Reaction of the organometallic planar tetracoordinate carbon compound [(Cp2Zr)2(μ-C≡CCH3)(μ-(η 1-C:η2-C,C)-CH3CCCH3)] +[BPh4]- with alkyl isocyanides

Organometallics

Volumn 15, Issue 4, 1996, Pages 1265-1267

  Röttger, Dirk ^a   Pflug, Jörg ^a   Erker, Gerhard ^a   Kotila, Sirpa ^a   Fröhlich, Roland ^a  

^a UNIVERSITY OF MÜNSTER   (Germany)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0642349693     PISSN: 02767333     EISSN: None     Source Type: Journal    
DOI: 10.1021/om950651h     Document Type: Article

References (29)

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3. (a) Benner, L. S.; Olmstead, M. M.; Balch, A. L. J. Organomet. Chem. 1978, 159, 289. Adams, R. D.; Katahira, D. A.; Yang, L.-W. Organometallics 1982, 1, 231. Adams, H.; Bailey, N. A.; Bannister, C.; Faers, M. A.; Fedorko, P.; Osborn, V. A.; Winter, M. J. J. Chem. Soc., Dalton Trans. 1987, 341. Riera, V.; Ruiz, M. A.; Villafañe, F.; Bois, C.; Jeannin, Y. J. Organomet. Chem. 1990, 382, 407.
4. (a) Benner, L. S.; Olmstead, M. M.; Balch, A. L. J. Organomet. Chem. 1978, 159, 289. Adams, R. D.; Katahira, D. A.; Yang, L.-W. Organometallics 1982, 1, 231. Adams, H.; Bailey, N. A.; Bannister, C.; Faers, M. A.; Fedorko, P.; Osborn, V. A.; Winter, M. J. J. Chem. Soc., Dalton Trans. 1987, 341. Riera, V.; Ruiz, M. A.; Villafañe, F.; Bois, C.; Jeannin, Y. J. Organomet. Chem. 1990, 382, 407.
5. (a) Benner, L. S.; Olmstead, M. M.; Balch, A. L. J. Organomet. Chem. 1978, 159, 289. Adams, R. D.; Katahira, D. A.; Yang, L.-W. Organometallics 1982, 1, 231. Adams, H.; Bailey, N. A.; Bannister, C.; Faers, M. A.; Fedorko, P.; Osborn, V. A.; Winter, M. J. J. Chem. Soc., Dalton Trans. 1987, 341. Riera, V.; Ruiz, M. A.; Villafañe, F.; Bois, C.; Jeannin, Y. J. Organomet. Chem. 1990, 382, 407.
6. (b) For a different synthetic approach, see: Brunner, H.; Buchner, H.; Wachter, J.; Bernal, I.; Ries, W. H. J. Organomet. Chem. 1983, 244, 247.
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9. Herrmann, W. A.; Cuenca, T.; Menjon, B.; Herdtweck, E. Angew. Chem. 1987, 99, 687; Angew. Chem., Int. Ed. Engl. 1987, 26, 697. Herrmann, W. A.; Menjon, B.; Herdtweck, E. Organometallics 1991, 10, 2134. Cuenca, T.; Gómez, R.; Gómez-Sal, P.; Rodriguez, G. M.; Royo, P. Organometallics 1992, 11, 1229.
10. Herrmann, W. A.; Cuenca, T.; Menjon, B.; Herdtweck, E. Angew. Chem. 1987, 99, 687; Angew. Chem., Int. Ed. Engl. 1987, 26, 697. Herrmann, W. A.; Menjon, B.; Herdtweck, E. Organometallics 1991, 10, 2134. Cuenca, T.; Gómez, R.; Gómez-Sal, P.; Rodriguez, G. M.; Royo, P. Organometallics 1992, 11, 1229.
11. Herrmann, W. A.; Cuenca, T.; Menjon, B.; Herdtweck, E. Angew. Chem. 1987, 99, 687; Angew. Chem., Int. Ed. Engl. 1987, 26, 697. Herrmann, W. A.; Menjon, B.; Herdtweck, E. Organometallics 1991, 10, 2134. Cuenca, T.; Gómez, R.; Gómez-Sal, P.; Rodriguez, G. M.; Royo, P. Organometallics 1992, 11, 1229.
