메뉴 건너뛰기




Volumn 45, Issue 4, 1997, Pages 1212-1219

Structural Analysis of Wheat Straw Lignin by Quantitative 31P and 2D NMR Spectroscopy. The Occurrence of Ester Bonds and α-O-4 Substructures

Author keywords

2D NMR; Structural analysis; Wheat straw lignin

Indexed keywords

TRITICUM AESTIVUM;

EID: 0642362796     PISSN: 00218561     EISSN: None     Source Type: Journal    
DOI: 10.1021/jf960568k     Document Type: Article
Times cited : (237)

References (48)
  • 1
    • 4243064911 scopus 로고
    • Lignin chemistry - Past, present and future
    • Adler, E. Lignin chemistry - past, present and future. Wood Sci. Technol. 1977, 11, 169-218.
    • (1977) Wood Sci. Technol. , vol.11 , pp. 169-218
    • Adler, E.1
  • 2
    • 0028374621 scopus 로고
    • Quantitative phosphorus-31 NMR analysis of lignins, a new tool for the lignin chemist
    • Argyropoulos, D. S. Quantitative phosphorus-31 NMR analysis of lignins, a new tool for the lignin chemist. J. Wood Chem. Technol. 1994, 14, 45-63.
    • (1994) J. Wood Chem. Technol. , vol.14 , pp. 45-63
    • Argyropoulos, D.S.1
  • 3
    • 0000786477 scopus 로고
    • 31P-NMR in wood chemistry: A review of recent progress
    • 31P-NMR in wood chemistry: a review of recent progress. Res. Chem. Intermed. 1995, 21, 373-395.
    • (1995) Res. Chem. Intermed. , vol.21 , pp. 373-395
    • Argyropoulos, D.S.1
  • 4
    • 5144233105 scopus 로고
    • MLEV-17-based two dimensional homonuclear magnetization transfer spectroscopy
    • Bax, A.; Davis, D. G. MLEV-17-based two dimensional homonuclear magnetization transfer spectroscopy. J. Magn. Reson. 1985, 65, 355.
    • (1985) J. Magn. Reson. , vol.65 , pp. 355
    • Bax, A.1    Davis, D.G.2
  • 5
    • 0010285919 scopus 로고
    • Sensitivity enhanced two dimensional heteronuclear shift correlation NMR spectroscopy
    • Bax, A.; Subramanian, S. Sensitivity enhanced two dimensional heteronuclear shift correlation NMR spectroscopy. J. Magn. Reson. 1986, 67, 565.
    • (1986) J. Magn. Reson. , vol.67 , pp. 565
    • Bax, A.1    Subramanian, S.2
  • 6
    • 0642365026 scopus 로고
    • Qualitative und quantitative unterschiede der lignine einiger holz- und stroharten
    • Beckman, E.; Liesche, O.; Lehmann, F. Qualitative und quantitative unterschiede der lignine einiger holz-und stroharten. Biochem. Z. 1923, 139, 491-508.
    • (1923) Biochem. Z. , vol.139 , pp. 491-508
    • Beckman, E.1    Liesche, O.2    Lehmann, F.3
  • 7
    • 4344576938 scopus 로고
    • On the mechanism of formation of non-cyclic benzyl ethers during lignin biosynthesis. Part 1. The reactivity of β-O-4 quinone methides with phenols and alcohols
    • Brunow, G.; Sipila, J.; Makela, T. On the mechanism of formation of non-cyclic benzyl ethers during lignin biosynthesis. Part 1. The reactivity of β-O-4 quinone methides with phenols and alcohols. Holzforschung 1989, 43, 55-59.
    • (1989) Holzforschung , vol.43 , pp. 55-59
    • Brunow, G.1    Sipila, J.2    Makela, T.3
  • 8
    • 0006705202 scopus 로고
    • Acid precipitable polymeric lignin. Production and analysis
    • Wood, W. A., Kellogg, S. T., Eds.; Academic Press, Inc.: New York
    • Crawford, D. L.; Pometto, A. L., III. Acid precipitable polymeric lignin. Production and analysis. In Methods in Enzymology; Wood, W. A., Kellogg, S. T., Eds.; Academic Press, Inc.: New York, 1988; Vol. 161, pp 46-47 and 179-183.
