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10444237228
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int = 0.028). Final R1(2σ) = 0.0355, wR2(all data) = 0.0986.
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24
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note
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2: C, 51.38; H, 4.84; N, 9.55. Found: C, 51.05; H, 4.99; N, 9.48.
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10444240267
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note
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2 at 60°C for 2 h in a sealed ampule. The mixture was filtered, the solution was concentrated in vacuo, and hexane was added to afford orange crystals of 4 (90 mg, 77%). See the Supporting Information for analytical data.
-
-
-
-
42
-
-
10444228881
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-
note
-
int = 0.027). Final R1(2σ) = 0.0469, wR2(all data) = 0.1271.
-
-
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43
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1842429601
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