Synthesis and electrochemical studies of osmium(VI) complexes with five- and six-membered nitrogen-containing heterocycles; the solid-state structures of [OsO2Cl2L2] (L=NC5H 4-4-C≡N, N2C4H4, N 2C3H4)

Inorganica Chimica Acta

Volumn 355, Issue , 2003, Pages 69-80

  Mayboroda, Andrey ^a   Rheinwald, Gerd ^a   Lang, Heinrich ^a  

^a CHEMNITZ UNIVERSITY OF TECHNOLOGY   (Germany)

Author keywords

Complexes; Electrochemistry; Heterocycles; Osmium; X ray

Indexed keywords

ATOMS; CHLORINE COMPOUNDS; CRYSTALS; DYES; ELECTROCHEMISTRY; HYDROGEN; LIGANDS; MIXTURES; MOLAR RATIO; NITRIC ACID; NITROGEN; OSMIUM; OXYGEN; POLYMERS; TRANSITION METALS; X RAYS;

COMPLEXES; ELECTROCHEMICAL BEHAVIOUR; ELECTROCHEMICAL STUDIES; HETEROCYCLES; MONOCLINIC SPACE GROUPS; NITROGEN-CONTAINING HETEROCYCLES; OCTAHEDRALLY COORDINATED; TRANSITION-METAL OSMIUM;

SYNTHESIS (CHEMICAL);

ACETONE; HYDROCHLORIC ACID; HYDROGEN; METAL COMPLEX; METHANOL; NITROGEN DERIVATIVE; OSMIUM DERIVATIVE; POLYMER;

ARTICLE; CARBON NUCLEAR MAGNETIC RESONANCE; COMPLEX FORMATION; CRYSTAL STRUCTURE; ELECTROCHEMISTRY; INFRARED SPECTROSCOPY; PHOSPHORUS NUCLEAR MAGNETIC RESONANCE; PHYSICAL CHEMISTRY; PRECIPITATION; PROTON NUCLEAR MAGNETIC RESONANCE; SOLID STATE; STRUCTURE ANALYSIS; SYNTHESIS;

EID: 1142287601     PISSN: 00201693     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0020-1693(03)00297-4     Document Type: Article

References (33)

1. Gelmini L., Stephan D.W. Organometallics. 7:1988;849.
2. Kalck P. Polyhedron. 7:1988;2441.
3. Mutin R., Lucas C., Thivole-Cazat J., Dufand V., Dany F., Basset J.M. J. Chem. Soc., Chem. Commun. 1988;896.
4. McKenzie J., Robson R. J. Chem. Soc., Chem. Commun. 1988;112.
5. Garsia M.P., López A.M., Esteruelas M.A., Lahoz F.J., Oro L.A. J. Chem. Soc., Chem. Commun. 1988;793.
6. Esteruelas M.A., Garcia M.P., Lopez A.M., Oro L. Organometallics. 10:1991;127.
7. Sola E., Bakhmutov V.I., Torres F., Elduque A., Lopez J.A., Lahoz F., Werner H., Oro L.A. Organometallics. 17:1998;683.
8. Torres F., Sole E., Elduque A., Martinez A.P., Lahoz F.J., Oro L.A. Chem. Eur. J. 6:2000;2120.
9. El-Hendawy A.M., Griffith W.P., Taha F.I., Musa M.N. J. Chem Soc. Dalton Trans. 5:1989;901.
10. Imbe Y., Umakoshi K., Matsunani C., Sasaki Y. Inorg. Chem. 34:1995;813.
11. Che C.M., Lai T.F., Chung W.C., Schaefer W.P., Grey H.B. Inorg. Chem. 26:1987;3907.
12. Che C.M., Chung W.C., Lai T.F. Inorg. Chem. 27:1988;2801.
13. Maiboroda A., Rheinwald G., Lang H. Eur. J. Inorg. Chem. 2001;2263.
14. Griffith W.P. Wilkinson G. Osmium, Comprehensive Coordination Chemistry. 4:1987;519-633 Pergamon Press, Oxford.
15. Spek A.L. Acta Crystallogr. A46:1990;C34.
16. Area-Detector Absorption Corrections. Siemens Industrial Automation, Inc., Madison, WI, 1996.
17. G.M. Sheldrick, SHELX-97, Programs for Crystal Structure Analysis (Release 97-2), University of Göttingen, Germany, 1997.
18. International Tables for X-ray Crystallography, 1985, Vol. IV, Table 2.2B.
19. O. Bayer, Oxidative Keton-Spaltung. In: E. Müller (Ed.) Methoden der organischen Chemie, Band VII/2b, Teil II, G. Thieme Vlg., Stuttgart, 1976, 1978-1982, and references therein.
20. 5(Thf): W. Strohmeier, F.-J. Müller, Chem. Ber. 102 (1969) 3608.
21. Chen Ya., Ernhoffer R.E., Rex E. Transition Met. Chem. (London). 23:1998;375.
22. Pannell K.H., Iglesias R. Inorg. Chim. Acta. 33:1979;L161.
23. Borownlee R.T.C., Shehan B.P., Wedd A.G. Aust. J. Chem. 41:1988;1457.
24. Nakamoto K. Infrared and Raman Spectra of Inorganic and Coordination Compounds. 1997;Wiley, NY.
25. Carmona D., Ferrer J., Arilla J.M., Reyes J., Lahoz F.J., Elipe S., Modrego J., Oro L.A. Organometallics. 19:2000;798.
26. Chin K.F., Cheng Y.K., Cheung K.K., Guo C.X., Che C.M. J. Chem. Soc. Dalton. Trans. 18:1995;2967.
27. Nasri H., Scheidt W.R. Acta Crystallogr. C46:1990;1096.
28. Carmona D., Ferrer J., Atencio R., Lahoz F.J., Oro L.A. Organometallics. 14:1995;2057.
29. Tejel C., Ciriano M.A., Edwards A.J., Lahoz F.J., Oro L.A. Organometallics. 16:1997;45.
30. Carmona D., Ferrer J., Arilla J.M., Reyes J., Lahoz F.J., Elipe S., Modrego J., Oro L.A. Eur. J. Inorg. Chem. 2000;159.
31. Ruiz J., Florenciano F., Sánchez M.A., López G., Carmen Ramírez de Arellano M., Pérez J. Eur. J. Inorg. Chem. 2000;943.
32. Torres F., Sola E., Elduque A., Martínez A.P., Lahoz F.J., Oro L.A. Chem. Eur. J. 6:2000;2120.
33. Komeda S., Lutz M., Spek A.L., Chikuma M., Reedijk J. Inorg. Chem. 39:2000;4230.