Optimization of conditions for PTV large-volume injection combined with fast GC-MS

Journal of Chromatographic Science

Volumn 42, Issue 10, 2004, Pages 531-535

  Korenková, Eva ^a   Matisová, Eva ^b   Slobodník, Jaroslav ^a  

^a Environmental Institute Slovakia   (Slovakia)

^b SLOVAK UNIVERSITY OF TECHNOLOGY   (Slovakia)

Author keywords

[No Author keywords available]

Indexed keywords

ACETIC ACID ETHYL ESTER; ORGANOCHLORINE DERIVATIVE; ORGANOCHLORINE PESTICIDE; SOLVENT;

ARTICLE; BOOK; CAPILLARY GAS CHROMATOGRAPHY; CHROMATOGRAPHY; COLUMN CHROMATOGRAPHY; DECOMPOSITION; GAS CHROMATOGRAPHY; INJECTION; LARGE VOLUME INJECTION; MASS SPECTROMETRY; TEMPERATURE; TEMPERATURE DEPENDENCE; THERMAL REACTION; VAPORIZATION; VAPORIZER;

PERU TOMATO MOSAIC VIRUS;

EID: 11144342032     PISSN: 00219665     EISSN: None     Source Type: Journal    
DOI: 10.1093/chromsci/42.10.531     Document Type: Article

References (22)

1. P. Korytár, H.-G. Janssen, E. Matisová, and U.A.Th. Brinkman. Practical fast gas chromatography: methods, instrumentation and applications. Trends Anal. Chem. 21: 558-72 (2002).
2. E. Matisová and M. Dömötörová. Fast gas chromatography and its use in trace analysis, j. Chromatogr. A 1000: 199-221 (2003).
3. F. David, D.R. Gere, F. Scanlan, and P. Sandra. Instrumentation and applications of fast high-resolution capillary gas chromatography. J. Chromatogr. A. 842: 309-19 (1999).
4. P.G. van Ysacker, H.M. Snijders, H.-G.M. Janssen, and C.A. Cramers. The use of non-splitting injection techniques for trace analysis in narrow-bore capillary gas chromatography. J. High Resol. Chromatogr. 21: 491-97 (1998).
5. S. Hrouzková, M. Simeková, E. Matisová, and P. Korytár. Present trends in analysis of mixtures of organic compounds by fast gas chromatography. Chem. Listy. 96: 673-83 (2002).
6. P. Sandra and F. David. High-throughput capillary gas chromatography for the determination of polychlorinated biphenyls and fatty acid methyl esters in food samples. J. Chromatogr. Sci. 40: 248-53 (2002).
7. J.W. Cochran. Fast gas chromatography time-of-flight mass spectrometry of polychlorinated biphenyls and other environmental contaminants. J. Chromatogr. Sci. 40: 254-68 (2002).
8. P. Korytár, E. Matisová, H. Lefflerová, and J. Slobodník. Large volume injection in fast gas chromatography with on-column injector. J. High Resol. Chromatogr. 23: 149-55 (2000).
9. E. Matisová, M. Simeková, S. Hrouzková, P. Korytár, and M. Dömötörová. Factors influencing chromatographic data in fast gas chromatography with on-column injection. J. Sep. Sci. 25: 1325-31 (2002).
10. M. Dömötörová. Fast capillary gas chromatography and its use in pesticides analysis. Diploma Thesis, Department of Analytical Chemistry, Faculty of Chemical and food Technology, STU, Bratislava, 2001.
11. J. Zrostlíková, J. Hajslová, M. Godula, and K. Mastovská. Performance of programmed temperature vaporizer, pulsed splitless and on-column injection techniques in analysis of pesticide residues in plant matrices. J. Chromatogr. A 937: 73-87 (2001).
12. W. Engewald, J. Teske, and J. Efer. Programmed temperature vaporisers-based large volume injection in capillary gas chromatography. J. Chromatogr. A 842: 143-61 (1999).
13. E. Korenková, E. Matisová, and J. Slobodník. Large volume injection in capillary gas chromatography. Chem. Listy. 95: 528-39 (2001).
14. E. Korenková, E. Matisová, and J. Slobodník. Large volume injection in capillary gas chromatography using programmable temperature vaporizer injector. Chem. Listy. 96: 82-89 (2002).
15. European Union Water Framework Directive, Amended proposal COM, 2001, p. 17.
16. E. Korenková, E. Matisová, and J. Slobodník. Study on the feasibility of coupling large-volume injection to fast gas chromatography with mass spectrometric detection for analysis of organochlorine pesticides. J. Sep. Sci. 26: 1193-97 (2003).
17. C. Aguilar, F. Borrull, and R.M. Marcé. Determination of pesticides in environmental waters by solid-phase extraction and gas chromatography with electron-capture and mass spectrometry detection. J. Chromatogr. A 771: 221-31 (1997).
18. M. Godula, J. Hajslová, K. Mastovská, and J. Ksivánková. Optimization and application of the PTV injector for the analysis of pesticide residues. J. Sep. Sci. 24: 355-66 (2001).
19. H.G.J. Mol, P.J.M. Hendriks, H.-G. Janssen, C.A. Cramers, and U.A.Th. Brinkman. Large volume injection in capillary GC using PTV injectors: comparison of inertness of packing materials. J. High Resol. Chmmatogr. 18: 124-28 (1995).
20. U.S. EPA. Method 608.1: Organochlorine Pesticides in Waste Water. 821/R-93-010-A, National Technical Information Service, Springfield, VA, 1993.
21. U.S. EPA. Method 508: Determination of Chlorinated Pesticides in Ground Water by GC-ECD. EA-600/4-88-039, National Technical Information Service, Springfield, VA, 1991.
22. U.S. EPA. Method 505: Organohalide Pesticides and PCB products in water. 821/R-93-010-B, National Technical Information Service, Springfield, VA, 1989.