메뉴 건너뛰기




Volumn 59, Issue 12, 2004, Pages 923-928

Nonequivalence behavior studies for the direct determination of enantiomeric purity and absolute configuration of timolol by NMR

Author keywords

[No Author keywords available]

Indexed keywords

TIMOLOL;

EID: 10844250182     PISSN: 00317144     EISSN: None     Source Type: Journal    
DOI: None     Document Type: Article
Times cited : (4)

References (33)
  • 1
    • 0026749348 scopus 로고
    • Chromatographic resolution of the chiral isomers of several beta-blockers over cellulose tris(3,5-dimethylphenylcarbamate) chiral stationary phase
    • Ching CB, Lim BG, Lee EJ, Ng DC (1992) Chromatographic resolution of the chiral isomers of several beta-blockers over cellulose tris(3,5- dimethylphenylcarbamate) chiral stationary phase. Chirality 4: 17407.
    • (1992) Chirality , vol.4 , pp. 17407
    • Ching, C.B.1    Lim, B.G.2    Lee, E.J.3    Ng, D.C.4
  • 3
    • 0024461298 scopus 로고
    • Separation and quantitation of (R)- and (S)-atenolol in human plasma and urine using an alpha 1-AGP column
    • Enquist M, Hermansson J (1989) Separation and quantitation of (R)- and (S)-atenolol in human plasma and urine using an alpha 1-AGP column. Chirality 1: 209-215.
    • (1989) Chirality , vol.1 , pp. 209-215
    • Enquist, M.1    Hermansson, J.2
  • 4
    • 0025009022 scopus 로고
    • Separation of the enantiomers of b-receptor blocking agents and other cationic drugs using the CHIRAL-AGP column. Binding properties and characterization of immobilized AGP
    • Enquist M, Hermansson J (1990) Separation of the enantiomers of b-receptor blocking agents and other cationic drugs using the CHIRAL-AGP column. Binding properties and characterization of immobilized AGP. J Chromatogr 519: 285.
    • (1990) J Chromatogr , vol.519 , pp. 285
    • Enquist, M.1    Hermansson, J.2
  • 5
    • 0025977150 scopus 로고
    • Chromatographic resolution of 1,2-amino alcohols on a chiral stationary phase containing N,N′-(3,5-dinitrobenzoyl)-trans-1,2-diaminocyclohexane Theoretical and practical aspects
    • Gasparrini F, Misiti D, Villani C, La Torre F (1991) Chromatographic resolution of 1,2-amino alcohols on a chiral stationary phase containing N,N′-(3,5-dinitrobenzoyl)-trans-1,2-diaminocyclohexane Theoretical and practical aspects. J Chromatogr 539: 25-36.
    • (1991) J Chromatogr , vol.539 , pp. 25-36
    • Gasparrini, F.1    Misiti, D.2    Villani, C.3    La Torre, F.4
  • 6
    • 0034492701 scopus 로고    scopus 로고
    • High performance liquid chromatographic enantionter separation of beta-blocking agents with a new isothiocyanate type chiral derivatizing agent
    • Gyeresi A, Peter M, Fulop F (2000) High performance liquid chromatographic enantionter separation of beta-blocking agents with a new isothiocyanate type chiral derivatizing agent. Acta Pharm Hung 70: 138-145.
    • (2000) Acta Pharm Hung , vol.70 , pp. 138-145
    • Gyeresi, A.1    Peter, M.2    Fulop, F.3
  • 7
    • 0026598093 scopus 로고
    • Investigation of enantioselectivity and enantiomeric elution order of propranolol and its ester derivatives on an ovomucoid bonded column
    • Haginaka J, Seyama C, Yasuda H, Takahashi K (1990) Investigation of enantioselectivity and enantiomeric elution order of propranolol and its ester derivatives on an ovomucoid bonded column. J Chromatogr A 598: 67-72.
