Complete 1H and 13C NMR assignments for two new monodesmoside saponins from Pentaclethra macroloba (Willd.) Kuntze

Magnetic Resonance in Chemistry

Volumn 42, Issue 8, 2004, Pages 695-699

  Viana, Francisco Arnaldo ^a   Pouliquen, Yvone Brígido M ^b   Andrade Neto, Manoel ^b   Santiago, Gilvandete Maria P ^b   Pessoa, Otília Deusdênia L ^b   Rodrigues Filho, Edson ^c   Braz Filho, Raimundo ^d  

^a DEPARTAMENTO DE FÍSICA   (Brazil)

^b FEDERAL UNIVERSITY OF CEARÁ   (Brazil)

^c FEDERAL UNIVERSITY OF SÃO CARLOS   (Brazil)

^d UNIVERSIDADE ESTADUAL DO NORTE FLUMINENSE DARCY RIBEIRO   (Brazil)

Author keywords

1D NMR; 2D NMR; 13C NMR; 1H NMR; Chemical shift assignments; Monodesmoside saponin; NMR; Pentaclethra macroloba

Indexed keywords

CHEMICAL SHIFT; ELECTROSPRAY IONIZATION; METABOLITES; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY;

13C NMR; 1D NMR; 1H NMR; 2-D NMR; CHEMICAL SHIFT ASSIGNMENT; MONODESMOSIDE SAPONIN; NMR ASSIGNMENT; NMR STUDIES; PENTACLETHRUM MACROLOBA; SPECTRAL DATA;

MASS SPECTROMETRY;

SAPONIN DERIVATIVE; 3 O ((O GLUCOPYRANOSYL 1 2 O GLUCOPYRANOSYL 1 4 GLUCOPYRANOSYL 1 3 O RHAMNOPYRANOSYL 1 2)(O GLUCOPYRANOSYL 1 3 O GLUCOPYRANOSYL 1 4))ARABINOPYRANOSYLHEDERAGENIN; 3 O ((O GLUCOPYRANOSYL 1 2 O GLUCOPYRANOSYL 1 4 GLUCOPYRANOSYL 1 3 O RHAMNOPYRANOSYL 1 2)(O GLUCOPYRANOSYL 1 3 O GLUCOPYRANOSYL 1 4))ARABINOPYRANOSYLOLEANOLIC ACID; 3-O-((O-GLUCOPYRANOSYL--1-2-O-GLUCOPYRANOSYL-1-4-GLUCOPYRANOSYL-1-3-O-RHAMNOPYRANOSYL-1-2)(O-GLUCOPYRANOSYL-1-3-O-GLUCOPYRANOSYL-1-4))ARABINOPYRANOSYLOLEANOLIC ACID; 3-O-((O-GLUCOPYRANOSYL-1-2-O-GLUCOPYRANOSYL-1-4-GLUCOPYRANOSYL-1-3-O-RHAMNOPYRANOSYL-1-2)(O-GLUCOPYRANOSYL-1-3-O-GLUCOPYRANOSYL-1-4))ARABINOPYRANOSYLHEDERAGENIN; CARBON; HYDROGEN; SAPOGENIN; SAPONIN;

ANALYTIC METHOD; ARTICLE; BARK; CARBON NUCLEAR MAGNETIC RESONANCE; CHEMICAL STRUCTURE; ELECTROSPRAY MASS SPECTROMETRY; LEGUME; NUCLEAR OVERHAUSER EFFECT; PROTON NUCLEAR MAGNETIC RESONANCE; STRUCTURE ANALYSIS; CARBOHYDRATE ANALYSIS; CHEMISTRY; ISOLATION AND PURIFICATION; MOLECULAR GENETICS; NUCLEAR MAGNETIC RESONANCE;

CARBOHYDRATE SEQUENCE; CARBON ISOTOPES; FABACEAE; HYDROGEN; MOLECULAR SEQUENCE DATA; MOLECULAR STRUCTURE; NUCLEAR MAGNETIC RESONANCE, BIOMOLECULAR; PLANT BARK; SAPOGENINS; SAPONINS;

EID: 10944222157     PISSN: 07491581     EISSN: None     Source Type: Journal    
DOI: 10.1002/mrc.1421     Document Type: Article

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