    • (1988) Methods in Enzymology , vol.161 , pp. 46-47
    • Crawford, D.L.1    Pometto III, A.L.2
  • 9
    • 0001059562 scopus 로고
    • Application of two dimensional homo and heteronuclear correlation NMR spectroscopy to wood lignin structure determination
    • Ede, R. M.; Brunow, G. Application of two dimensional homo and heteronuclear correlation NMR spectroscopy to wood lignin structure determination. J. Org. Chem. 1992, 57, 1477-1480.
    • (1992) J. Org. Chem. , vol.57 , pp. 1477-1480
    • Ede, R.M.1    Brunow, G.2
  • 10
    • 0001740247 scopus 로고
    • Homo- and hetero-nuclear 2D NMR techniques: Unambiguous structural probes for non-cyclic benzyl aryl ethers in soluble lignin samples
    • Ede, R. M.; Kilpelainen, I. Homo- and hetero-nuclear 2D NMR techniques: unambiguous structural probes for non-cyclic benzyl aryl ethers in soluble lignin samples. Res. Chem. Intermed. 1995, 21, 313-328.
    • (1995) Res. Chem. Intermed. , vol.21 , pp. 313-328
    • Ede, R.M.1    Kilpelainen, I.2
  • 11
    • 0011323154 scopus 로고
    • 1H chemical shift correlation and J.-resolved NMR studies on isolated and synthetic lignins
    • 1H chemical shift correlation and J.-resolved NMR studies on isolated and synthetic lignins. Holzforschung 1990, 44, 95-101.
    • (1990) Holzforschung , vol.44 , pp. 95-101
    • Ede, R.M.1    Brunow, G.2    Simola, L.K.3    Lemmetynen, J.4
  • 12
    • 84986793528 scopus 로고
    • Monomeric and dimeric phenolic constituents of plant cell walls - Possible factors influencing wall biodegradability
    • Eraso, F.; Hartley, R. D. Monomeric and dimeric phenolic constituents of plant cell walls - possible factors influencing wall biodegradability. J. Sci. Food Agric. 1990, 51, 163-170.
    • (1990) J. Sci. Food Agric. , vol.51 , pp. 163-170
    • Eraso, F.1    Hartley, R.D.2
  • 13
    • 0004610903 scopus 로고
    • Charakterisierung der lignine von Angiospermen durch oxidativen Abbau. II. Monokotilen (Characterization of angiosperm lignins by degradation. II. Monocotyledons)
    • Erickson, M.; Miksche, G. E.; Somfai, I. Charakterisierung der lignine von Angiospermen durch oxidativen Abbau. II. Monokotilen (Characterization of angiosperm lignins by degradation. II. Monocotyledons). Holzforschung 1973, 27, 147-150.
    • (1973) Holzforschung , vol.27 , pp. 147-150
    • Erickson, M.1    Miksche, G.E.2    Somfai, I.3
  • 14
    • 0000506710 scopus 로고
    • Cross-linking of matrix polymers in the growing cell walls of angiosperms
    • Fry, S. C. Cross-linking of matrix polymers in the growing cell walls of angiosperms. Annu. Rev. Plant Physiol. 1986, 37, 165-189.
    • (1986) Annu. Rev. Plant Physiol. , vol.37 , pp. 165-189
    • Fry, S.C.1
  • 15
    • 33751156578 scopus 로고
    • 2-Chloro-4,4,5,5-tetramethyl-1,3,2-dioxaphospholane, a reagent for the accurate determination of the uncondensed and condensed phenolic moieties in lignins
    • Granata, A.; Argyropoulos, D. S. 2-Chloro-4,4,5,5-tetramethyl-1,3,2-dioxaphospholane, a reagent for the accurate determination of the uncondensed and condensed phenolic moieties in lignins. J. Agric. Food Chem. 1995, 43, 1538-1544.
    • (1995) J. Agric. Food Chem. , vol.43 , pp. 1538-1544
    • Granata, A.1    Argyropoulos, D.S.2
  • 16
    • 0642365024 scopus 로고
    • Comparison between utilization of cellulose for paper from wood and straw
