Crystal structure of 4-acetyl-l-(4'-fluorophenyl)-5-methyl-2,3-dihydro-1H-pyrrole-2,3-dione verifies the scheme of synthesis

Zeitschrift fur Kristallographie - New Crystal Structures

Volumn 211, Issue 9, 1996, Pages 622-625

  Grochowski, J ^a   Serda, P ^a   Dauter, Z ^b   Kolasa, A ^a  

^a JAGIELLONIAN UNIVERSITY   (Poland)

^b EUROPEAN MOLECULAR BIOLOGY LABORATORY   (Germany)

Author keywords

Crystal structure; Imaging plate

Indexed keywords

EID: 0542431007     PISSN: 14337266     EISSN: None     Source Type: Journal    
DOI: 10.1524/zkri.1996.211.9.622     Document Type: Article

References (15)

1. Zankowska-Jasihska, W.; Burgief M.; Golus, J.; Kolasa, A.; Walocha, K.; Zaleska, B.; Chojnacka-Wójcik, E.; Wiczynska, B.; Tatarczynska, E.: Synthesis and pharmacological activity of some 2,3-dihydrofuran-2,3-dione derivatives. Pol. J. Pharmacol. Pharm. 34 (1982) 391-398.
2. Ziegler, E.; Eder, M.; Belegratis, K.; Prewedourakis, E.: Syntheses of heterocycles. Oil. Reactions with oxalyl chloride. Monatsh. Chem. 98 (6) (1967) 2249-2251.
3. White, J. D.; Badger, R. A.; Kezar III, H. S.; Pallenberg, A. J.; Schiehser, G. A.: Structure, synthesis and absolute configuration of Leptosphaerin, a metabolite of the marine Ascomycete Leptosphaeria oraemaris. Tetrahedron 45 (21) (1989) 6631-6644.
4. Schagen, J. D.; Staver, L.; van Meurs, F.; Williams, G.: CAD-4 version 5.0. Enraf-Nonius, Delft, The Netherlands 1989.
5. Duisenberg, A. J. M.: Diffractometry and reflection profiles of anisotropic mosaic and split crystals. Acta Crystallogr. A39 (1983) 211-216.
6. Andrews, S. J.; Hails, J. E.; Harding. M. H.; Cruickshank, D. W. J.: The mosaic spread of very small crystals deduced from Laue diffraction patterns. Acta Crystallogr. A43 (1987) 70-73.
7. Grochowski, J.; Serda, P.; Dauter, Z.: The use of imaging plate for collecting diffraction data. Universitatis Iagellonicae Folia Phys., Fase. XXXVI (1994) 64-69.
8. Iwasaki, F.; Sakuratani, M.; Kaneko, H.; Yasui, M.; Kamiya, M.; Iwasaki, H.: Structure determination of organic compounds using an in-laboratory rapid X-ray measurement system-comparison with structures determined by a four-circle diffractometer. Acta Crystallogr. B51 (1995) 1028-1035.
9. Arndt, U. W.; Wonacott, A. J. (Ed.): The rotation method in crystallography. North Holland, Amsterdam 1977.
10. Otwinowski, Z.: DENZO-A film processing program for macromolecular crystallography. Yale University, New Haven, USA 1992.
11. Sheldrick, G. M.: SHELXS86-program for crystal structure solution. University of Göttingen, Germany 1986.
12. Sheldrick, G. M.: SHELXL-93-program for crystal structure refinement. University of Göttingen, Germany 1993.
13. Johnson, C. K.: ORTEP-a Fortran thermal-ellipsoid plot program for crystal structure illustrations. Oak Ridge, USA, 1976.
14. Kappe, C. O.; Kollenz, G.; Leung-Toung, R.; Wentrup, G.: Imidoylketene-azetin-2-one-oxoketenimine rearrangement. J. Chem. Soc, Chem. Commun. 1992 (6) 488-490.
15. Gein, V. L.; Shumilovskikh, E. V.; Andreichikov, Yu. S.; Saraeva, R. F.; Korobchenko, L. V.; Vladyko, V. G.; Boreko, E. L.: Synthesis of 4-substituted l-methyl-5-aryl-and 1,5-diaryltetrahydropyrrole-2,3-diones and their antiviral action. Khim-Farm. Zh. 25 (12) (1991) 37-40.