Synthesis, crystal structure, and high-resolution NMR spectroscopy of methyl 3-azido-2,3-dideoxy-4,6-di-O-p-tolylsulfonyl-α-d-xylo- hexopyranoside

Carbohydrate Research

Volumn 340, Issue 1, 2005, Pages 143-147

  Liberek, Beata ^a   Sikorski, Artur ^a   Konitz, Antoni ^a,b  

^a UNIVERSITY OF GDA SK   (Poland)

^b GDANSK UNIVERSITY OF TECHNOLOGY   (Poland)

Author keywords

Methyl 3 azido 2,3 dideoxy d xylo hexopyranoside, tosylated; O Protection, influence on chemical shift; X ray diffraction, single crystal

Indexed keywords

CHEMICAL SHIFT; HEXOPYRANOSIDE; PRECURSORS;

COMPLEXATION; CRYSTAL STRUCTURE; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; ORGANIC COMPOUNDS; SINGLE CRYSTALS; X RAY DIFFRACTION ANALYSIS;

SYNTHESIS (CHEMICAL);

CARBOHYDRATE DERIVATIVE; METHYL 3 AZIDO 2,3 DIDEOXY 4,6 DI O 4 TOLYLSULFONYL ALPHA DEXTRO XYLOHEXOPYRANOSIDE; METHYL 3 AZIDO 2,3 DIDEOXY 6 O 4 TOLYLSULFONYL ALPHA DEXTRO XYLOHEXOPYRANOSIDE; PYRANOSIDE; UNCLASSIFIED DRUG;

ANALYTIC METHOD; ARTICLE; CARBOHYDRATE ANALYSIS; CARBON NUCLEAR MAGNETIC RESONANCE; CHEMICAL ANALYSIS; CRYSTAL STRUCTURE; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; PRIORITY JOURNAL; PROTON NUCLEAR MAGNETIC RESONANCE; STRUCTURE ANALYSIS; X RAY DIFFRACTION;

AZIDES; CARBOHYDRATE CONFORMATION; CRYSTALLIZATION; CRYSTALLOGRAPHY, X-RAY; GLYCOSIDES; HYDROGEN BONDING; MAGNETIC RESONANCE SPECTROSCOPY; MODELS, MOLECULAR; MOLECULAR STRUCTURE; NUCLEAR MAGNETIC RESONANCE, BIOMOLECULAR; X-RAY DIFFRACTION;

EID: 11144305777     PISSN: 00086215     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.carres.2004.10.016     Document Type: Article

References (10)

1. B. Liberek, A. Da̧browska, R. Frankowski, M. Matuszewska, and Z. Smiatacz Carbohydr. Res. 337 2002 1803 1820
2. B. Liberek, A. Sikorski, A. Melcer, and A. Konitz Carbohydr. Res. 338 2003 795 799
3. G.M. Sheldrick Acta Crystallogr., Sect. A 46 1990 467 473
4. G.M. Sheldrick shelxl-97; Program for the Refinement of Crystal Structures 1997 University of Goetingen Goetingen
5. C.K. Johnson ortep II; Report ORNL-5138 1976 Oak Ridge National Laboratory Oak Ridge, TN
6. S. Motherwell, and S. Clegg pluto-78; Program for Drawing Crystal and Molecular Structure 1978 University of Cambridge Cambridge
7. M. Nardelli Comput. Chem. 7 1983 95 97
8. M. Nardelli J. Appl. Crystallogr. 28 1995 659
9. F.H. Allen, O. Kennard, D.G. Watson, L. Brammer, A.G. Orpen, and R. Taylor J. Chem. Soc., Perkin Trans. 2 1987 S1 19
10. D. Cremer, and J.A. Pople J. Am. Chem. Soc. 97 1975 1354 1358