    • Hill, R. D., Munck, L., Eds.; Elsevier Science Publishers: Amsterdam
    • Hartler, N.; Ryrberg, G. Comparison between utilization of cellulose for paper from wood and straw. In New Approaches to Research on Cereal Carbyhydrates; Hill, R. D., Munck, L., Eds.; Elsevier Science Publishers: Amsterdam, 1985; pp 323-327.
    • (1985) New Approaches to Research on Cereal Carbyhydrates , pp. 323-327
    • Hartler, N.1    Ryrberg, G.2
  • 17
    • 84985205335 scopus 로고
    • p-Coumaric and ferulic acid components of cell walls of ryegrass and their relationships with lignin and digestibility
    • Hartley, R. D. p-Coumaric and ferulic acid components of cell walls of ryegrass and their relationships with lignin and digestibility. J. Sci. Food Agric. 1972, 1347-1354.
    • (1972) J. Sci. Food Agric. , pp. 1347-1354
    • Hartley, R.D.1
  • 18
    • 0000292769 scopus 로고
    • Lignin-hydroxycinnamyl model compounds related to forage cell wall structure. 1. Ether-linked structures
    • Helm, R. F.; Ralph, J. Lignin-hydroxycinnamyl model compounds related to forage cell wall structure. 1. Ether-linked structures. J. Agric. Food Chem. 1992, 40, 2167-2175.
    • (1992) J. Agric. Food Chem. , vol.40 , pp. 2167-2175
    • Helm, R.F.1    Ralph, J.2
  • 19
    • 0011436581 scopus 로고
    • Lignin - Hydroxycinnamyl model compounds related to forage cell wall structure. 2. Ester-linked structures
    • Helm, R. F.; Ralph, J. Lignin - hydroxycinnamyl model compounds related to forage cell wall structure. 2. Ester-linked structures. J. Agric. Food Chem. 1993, 41, 570-576.
    • (1993) J. Agric. Food Chem. , vol.41 , pp. 570-576
    • Helm, R.F.1    Ralph, J.2
  • 20
    • 0041138736 scopus 로고
    • Occurrence of p-hydroxyl-phenylglycerol-β-aryl ether structure in lignins
    • Higuchi, R.; Kawamura, I. Occurrence of p-hydroxyl-phenylglycerol-β-aryl ether structure in lignins. Holzforschung 1966, 20, 16-21.
    • (1966) Holzforschung , vol.20 , pp. 16-21
    • Higuchi, R.1    Kawamura, I.2
  • 21
    • 0001627269 scopus 로고
    • Chemical properties of milled wood lignin of grasses
    • Higuchi, T.; Ito, Y.; Shimada, M.; Kawamura, I. Chemical properties of milled wood lignin of grasses. Phytochem. 1967, 6, 1551-1556.
    • (1967) Phytochem. , vol.6 , pp. 1551-1556
    • Higuchi, T.1    Ito, Y.2    Shimada, M.3    Kawamura, I.4
  • 22
    • 0028533723 scopus 로고
    • Ester linkages between lignin and glucuronic acid in lignin-carbohydrate complexes from Fagus crenata
    • Imamura, T.; Watanabe, T.; Kuwahara, M.; Koshijima, T. Ester linkages between lignin and glucuronic acid in lignin-carbohydrate complexes from Fagus crenata. Phytochemistry 1994, 37, 1165-1173.
    • (1994) Phytochemistry , vol.37 , pp. 1165-1173
    • Imamura, T.1    Watanabe, T.2    Kuwahara, M.3    Koshijima, T.4
  • 23
    • 0344749353 scopus 로고
    • The alkali treatment of straws
    • Jackson, M. G. The alkali treatment of straws. Anim. Feed Sci. Technol. 1977, 2, 105-130.
    • (1977) Anim. Feed Sci. Technol. , vol.2 , pp. 105-130
    • Jackson, M.G.1
  • 24
    • 0001449541 scopus 로고
    • New ether-linked ferulic acid-coniferyl alcohol dimers identified in grass straws
    • Jacquet, G.; Pollet, B.; Lapierre, C.; Mhamdi, F.; Rolando, C. New ether-linked ferulic acid-coniferyl alcohol dimers identified in grass straws. J. Agric. Food Chem. 1995, 43, 2746-2751.