    • (1990) J Chromatogr A , vol.598 , pp. 67-72
    • Haginaka, J.1    Seyama, C.2    Yasuda, H.3    Takahashi, K.4
  • 8
    • 0028892478 scopus 로고
    • Determination of optical purity of timolol maleate by proton nuclear magnetic resonance spectroscopy with chiral Pr(III) shift reagent
    • Hanna GM, Lau-Cam CA (1995) Determination of optical purity of timolol maleate by proton nuclear magnetic resonance spectroscopy with chiral Pr(III) shift reagent. J Pharm Biomed Anal 1313-1319.
    • (1995) J Pharm Biomed Anal , pp. 1313-1319
    • Hanna, G.M.1    Lau-Cam, C.A.2
  • 9
    • 0000178878 scopus 로고
    • 1-acid glycoprotein column
    • 1-acid glycoprotein column. J Chromatogr 325: 379-184.
    • (1985) J Chromatogr , vol.325 , pp. 379-184
    • Hermansson, J.1
  • 10
    • 0019276840 scopus 로고
    • Simultaneous determination of d- and l-propranolol in human plasma by high-performance liquid chromatography
    • Hermansson J, von Bahr C (1980) Simultaneous determination of d- and l-propranolol in human plasma by high-performance liquid chromatography. J Chromatogr 221: 109-17.
    • (1980) J Chromatogr , vol.221 , pp. 109-117
    • Hermansson, J.1    Von Bahr, C.2
  • 11
    • 0034698506 scopus 로고    scopus 로고
    • Experimental support differenciating two proposed chiral recognition models for the resolution of N-(3,5-dinitrobenzoyl)-alpha-arylalkylamines on high-performance liquid chromatography chiral stationary phases
    • Hyun MH, Ryoo JJ, Pirkle WH (2000) Experimental support differenciating two proposed chiral recognition models for the resolution of N-(3,5-dinitrobenzoyl)-alpha-arylalkylamines on high-performance liquid chromatography chiral stationary phases. J Chromatogr 886: 47-53.
    • (2000) J Chromatogr , vol.886 , pp. 47-53
    • Hyun, M.H.1    Ryoo, J.J.2    Pirkle, W.H.3
  • 12
    • 0024463818 scopus 로고
    • Beta-adrenoceptor antagonist activities and binding affinities of timolol enantiomers in rat atria
    • Karhuvaara S, Kaila T, Huupponen R (1989) Beta-adrenoceptor antagonist activities and binding affinities of timolol enantiomers in rat atria. J Pharm Pharmacol 41: 649-650.
    • (1989) J Pharm Pharmacol , vol.41 , pp. 649-650
    • Karhuvaara, S.1    Kaila, T.2    Huupponen, R.3
  • 13
    • 0023768529 scopus 로고
    • Direct enantiomeric separation of betaxolol with applications to analysis of bulk drug and biological samples
    • Krstulovic AM, Fouchet MH, Bruke JT, Gillet G, Durand A (1988) Direct enantiomeric separation of betaxolol with applications to analysis of bulk drug and biological samples. J Chromatogr 452: 477-483.
    • (1988) J Chromatogr , vol.452 , pp. 477-483
    • Krstulovic, A.M.1    Fouchet, M.H.2    Bruke, J.T.3    Gillet, G.4    Durand, A.5
  • 14
    • 0000494290 scopus 로고
    • The significance of HPLC time scale: An example of interconvertible enantiomers
    • Mannschreck A, Zinner H, Paustet N (1989) The significance of HPLC time scale: An example of interconvertible enantiomers. Chimia 43: 165-166.
    • (1989) Chimia , vol.43 , pp. 165-166
    • Mannschreck, A.1    Zinner, H.2    Paustet, N.3
  • 15
    • 0028598455 scopus 로고
    • Studies of ovomucoid-, avidin-, conalbumin- and flavoprotein-conjugated chiral stationary phases for separation of enantiomers by high-performance liquid chromatography
