Copper oxide precipitates in NBS standard reference material 482

Journal of Research of the National Institute of Standards and Technology

Volumn 107, Issue 6, 2002, Pages 663-679

  Windsor, Eric S ^a   Carlton, Robert A ^b   Gillen, Greg ^a   Wight, Scott A ^a   Bright, David S ^a  

^a NATIONAL INSTITUTE OF STANDARDS AND TECHNOLOGY   (United States)

^b King of Prussia PA 19406 USA   (United States)

Author keywords

Copper gold alloy; Electron probe microanalysis; Metallography; NBS Standard Reference Material 482; Oxide inclusions; Sample preparation; Secondary ion mass spectrometry

Indexed keywords

COMPOSITION; COPPER METALLOGRAPHY; ELECTRON MICROSCOPY; GRINDING (MACHINING); OPTICAL MICROSCOPY; POLISHING; PRECIPITATION (CHEMICAL); SECONDARY ION MASS SPECTROMETRY; SILICA; STANDARDS; X RAY ANALYSIS;

ELECTRON PROBE MICROANALYSIS (EPMA);

COPPER OXIDES;

EID: 12244304155     PISSN: 1044677X     EISSN: None     Source Type: Journal    
DOI: 10.6028/jres.107.053     Document Type: Conference Paper

References (24)

1. K. F. J. Heinrich, et al., Preparation and Evaluation of SRM's 481 and 482 Gold-Silver and Gold-Copper Alloys for Microanalysis, NBS Special Publication 260-28 (1971).
2. K. F. J. Heinrich, Advances in X-ray Analysis 11, Plenum Press, New York (1968) p. 40.
3. K. F. J. Heinrich and H. Yakowitz, Absorption of Primary X-Rays in Electron Probe Microanalysis, Anal. Chem. 47 (14), 2408-2411 (1975).
4. D. A. Sewell, G. Love, and V. D. Scott, Universal Correction Procedure for Electron-Probe Microanalysis: II. The Absorption Correction, J. Phys. D Appl. Phys. 18 (7), 1245-1268 (1985).
5. G. F. Bastin, H. J. M. Heijligers, and F. J. J. vanLoo, A Further Improvement in the Gaussian φ (ρz) Approach for Matrix Correction in Quantitative Electron Probe Microanalysis, Scanning 8, 45-67 (1986).
6. J. L. Pouchou and F. Pichoir, Very High Elements X-Ray-Microanalysis - Recent Models of Quantification, J. Microsc. Spect. Elec. 11 (4), 229-250 (1986).
7. J. L. Pouchou and F. Pichoir, Quantitative Analysis of Homogeneous or Stratified Microvolumes Applying the Model "PAP," Electron Probe Quantitation, K. F. J. Heinrich and D. E. Newbury, eds., Plenum Press, New York (1991) pp. 31-75.
8. J. T. Armstrong, (personal communication).
9. J. T. Armstrong, Propagation of Errors in the Precision and Accuracy of Quantitative Electron Microprobe Analysis, Proc. Microscopy and Microanalysis, 7, Suppl. 2 (2001) pp. 670-671.
10. R. B. Marinenko, NIST Standards for Microanalysis and the Certification Process, J. Res. Natl. Inst. Stand. Technol. 107, 000-000 (2002).
11. R. A. Carlton, Ph.D. Thesis, Lehigh University, 2001.
12. E. S. Windsor, et al., SRM 482: Revisited After 30 Years, Proc. Microscopy and Microanalysis, 7, Suppl. 2 (2001) pp. 678-679.
13. R. E. Ricksecker and T. F. Bower, Copper and Copper Alloys, in Metallography and Microstructures, ASM Handbook, Vol. 9 (1985) pp. 399-414.
14. D. S. Bright, MacLispix: A Special Purpose Public Domain Image Analysis Program for the Macintosh, Microbeam Anal. 4, 151-163 (1995).
15. K. Kanaya and S. Okayama, Penetration and Energy-Loss Theory of Electrons in Solid Targets. J. Phys. D: Appl. Phys. 5, 43-58 (1972).
16. W. H. J. Vernon, First (Experimental) Report to the Atmospheric Corrosion Research Committee (of the British Non-Ferrous Metals Research Association), Trans. Faraday Soc. 19, 839-934 (1924).
17. N. B. Pilling and R. E. Bedworth, The Oxidation of Metals at High Temperatures, J. Inst. Met. 29, 529-591 (1923).
18. W. H. J. Vernon, Second Experimental Report to the Atmospheric Corrosion Research Committee (British Non-Ferrous Metals Research Association), Trans. Faraday Soc. 23, 113-204 (1927).
19. W. H. J. Vernon, A Laboratory Study of the Atmospheric Corrosion of Metals, Trans. Faraday Soc. 27, 255-277 (1931).
20. E. G. West, Copper and its Alloys, Ellis Horwood Limited, Great Britian (1982) pp. 13 and 85.
21. H. Pops, Metallurgy and Technology of Commercial Copper Electrical Conductor Wires, in Proceedings of Metallurgy, Processing and Applications of Metal Wires: State of the Art Technology and Challenges for the Future, H. G. Paris and D. K. Kim, eds., The Minerals, Metals & Materials Society, Warrendale, PA (1996) pp. 43-61.
22. L. E. Samuels, Metallographic Polishing by Mechanical Methods, American Society for Metals, Ohio (1982).
23. G. F. Vander Voort, Metallography Principles and Practice, ASM International, Ohio (1999).
24. G. M. Chalfant, Revealing Lead Inclusions in Leaded Steels, Met. Prog. 78, 77-79 (1960).