    • (1995) J. Agric. Food Chem. , vol.43 , pp. 2746-2751
    • Jacquet, G.1    Pollet, B.2    Lapierre, C.3    Mhamdi, F.4    Rolando, C.5
  • 26
    • 0001863044 scopus 로고
    • Isolation and characterization of wheat straw lignin
    • Jung, H.-J. G.; Himmelsbach, D. S. Isolation and characterization of wheat straw lignin. J. Agric. Food Chem. 1989, 37, 81-87.
    • (1989) J. Agric. Food Chem. , vol.37 , pp. 81-87
    • Jung, H.-J.G.1    Himmelsbach, D.S.2
  • 27
    • 0002442590 scopus 로고
    • Structural feature of lignin in cell walls of normal and fast growing poplar (Populus maxinowiczii henry)
    • Kim, Y.; Iijama, K; Kurahashi, A.; Meshitsuka, G. Structural feature of lignin in cell walls of normal and fast growing poplar (Populus maxinowiczii henry). Mokuzai Gakkaishi 1995, 41, 837-843.
    • (1995) Mokuzai Gakkaishi , vol.41 , pp. 837-843
    • Kim, Y.1    Iijama, K.2    Kurahashi, A.3    Meshitsuka, G.4
  • 28
    • 0000197791 scopus 로고
    • Methoxyl deficient structural elements in lignin of sweetgum decayed by a brown-rot fungus
    • Kirk, T. K.; Adler, E. Methoxyl deficient structural elements in lignin of sweetgum decayed by a brown-rot fungus. Acta Chem. Scand. 1970, 24, 3379.
    • (1970) Acta Chem. Scand. , vol.24 , pp. 3379
    • Kirk, T.K.1    Adler, E.2
  • 30
    • 44049116557 scopus 로고
    • Cinnamic acid bridges between cell wall polymers in wheat and phalaris internodes
    • Lam, T. B. T.; Iiama, K.; Stone, K. A. Cinnamic acid bridges between cell wall polymers in wheat and phalaris internodes. Phytochemistry 1992, 31, 1179.
    • (1992) Phytochemistry , vol.31 , pp. 1179
    • Lam, T.B.T.1    Iiama, K.2    Stone, K.A.3
  • 33
    • 77957027051 scopus 로고
    • Preparation of dioxane lignin fraction by acidolysis
    • Wood, W. A., Kellogg, S. T., Eds.; Academic Press, Inc.: New York
    • Monties, B. Preparation of dioxane lignin fraction by acidolysis. In Methods in Enzymology; Wood, W. A., Kellogg, S. T., Eds.; Academic Press, Inc.: New York, 1988; Vol. 161, pp 31-35.
    • (1988) Methods in Enzymology , vol.161 , pp. 31-35
    • Monties, B.1
  • 34
    • 0000223114 scopus 로고
    • Ester linkage of p-coumaric acid in bamboo lignin
    • Nakamura, Y.; Higuchi, T. Ester linkage of p-coumaric acid in bamboo lignin. Holzforschung 1976, 30, 187-191.
    • (1976) Holzforschung , vol.30 , pp. 187-191
    • Nakamura, Y.1    Higuchi, T.2
  • 35
    • 84942493722 scopus 로고
    • Carbon-13 lignins, 8. structural differences between lignins of hardwoods, softwoods, grasses and compression wood
    • Nimz, H. H.; Robert, D.; Faix, O.; Nemr, M. Carbon-13 lignins, 8. structural differences between lignins of hardwoods, softwoods, grasses and compression wood. Holzforschung 1981, 35, 16-26.
    • (1981) Holzforschung , vol.35 , pp. 16-26
    • Nimz, H.H.1    Robert, D.2    Faix, O.3    Nemr, M.4
  • 36
    • 0342680613 scopus 로고
    • Isolation of lignin
    • Wood, W. A., Kellogg, S. T., Eds.; Academic Press, Inc.: New York
    • Obst, R.; Kirk, K. T. Isolation of lignin. In Methods in Enzymology; Wood, W. A., Kellogg, S. T., Eds.; Academic Press, Inc.: New York, 1988; Vol. 161, pp 6-8.
    • (1988) Methods in Enzymology , vol.161 , pp. 6-8
    • Obst, R.1    Kirk, K.T.2
  • 37
    • 37049067514 scopus 로고
