β-cyclodextrin columns for separation of fluorous and non-fluorous compounds: How to use β-cyclodextrin columns in fluorous mixture synthesis and racemic synthesis

Synlett

Volumn , Issue 15, 2004, Pages 2713-2716

  Mikami, Koichi ^a   Matsuzawa, Hiroshi ^a   Tekeuchi, Seiji ^b   Nakamura, Yutaka ^b   Curran, Dennis P ^c  

^a TOKYO INSTITUTE OF TECHNOLOGY   (Japan)

^b NIIGATA UNIVERSITY OF PHARMACY AND APPLIED LIFE SCIENCES   (Japan)

^c UNIVERSITY OF PITTSBURGH   (United States)

Author keywords

cyclodextrin; Chromatography; Combinatorial chemistry; Fluorous mixture synthesis; Racemic synthesis

Indexed keywords

BETA CYCLODEXTRIN; FLUORINE DERIVATIVE; WATER;

ARTICLE; CHROMATOGRAPHIC COLUMN; CHROMATOGRAPHY; COMBINATORIAL CHEMISTRY; DEVICE; FLUOROUS MIXTURE SYNTHESIS; LABORATORY; RACEMIC MIXTURE; RACEMIC SYNTHESIS; SYNTHESIS; WATER CONTENT;

EID: 10844233858     PISSN: 09365214     EISSN: None     Source Type: Journal    
DOI: 10.1055/s-2004-835649     Document Type: Article

References (18)

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4. (d) Curran, D. P. In Handbook of Fluorous Chemistry; Gladysz, J.; Curran, D. P.; Horváth, I. T., Eds.; Wiley-VCH: Weinheim, 2004, Chapt. 7, 8.
5. (e) Curran, D. P. Synlett 2001, 1488.
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14. Nakamura, Y.; Takeuchi, S.; Okumura, K.; Ohgo, Y.; Matsuzawa, H.; Mikami, K. Tetrahedron Lett. 2003, 44, 6221.
15. GL cart is commercially available from GL Sciences. URL of GL Sciences: http://www.gls.co.jp/
16. Wilson, L. D.; Verrall, R. E. J. Phys. Chem. B 1997, 101, 9270.
17. Curran, D. P.; Dandapani, S.; Werner, S.; Matsugi, M. Synlett 2004, 1545.
18. Mismatched compounds with fluorous or non-fluorous tags are now under investigation with OA-7000 and -7100, in particular.