Conventional, microwave induced and photochemical fries rearrangement of resorcinol diacetate

Bulletin of the Korean Chemical Society

Volumn 25, Issue 10, 2004, Pages 1447-1448

  Kim, Ji Hoon ^a   Yoon, Hyo Jung ^a   Chae, Woo Ki ^a  

^a Seoul National University   (South Korea)

Author keywords

Fries rearrangement; Resorcinol

Indexed keywords

ACETOACETIC ACID; RESORCINOL DERIVATIVE; RESORCINOL DIACETATE; UNCLASSIFIED DRUG;

ARTICLE; CHEMICAL REACTION; CHEMICAL STRUCTURE; FRIES REARRANGEMENT REACTION; HEATING; MICROWAVE IRRADIATION; MICROWAVE RADIATION; PHOTOCHEMISTRY; REACTION ANALYSIS; REACTION TIME; STRUCTURE ANALYSIS; SYNTHESIS;

EID: 10644260336     PISSN: 02532964     EISSN: None     Source Type: Journal    
DOI: 10.5012/bkcs.2004.25.10.1447     Document Type: Article

References (9)

1. (a) Sammes, P. G.; Kennewell, P. D. J. Chem. Soc. Perkin Trans. 1 1980, 170.
2. (b) Boyer, J. L.; Krum, J. E.; Myers, M. C.; Fazal, A. N.; Wigal, C. T. J. Org. Chem. 2000, 65, 4712.
3. (c) Kotnis, A. S. Tetrahedron Letters 1991, 29, 3441.
4. Stealey, M. A.; Shone, R. L.; Miyano, M. Synthetic Communications 1990, 20(12), 1869.
5. A modified domestic microwave oven which produces 2450 MHz radiation (700W) was used for irradiation.
6. Blatt, A. H. Org. Reaction; Wiley: New York, U.S.A., 1940; Vol. 1, p 342.
7. A solution of 129 mg of 1 in 20 mL of diethylether was transferred to a quartz cell and degassed with purified nitrogen. The sample was irradiated with 16-RPR-254 nm lamps for 10 hours.
8. Mirranda, M. A. Organic Photochemistry and Photobiology; Horspool, W. M.; Song, P. S., Eds.; CRC Press: New York, U.S.A., 1995; p 570.
9. 4: 194.0579 Found 194.0577.