim. Acta, 1999, 284, 71.
24. G. R. Willey, P. R. Meehan and M. G. B. Drew, Polyhedron, 1996, 15, 1397.
25. G. A. Kirakosyan, V. P. Tarasov and Yu. A. Buslaev, Magn. Reson. Chem., 1989, 27, 103.
26. Z. Jin, Y. Liu, S. Zhana, F. Yu and J. Ni, Hiiaxue Xtiebao, 1987, 45, 1048
27. (Chem. Abs., 1988, 108, 105242);
28. M. Tan, X. Can, N. Tang, J. Zhou, X. Wang and Y. Zhu, Wuli Huaxue Xuebao, 1990, 6, 5
29. (Chem. Abs., 1991, 115, 221711);
30. S. Ng and S. Hu, Wuli Huaxue Xuebao, 2000, 16, 804
31. (Chem. Abs., 2000, 133, 357492).
32. K. Nakamoto, Infrared Spectra of Inorganic and Coordination Compounds, Wiley, New York, 1970.
33. X. Can, N. Tang, Y. Zhu, Y. Zhai and M. Tan, Zhongguo Xitu Xuebao, 1989, 7, 13
34. (Chem. Abs., 1990, 112, 150561).