12. Herrmann, W. A.; Cuenca, T.; Menjon, B.; Herdtweck, E. Angew. Chem. 1987, 99, 687; Angew. Chem., Int. Ed. Engl. 1987, 26, 697. Herrmann, W. A.; Menjon, B.; Herdtweck, E. Organometallics 1991, 10, 2134. Cuenca, T.; Gómez, R.; Gómez-Sal, P.; Rodriguez, G. M.; Royo, P. Organometallics 1992, 11, 1229.
13. (a) Erker, G.; Röttger, D. Angew. Chem. 1993, 105, 1691; Angew. Chem., Int. Ed. Engl. 1993, 32, 1623. Röttger, D.; Erker, G.; Fröhlich, R.; Grehl, M.; Silverio, S. J.; Hyla-Kryspin, I.; Gleiter, R. J. Am. Chem. Soc. 1995, 117, 10503.
14. (a) Erker, G.; Röttger, D. Angew. Chem. 1993, 105, 1691; Angew. Chem., Int. Ed. Engl. 1993, 32, 1623. Röttger, D.; Erker, G.; Fröhlich, R.; Grehl, M.; Silverio, S. J.; Hyla-Kryspin, I.; Gleiter, R. J. Am. Chem. Soc. 1995, 117, 10503.
15. (a) Erker, G.; Röttger, D. Angew. Chem. 1993, 105, 1691; Angew. Chem., Int. Ed. Engl. 1993, 32, 1623. Röttger, D.; Erker, G.; Fröhlich, R.; Grehl, M.; Silverio, S. J.; Hyla-Kryspin, I.; Gleiter, R. J. Am. Chem. Soc. 1995, 117, 10503.
16. (b) For related organometallic complexes containing a planar tetracoordinate carbon center, see: Erker, G.; Zwettler, R.; Krüger, C.; Noe, R.; Werner, S. J. Am. Chem. Soc. 1990, 112, 9620. Gleiter, R.; Hyla-Kryspin, I.; Niu, S.; Erker, G. Angew. Chem. 1993, 105, 753; Angew. Chem., Int. Ed. Engl. 1993, 32, 754. Reviews: Erker, G. Comments Inorg. Chem. 1992, 13, 111. Erker, G. Nachr. Chem. Techn. Lab. 1992, 40, 1099. Albrecht, M.; Erker, G.; Krüger, C. Synlett 1993, 441.
17. (b) For related organometallic complexes containing a planar tetracoordinate carbon center, see: Erker, G.; Zwettler, R.; Krüger, C.; Noe, R.; Werner, S. J. Am. Chem. Soc. 1990, 112, 9620. Gleiter, R.; Hyla-Kryspin, I.; Niu, S.; Erker, G. Angew. Chem. 1993, 105, 753; Angew. Chem., Int. Ed. Engl. 1993, 32, 754. Reviews: Erker, G. Comments Inorg. Chem. 1992, 13, 111. Erker, G. Nachr. Chem. Techn. Lab. 1992, 40, 1099. Albrecht, M.; Erker, G.; Krüger, C. Synlett 1993, 441.
18. (b) For related organometallic complexes containing a planar tetracoordinate carbon center, see: Erker, G.; Zwettler, R.; Krüger, C.; Noe, R.; Werner, S. J. Am. Chem. Soc. 1990, 112, 9620. Gleiter, R.; Hyla-Kryspin, I.; Niu, S.; Erker, G. Angew. Chem. 1993, 105, 753; Angew. Chem., Int. Ed. Engl. 1993, 32, 754. Reviews: Erker, G. Comments Inorg. Chem. 1992, 13, 111. Erker, G. Nachr. Chem. Techn. Lab. 1992, 40, 1099. Albrecht, M.; Erker, G.; Krüger, C. Synlett 1993, 441.
19. (b) For related organometallic complexes containing a planar tetracoordinate carbon center, see: Erker, G.; Zwettler, R.; Krüger, C.; Noe, R.; Werner, S. J. Am. Chem. Soc. 1990, 112, 9620. Gleiter, R.; Hyla-Kryspin, I.; Niu, S.; Erker, G. Angew. Chem. 1993, 105, 753; Angew. Chem., Int. Ed. Engl. 1993, 32, 754. Reviews: Erker, G. Comments Inorg. Chem. 1992, 13, 111. Erker, G. Nachr. Chem. Techn. Lab. 1992, 40, 1099. Albrecht, M.; Erker, G.; Krüger, C. Synlett 1993, 441.
