Synthesis and X-ray crystal structures of hydridotris(3,5- dimethylpyrazolyl)borate (Tp′) molybdenum(VI) bis(imido) complexes

Polyhedron

Volumn 23, Issue 1, 2004, Pages 189-194

  Gibson, Vernon C ^a   Redshaw, Carl ^b   Clegg, William ^c   Elsegood, Mark R J ^d   Siemeling, Ulrich ^e   Türk, Thomas ^e  

^a IMPERIAL COLLEGE LONDON   (United Kingdom)

^b UNIVERSITY OF EAST ANGLIA   (United Kingdom)

^c NEWCASTLE UNIVERSITY   (United Kingdom)

^d LOUGHBOROUGH UNIVERSITY   (United Kingdom)

^e UNIVERSITY OF KASSEL   (Germany)

Author keywords

Bis(imido); Molybdenum; Structures; Synthesis; Tris(pyrazolyl)borate

Indexed keywords

CRYSTALS; MOLYBDENUM COMPOUNDS;

BIS(IMIDO); CRYSTALLINE SOLIDS; IMIDO COMPLEXES; OCTAHEDRAL STRUCTURES; REFLUXING; TRIS(PYRAZOLYL)BORATES; X RAY CRYSTAL STRUCTURES;

SYNTHESIS (CHEMICAL);

BORIC ACID; CRYSTALLIN; HYDRIDOTRIS(3,5 DIMETHYLPYRAZOLYL)BORATE; MOLYBDENUM; UNCLASSIFIED DRUG;

ARTICLE; CHEMICAL REACTION; COMPLEX FORMATION; CRYSTAL STRUCTURE; STEREOCHEMISTRY; X RAY CRYSTALLOGRAPHY;

EID: 0742321945     PISSN: 02775387     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.poly.2003.10.005     Document Type: Article

References (22)

1. Schrock R.R. Acc. Chem. Res. 23:1990;158.
2. Bell A., Clegg W., Dyer P.W., Elsegood M.R.J., Gibson V.C., Marshall E.L. Chem. Commun. 1994;2547.
3. Gibson V.C., Redshaw C., Clegg W., Elsegood M.R.J., Siemeling U., Türk T. J. Chem. Soc., Dalton Trans. 1996;4513.
4. Siemeling U., Türk T., Schoeller W.W., Redshaw C., Gibson V.C. Inorg. Chem. 37:1998;4738.
5. Gibson V.C., Marshall E.L., Redshaw C., Clegg W., Elsegood M.R.J. J. Chem. Soc., Dalton Trans. 1996;4197.
6. Barrie P., Coffey T.A., Forster G.D., Hogarth G. J. Chem. Soc., Dalton Trans. 1999;4519.
7. Gamble A.S., Boncella J.M. Organometallics. 12:1993;2814.
8. Sundermeyer J., Putterlik J., Foth M., Field J.S., Ramesar N. Chem. Ber. 127:1994;1201.
9. Scheuer S., Fischer J., Kress J. Organometallics. 14:1995;2627.
10. Vaughan W.M., Abboub K.A., Boncella J.M. J. Organomet. Chem. 485:1995;37.
11. Boncella J.M., Cajigal M.L., Gamble A.S., Abboud K.H. Polyhedron. 15:1996;2071.
12. Galindo A., Montilla F., Pastor A., Carmona E., Gutierrez-Puebla E., Monge A., Ruiz C. Inorg. Chem. 36:1997;2379.
13. Lee S.-M., Kowallick R., Marcaccio M., McCleverty J.A., Ward M.D. J. Chem. Soc., Dalton Trans. 1998;3443.
14. Montilla F., Pastor A., Galindo A. J. Organomet. Chem. 590:1999;202.
15. Dilworth J.R., Gibson V.C., Davies N., Redshaw C., White A.P., Williams D.J. J. Chem. Soc., Dalton Trans. 1999;2695.
16. Clark J.H., Miller J.M., So K.H. J. Chem. Soc., Perkin Trans. 1:1978;941.
17. Teuben H.J., Glossauer O. Chem. Ber. 98:1965;2939.
18. Dyer P.W., Gibson V.C., Clegg W. J. Chem. Soc., Dalton Trans. 1995;3313.
19. Bell A., Clegg W., Dyer P.W., Elsegood M.R.J., Gibson V.C., Marshall E.L. J. Chem. Soc., Chem. Commun. 1994;2247.
20. SMART (diffractometer control) and SAINT (integration) software, Siemens Analytical X-Ray Instruments Inc., Madison, WI, USA, 1995.
21. Sheldrick G.M. SHELXTL version 5. 1995;Siemens Analytical X-Ray Instruments Inc. Madison, WI, USA.
22. Flack H.D. Acta Crystallogr. Sect. A. 39:1983;876.