    • Mano N, Oda Y, Asakawa N, Yoshida Y, Sato T, Miwa T (1994) Studies of ovomucoid-, avidin-, conalbumin- and flavoprotein-conjugated chiral stationary phases for separation of enantiomers by high-performance liquid chromatography. J Chromatogr A 687: 223-232.
    • (1994) J Chromatogr A , vol.687 , pp. 223-232
    • Mano, N.1    Oda, Y.2    Asakawa, N.3    Yoshida, Y.4    Sato, T.5    Miwa, T.6
  • 17
    • 0023922018 scopus 로고
    • Stereoselectivity of beta-adrenergic antagonists: R-enantiomers show increased selectivity for beta-2 receptors in ciliary process
    • Nathanson JA (1988) Stereoselectivity of beta-adrenergic antagonists: R-enantiomers show increased selectivity for beta-2 receptors in ciliary process. J Pharmacol Exp Ther 245: 94-101.
    • (1988) J Pharmacol Exp Ther , vol.245 , pp. 94-101
    • Nathanson, J.A.1
  • 18
    • 0027308864 scopus 로고
    • Chiral separations of β-blocking drug substances using derivatization with chiral reagents and normal-phase high-performance liquid chromatography
    • Olsen L, K Brønnum-Hansen K, Helboe P, Jørgensen GH, Kryger S (1993) Chiral separations of β-blocking drug substances using derivatization with chiral reagents and normal-phase high-performance liquid chromatography. J Chromatogr 636: 231-241.
    • (1993) J Chromatogr , vol.636 , pp. 231-241
    • Olsen, L.K.1    Brønnum-Hansen, K.2    Helboe, P.3    Jørgensen, G.H.4    Kryger, S.5
  • 19
    • 0035794055 scopus 로고    scopus 로고
    • Liquid chromatographic enantioseparation of beta-blocking agents with (1R,2R)-1,3-diacetoxy-1-(4-nitro-phenyl)-2-propylisothiocyanate as derivatizing agent
    • Peter M, Gyeresi A, Fulop F (2001) Liquid chromatographic enantioseparation of beta-blocking agents with (1R,2R)-1,3-diacetoxy-1-(4-nitro- phenyl)-2-propylisothiocyanate as derivatizing agent. J Chromatogr 910: 247-253.
    • (2001) J Chromatogr , vol.910 , pp. 247-253
    • Peter, M.1    Gyeresi, A.2    Fulop, F.3
  • 20
    • 0025741080 scopus 로고
    • Chiral stationary phase designed for β-blockers
    • Pirkle WH, Burke JA (1991) Chiral stationary phase designed for β-blockers. J Chromatogr 557: 173-185.
    • (1991) J Chromatogr , vol.557 , pp. 173-185
    • Pirkle, W.H.1    Burke, J.A.2
  • 21
    • 0001151298 scopus 로고
    • A widely useful chiral stationary phase for the high-performance liquid chromatography separation of enantiomers
    • Pirkle WH, Finn JM, Schreiner JL, Hamper BC (1981) A widely useful chiral stationary phase for the high-performance liquid chromatography separation of enantiomers. J Am Chem Soc 103: 3464-3466.
    • (1981) J Am Chem Soc , vol.103 , pp. 3464-3466
    • Pirkle, W.H.1    Finn, J.M.2    Schreiner, J.L.3    Hamper, B.C.4
  • 22
    • 0022381779 scopus 로고
    • Bronchial beta-adrenoceptor blockade following eyedrops of timolol and its isomer L-714,465 in normal subjects
    • Richards R, Tattersfield AE (1985) Bronchial beta-adrenoceptor blockade following eyedrops of timolol and its isomer L-714,465 in normal subjects. Br J Clin Pharmacol 20: 459-462.
    • (1985) Br J Clin Pharmacol , vol.20 , pp. 459-462
    • Richards, R.1    Tattersfield, A.E.2
  • 23
    • 0023429019 scopus 로고
    • Comparison of the airway response to eye drops of timolol and its isomer L-714,465 in asthmatic subjects
    • Richards R, Tattersfield AE (1987) Comparison of the airway response to eye drops of timolol and its isomer L-714,465 in asthmatic subjects. Br J Clin Pharmaco 24: 485-491.