20. (b) For related organometallic complexes containing a planar tetracoordinate carbon center, see: Erker, G.; Zwettler, R.; Krüger, C.; Noe, R.; Werner, S. J. Am. Chem. Soc. 1990, 112, 9620. Gleiter, R.; Hyla-Kryspin, I.; Niu, S.; Erker, G. Angew. Chem. 1993, 105, 753; Angew. Chem., Int. Ed. Engl. 1993, 32, 754. Reviews: Erker, G. Comments Inorg. Chem. 1992, 13, 111. Erker, G. Nachr. Chem. Techn. Lab. 1992, 40, 1099. Albrecht, M.; Erker, G.; Krüger, C. Synlett 1993, 441.
21. (b) For related organometallic complexes containing a planar tetracoordinate carbon center, see: Erker, G.; Zwettler, R.; Krüger, C.; Noe, R.; Werner, S. J. Am. Chem. Soc. 1990, 112, 9620. Gleiter, R.; Hyla-Kryspin, I.; Niu, S.; Erker, G. Angew. Chem. 1993, 105, 753; Angew. Chem., Int. Ed. Engl. 1993, 32, 754. Reviews: Erker, G. Comments Inorg. Chem. 1992, 13, 111. Erker, G. Nachr. Chem. Techn. Lab. 1992, 40, 1099. Albrecht, M.; Erker, G.; Krüger, C. Synlett 1993, 441.
22. Erker, G.; Röttger, D.; Fröhlich, R. Chem. Ber. 1995, 128, 1045.
23. In this case, C-C coupling between the isonitrile and the coordinated π-ligand was not observed. For an example of such a reaction, see: Hessen, B.; Blenkers, J.; Teuben, J. H.; Helgesson, G.; Jagner, S. Organometallics 1989, 8, 830.
24. Erker, G.; Frömberg, W.; Mynott, R.; Gabor, B.; Krüger, C. Angew. Chem. 1986, 98, 456; Angew. Chem., Int. Ed. Engl. 1986, 25, 463. Erker, G.; Frömberg, W.; Benn, R.; Mynott, R.; Angermund, K.; Krüger, C. Organometallics 1989, 8, 911. Erker, G.; Albrecht, M.; Krüger, C.; Nolte, M.; Werner, S. Organometallics 1993, 12, 4979.
25. Erker, G.; Frömberg, W.; Mynott, R.; Gabor, B.; Krüger, C. Angew. Chem. 1986, 98, 456; Angew. Chem., Int. Ed. Engl. 1986, 25, 463. Erker, G.; Frömberg, W.; Benn, R.; Mynott, R.; Angermund, K.; Krüger, C. Organometallics 1989, 8, 911. Erker, G.; Albrecht, M.; Krüger, C.; Nolte, M.; Werner, S. Organometallics 1993, 12, 4979.
26. Erker, G.; Frömberg, W.; Mynott, R.; Gabor, B.; Krüger, C. Angew. Chem. 1986, 98, 456; Angew. Chem., Int. Ed. Engl. 1986, 25, 463. Erker, G.; Frömberg, W.; Benn, R.; Mynott, R.; Angermund, K.; Krüger, C. Organometallics 1989, 8, 911. Erker, G.; Albrecht, M.; Krüger, C.; Nolte, M.; Werner, S. Organometallics 1993, 12, 4979.
27. Erker, G.; Frömberg, W.; Mynott, R.; Gabor, B.; Krüger, C. Angew. Chem. 1986, 98, 456; Angew. Chem., Int. Ed. Engl. 1986, 25, 463. Erker, G.; Frömberg, W.; Benn, R.; Mynott, R.; Angermund, K.; Krüger, C. Organometallics 1989, 8, 911. Erker, G.; Albrecht, M.; Krüger, C.; Nolte, M.; Werner, S. Organometallics 1993, 12, 4979.
28. Sheldrick, G. M. Acta Crystallogr. 1990, A46, 467. Sheldrick, G. M. SHELXL-93, Program for the Refinement of Structures; University of Göttingen: Göttingen, Germany, 1993.
29. Sheldrick, G. M. Acta Crystallogr. 1990, A46, 467. Sheldrick, G. M. SHELXL-93, Program for the Refinement of Structures; University of Göttingen: Göttingen, Germany, 1993.