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11244261814
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note
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The differential scanning calorimetric (DSC) analysis showed that the crystals of 1o undergo a phase transition on heating above 92°C, while those of 1t melted at 111°C; see ESI.
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18
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11244265378
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note
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We have experimental results that provide ample evidence for the participation of formyl hydrogen in hydrogen bonding. These results will be published elsewhere.
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19
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11244351086
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note
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The TGA analysis revealed no perceptible loss of solvent molecules on heating from 30 to 110°C. Presumably, the solvent molecules readily escape the lattice.
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20
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37049070979
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