    • Lignin-feruloyl esters cross-links in grasses. Part 1. Incorporation of feruloyl esters into dehydrogenation polymers
    • Ralph, J.; Helm, R. F.; Qideau, S.; Hatfield, R. P. Lignin-feruloyl esters cross-links in grasses. Part 1. Incorporation of feruloyl esters into dehydrogenation polymers. J. Chem. Soc., Perkin Trans. 1 1992, 2961-2969.
    • (1992) J. Chem. Soc., Perkin Trans. 1 , pp. 2961-2969
    • Ralph, J.1    Helm, R.F.2    Qideau, S.3    Hatfield, R.P.4
  • 40
    • 46549102057 scopus 로고
    • Ether linkage between phenolic acids and lignin fractions from wheat straw
    • Scalbert, A.; Monties, B.; Lallemand, J. Y.; Guittet, E.; Rolando, C. Ether linkage between phenolic acids and lignin fractions from wheat straw. Phytochemistry 1985, 24, 1359-1362.
    • (1985) Phytochemistry , vol.24 , pp. 1359-1362
    • Scalbert, A.1    Monties, B.2    Lallemand, J.Y.3    Guittet, E.4    Rolando, C.5
  • 41
    • 0000448496 scopus 로고
    • Formation of ether linkage between phenolic acids and-gramineae lignin: A possible mechanism involving quinone methides
    • Scalbert, A.; Monties, B.; Rolando, C.; Sierra-Escudero, A. Formation of ether linkage between phenolic acids and-gramineae lignin: a possible mechanism involving quinone methides. Holzforschung 1986a, 40, 191.
    • (1986) Holzforschung , vol.40 , pp. 191
    • Scalbert, A.1    Monties, B.2    Rolando, C.3    Sierra-Escudero, A.4
  • 42
    • 0001986976 scopus 로고
    • Comparison of wheat straw lignin preparations. I. Chemical and spectroscopic characterizations
    • Scalbert, A.; Monties, B.; Guittet, E.; Lallemand, J. Y. Comparison of wheat straw lignin preparations. I. Chemical and spectroscopic characterizations. Holzforschung 1986b, 40, 119-127.
    • (1986) Holzforschung , vol.40 , pp. 119-127
    • Scalbert, A.1    Monties, B.2    Guittet, E.3    Lallemand, J.Y.4
  • 43
    • 0014971099 scopus 로고
    • Ester linkages of p-coumaric acid in bamboo and grass lignins
    • Shimada, M.; Fukuzuka, T.; Higuchi, T. Ester linkages of p-coumaric acid in bamboo and grass lignins. Tappi 1971, 54, 72-78.
    • (1971) Tappi , vol.54 , pp. 72-78
    • Shimada, M.1    Fukuzuka, T.2    Higuchi, T.3
  • 44
    • 0040612145 scopus 로고
    • Ester groups in lignin
    • Smith, D. C. C. Ester groups in lignin. Nature 1955, 176, 267-269.
    • (1955) Nature , vol.176 , pp. 267-269
    • Smith, D.C.C.1
  • 46
    • 0000199142 scopus 로고
    • Ester linkages between lignin and glucuronoxylan in a lignin-carbohydrate complex from beech (Fagus crenata)
    • Takahashi, N.; Koshijima, T. Ester linkages between lignin and glucuronoxylan in a lignin-carbohydrate complex from beech (Fagus crenata). Wood Sci. Technol. 1988, 22, 231-241.
    • (1988) Wood Sci. Technol. , vol.22 , pp. 231-241
    • Takahashi, N.1    Koshijima, T.2
  • 47
    • 0004706049 scopus 로고
    • Chemical degradation methods for characterization of lignins
    • Wood, W. A., Kellogg, S. T., Eds.; Academic Press, Inc.: New York
    • Tanahashi, M.; Higuchi, T. Chemical degradation methods for characterization of lignins. In Methods in Enzymology; Wood, W. A., Kellogg, S. T., Eds.; Academic Press, Inc.: New York, 1988; Vol. 161, pp 107-109.
    • (1988) Methods in Enzymology , vol.161 , pp. 107-109
    • Tanahashi, M.1    Higuchi, T.2


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.