Resolving ambiguities in two-dimensional NMR spectra: The 'TILT' experiment

Journal of Magnetic Resonance

Volumn 172, Issue 2, 2005, Pages 329-332

  Kupče, Eriks ^a   Freeman, Ray ^b  

^a Varian Limited UK   (United Kingdom)

^b JESUS COLLEGE   (United Kingdom)

Author keywords

Resolving ambiguities; Tilted projections; Two dimensional NMR

Indexed keywords

RESOLVING AMBIGUITIES; TILTED PROJECTIONS; TIME-DOMAIN SIGNAL;

CORRELATION METHODS; DATA ACQUISITION; FOURIER TRANSFORMS; MOLECULAR STRUCTURE; PROTONS; TIME DOMAIN ANALYSIS;

NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY;

AGITOXIN 1; CARBON; NITROGEN; SCORPION VENOM;

ARTICLE; CHEMISTRY; METHODOLOGY; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; THEORETICAL MODEL;

CARBON ISOTOPES; MAGNETIC RESONANCE SPECTROSCOPY; MODELS, THEORETICAL; NITROGEN ISOTOPES; SCORPION VENOMS;

EID: 11344269327     PISSN: 10907807     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.jmr.2004.11.007     Document Type: Article

References (21)

1. J. Jeener Ampère International Summer School 1971 Basko Polje Yugoslavia
2. W.P. Aue, E. Bartholdi, and R.R. Ernst Two-dimensional spectroscopy. Application to nuclear magnetic resonance J. Chem. Phys. 64 1976 2229
3. E. Kupče, and R. Freeman Reconstruction of the three-dimensional NMR spectrum of a protein from a set of plane projections J. Biomol. NMR 27 2003 383 387
4. E. Kupče, and R. Freeman Projection-reconstruction of three-dimensional NMR spectra J. Am. Chem. Soc. 125 2003 13958 13959
5. E. Kupče, and R. Freeman Fast reconstruction of four-dimensional NMR spectra from plane projections J. Biomol. NMR 28 2004 391 395
6. E. Kupče, and R. Freeman The Radon transform: a new scheme for fast multidimensional NMR Concepts Magn. Reson. 22 A 2004 4 11
7. E. Kupče, and R. Freeman The projection-reconstruction technique for speeding up multidimensional NMR spectroscopy J. Am. Chem. Soc. 126 2004 6429 6440
8. R. Freeman, and E. Kupče New methods for fast multidimensional NMR J. Biomol. NMR 27 2003 101 113
9. R.N. Bracewell Aust. J. Phys. 9 1956 198
10. K. Nagayama, P. Bachmann, K. Wüthrich, and R.R. Ernst The use of cross-sections and of projections in two-dimensional NMR spectroscopy J. Magn. Reson. 31 1978 133
11. 15N relaxation measurements, J. Biomol. NMR (2004) (in press)
12. G. Bodenhausen, and R.R. Ernst The accordion experiment, a simple approach to three-dimensional spectroscopy J. Magn. Reson. 45 1981 367 373
13. G. Bodenhausen, and R.R. Ernst Direct determination of rate constants of slow dynamic processes by two-dimensional 'Accordion' spectroscopy in nuclear magnetic resonance J. Am. Chem. Soc. 104 1982 1304 1309
14. K. Ding, and A. Gronenborn Novel 2D triple-resonance NMR experiments for sequential resonance assignments of proteins J. Magn. Reson. 156 2002 262 268
15. S. Kim, and T. Szyperski GFT NMR, a new approach to rapidly obtain precise high-dimensional NMR spectral information J. Am. Chem. Soc. 125 2003 1385 1393
16. β chemical shift assignment J. Biomol. NMR 28 2004 117 130
17. W. Kozminski, and I. Zhukov Multiple quadrature detection in reduced dimensionality experiments J. Biomol. NMR 26 2003 157 166
18. B. Simon, and M. Sattler Speeding up biomolecular NMR spectroscopy Angew. Chem. Int. Ed. 43 2004 782 786
19. A. Krezel, C. Khasibhatla, P. Hidalgo, R. McKinnon, and G. Wagner Solution structure of the potassium channel inhibitor agitoxin 2: callipers for probing channel geometry Protein Sci. 4 1995 1478 1489
20. 15N labeled proteins J. Am. Chem. Soc. 111 1989 1515 1517
21. L.E. Kay, P. Keifer, and T. Saarinen Pure absorption gradient-enhanced heteronuclear single-quantum correlation spectroscopy with improved sensitivity J. Am. Chem. Soc. 114 1992 10663 10665