    • (1987) Br J Clin Pharmaco , vol.24 , pp. 485-491
    • Richards, R.1    Tattersfield, A.E.2
  • 26
    • 0019196959 scopus 로고
    • Stereospecific assay for (-)- and (+)-propranolol in human and dog plasma
    • Silber B, Riegelman S (1980) Stereospecific assay for (-)- and (+)-propranolol in human and dog plasma. J Pharmacol Exp Ther 215: 643-648.
    • (1980) J Pharmacol Exp Ther , vol.215 , pp. 643-648
    • Silber, B.1    Riegelman, S.2
  • 27
    • 0019964117 scopus 로고
    • Procedure for the chiral derivatization and chromatographic resolution of R-(+)- and S-(-)-propranolol
    • Thompson JA, Holtzman JL, Tsuru M, Lerman CL (1982) Procedure for the chiral derivatization and chromatographic resolution of R-(+)- and S-(-)-propranolol. J Chromatogr 238: 470-475.
    • (1982) J Chromatogr , vol.238 , pp. 470-475
    • Thompson, J.A.1    Holtzman, J.L.2    Tsuru, M.3    Lerman, C.L.4
  • 28
    • 0017078262 scopus 로고
    • Stereospecific binding of timolol, a beta-adrenergic blocking agent
    • Tocco DJ, Hooke KF, Deluna FA, Duncan AE (1976) Stereospecific binding of timolol, a beta-adrenergic blocking agent. Drug Metab Dispos 4: 323-329.
    • (1976) Drug Metab Dispos , vol.4 , pp. 323-329
    • Tocco, D.J.1    Hooke, K.F.2    Deluna, F.A.3    Duncan, A.E.4
  • 29
    • 0031009085 scopus 로고    scopus 로고
    • Enantioseparation of beta-blockers labeled with chiral fluorescent reagent, R(-)-DBD-PyNCS, by reversed-phase liquid chromatography
    • Toyo'oko T, Toriumi M, Ishii Y (1997) Enantioseparation of beta-blockers labeled with chiral fluorescent reagent, R(-)-DBD-PyNCS, by reversed-phase liquid chromatography. J Pharm Biomed Anal 15: 1467-1476.
    • (1997) J Pharm Biomed Anal , vol.15 , pp. 1467-1476
    • Toyo'oko, T.1    Toriumi, M.2    Ishii, Y.3
  • 30
    • 0021758558 scopus 로고
    • The direct enantiomeric determination of (-)- and (+)-propranolol in human serum by high-performance liquid chromatography on a chiral stationary phase
    • Wainer IW, Doyle TD, Donn KH, Powell JR (1984) The direct enantiomeric determination of (-)- and (+)-propranolol in human serum by high-performance liquid chromatography on a chiral stationary phase. J Chromatogr 306: 405-411
    • (1984) J Chromatogr , vol.306 , pp. 405-411
    • Wainer, I.W.1    Doyle, T.D.2    Donn, K.H.3    Powell, J.R.4
  • 32
    • 0023772827 scopus 로고
    • Resolution of enantiomeric drugs of some β-amino alcohols as their urea derivatives by high-performance liquid chromatography on a chiral stationary phase
    • Yang Q, Sun ZP, Ling DK (1988) Resolution of enantiomeric drugs of some β-amino alcohols as their urea derivatives by high-performance liquid chromatography on a chiral stationary phase. J Chromatogr 447: 208-211.
    • (1988) J Chromatogr , vol.447 , pp. 208-211
    • Yang, Q.1    Sun, Z.P.2    Ling, D.K.3
  • 33
    • 0025616917 scopus 로고
    • Resolution of the enantiomers of some beta-amino alcohols using chiral derivatization and reversed-phase liquid chromatography
    • Zhou and Sun (1990) Resolution of the enantiomers of some beta-amino alcohols using chiral derivatization and reversed-phase liquid chromatography. Yao Xue Xue Bao 25: 311-314.
    • (1990) Yao Xue Xue Bao , vol.25 , pp. 311-314
    • Zhou1    Sun2


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.