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note
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w=0.0687 . CCDC-219155 for 1 and 219156 for 2. Suitable single crystals of 1 and 2 were selected and mounted on a Bruker Smart 1000 CCD diffractometer equipped with graphite monochromated Mo K α radiation ( λ=0.71073 Å by ω -2 θ scan technique at 293(2) K. Unit cell dimensions were obtained with least-squares refinements and all structures were solved by direct methods using SHELXS-97 program.
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