메뉴 건너뛰기




Volumn 46, Issue 3, 1998, Pages 1022-1026

Simplex Optimization of the Direct Analysis of Free Sterols in Sunflower Oil by On-Line Coupled Reversed Phase Liquid Chromatography-Gas Chromatography

Author keywords

Direct free sterol analysis; Edible oil; On line coupled RPLC GC; Simplex method

Indexed keywords

HELIANTHUS;

EID: 0542417489     PISSN: 00218561     EISSN: None     Source Type: Journal    
DOI: 10.1021/jf970844a     Document Type: Article
Times cited : (25)

References (38)
  • 1
    • 0000383767 scopus 로고    scopus 로고
    • Detection of desterolized sunflower oil in olive oil through isomerized △7-sterols
    • Biedermann, M.; Grob, K.; Mariani, C.; Schmidt, J. P. Detection of desterolized sunflower oil in olive oil through isomerized △7-sterols. Z. Lebensm. Unters. Forsch. 1996, 202, 199-204.
    • (1996) Z. Lebensm. Unters. Forsch. , vol.202 , pp. 199-204
    • Biedermann, M.1    Grob, K.2    Mariani, C.3    Schmidt, J.P.4
  • 2
    • 0027534041 scopus 로고
    • Preconcentration of volatile components of foods: Optimization of the steam distillation-solvent extraction at normal pressure
    • Blanch, G. P.; Tabera, J.; Herraiz, M.; Reglero, G. Preconcentration of volatile components of foods: optimization of the steam distillation-solvent extraction at normal pressure. J. Chromatogr. 1993a, 628, 261-8.
    • (1993) J. Chromatogr. , vol.628 , pp. 261-268
    • Blanch, G.P.1    Tabera, J.2    Herraiz, M.3    Reglero, G.4
  • 3
    • 0027744385 scopus 로고
    • Preconcentration of samples by steam distillation-solvent extraction at low temperature
    • Blanch, G. P.; Herraiz, M.; Reglero, G.; Tabera, J. Preconcentration of samples by steam distillation-solvent extraction at low temperature. J. Chromatogr. A 1993b, 655, 141-49.
    • (1993) J. Chromatogr. A , vol.655 , pp. 141-149
    • Blanch, G.P.1    Herraiz, M.2    Reglero, G.3    Tabera, J.4
  • 5
    • 0026940088 scopus 로고
    • Rapid analysis of whey proteins from different animal species by reversed-phase high-performance liquid chromatography
    • de Frutos, M.; Cifuentes, A.; Amigo, L.; Ramos, M.; Diez-Masa, J. C. Rapid analysis of whey proteins from different animal species by reversed-phase high-performance liquid chromatography. Z. Lebensm. Unters. -Forsch. 1992, 195, 326-31.
    • (1992) Z. Lebensm. Unters. -Forsch. , vol.195 , pp. 326-331
    • De Frutos, M.1    Cifuentes, A.2    Amigo, L.3    Ramos, M.4    Diez-Masa, J.C.5
  • 6
    • 0000485722 scopus 로고
    • Simplex optimization of variables in analytical chemistry
    • Deming, S. N.; Morgan, S. L. Simplex optimization of variables in analytical chemistry. Anal. Chem. 1973, 45, 278A-83A.
    • (1973) Anal. Chem. , vol.45
    • Deming, S.N.1    Morgan, S.L.2
  • 7
    • 84986774165 scopus 로고
    • Reversed-phase liquid chromatography coupled on-line with capillary gas chromatography. II. Use of a solvent vapor exit to increase introduction volumes and introduction rates into the gas Chromatograph
    • Goosens, E. C.; de Jong, D.; de Jong, G. J.; Brinkman, U. A. Th. Reversed-phase liquid chromatography coupled on-line with capillary gas chromatography. II. Use of a solvent vapor exit to increase introduction volumes and introduction rates into the gas Chromatograph. J. Microcolumn Sep. 1994, 6, 207-15.
    • (1994) J. Microcolumn Sep. , vol.6 , pp. 207-215
    • Goosens, E.C.1    De Jong, D.2    De Jong, G.J.3    Brinkman, U.A.Th.4
  • 9
    • 0027085792 scopus 로고
    • Hypenated high-performance liquid chromatography-capillary gas chromatography
    • Grob, K. Hypenated high-performance liquid chromatography-capillary gas chromatography. J. Chromatogr. 1992, 626, 25-32.
    • (1992) J. Chromatogr. , vol.626 , pp. 25-32
    • Grob, K.1
  • 10
    • 0029052192 scopus 로고
    • Development of the transfer techniques for on-line high-performance liquid chromatography-capillary gas chromatography
    • Grob, K. Development of the transfer techniques for on-line high-performance liquid chromatography-capillary gas chromatography. J. Chromatogr. 1995, 703, 265-76.
    • (1995) J. Chromatogr. , vol.703 , pp. 265-276
    • Grob, K.1
  • 11
    • 84986492823 scopus 로고
    • Reproducibility of results from LC-GC of sterols and wax esters in olive oil
    • Grob, K.; Lanfranchi, M. Reproducibility of results from LC-GC of sterols and wax esters in olive oil. J. High Resolut. Chromatogr. 1989, 12, 624-26.
    • (1989) J. High Resolut. Chromatogr. , vol.12 , pp. 624-626
    • Grob, K.1    Lanfranchi, M.2
  • 12
    • 0000480272 scopus 로고
    • Determination of free and esterified sterols and of wax esters in oils and fats by coupled liquid chromatography-gas chromatography
    • Grob, K.; Lanfranchi, M.; Mariani, C. Determination of free and esterified sterols and of wax esters in oils and fats by coupled liquid chromatography-gas chromatography. J. Chromatogr. 1989, 471, 397-405.
    • (1989) J. Chromatogr. , vol.471 , pp. 397-405
    • Grob, K.1    Lanfranchi, M.2    Mariani, C.3
  • 13
    • 0025508177 scopus 로고
    • Evaluation of olive oil through the fatty alcohols, the sterols and their esters by coupled LC-GC
    • Grob, K.; Lanfranchi, M.; Mariani, C. Evaluation of olive oil through the fatty alcohols, the sterols and their esters by coupled LC-GC. J. Am. Oil Chem. Soc. 1990, 67, 626-34.
    • (1990) J. Am. Oil Chem. Soc. , vol.67 , pp. 626-634
    • Grob, K.1    Lanfranchi, M.2    Mariani, C.3
  • 14
    • 0345876141 scopus 로고    scopus 로고
    • On-line HPLC-HRGC coupling and simultaneous transfer of two different LC fractions. Determination of aliphatic alcohols and sterols in olive oil
    • Lanuzza, F.; Micali, G.; Calabrò. G. On-line HPLC-HRGC coupling and simultaneous transfer of two different LC fractions. Determination of aliphatic alcohols and sterols in olive oil. J. High Resolut. Chromatogr. 1996, 19, 444-8.
    • (1996) J. High Resolut. Chromatogr. , vol.19 , pp. 444-448
    • Lanuzza, F.1    Micali, G.2    Calabrò, G.3
  • 15
    • 0027468194 scopus 로고
    • Trace level analysis of micropollutants in aqueous samples using gas chromatography with on-line sample enrichment and large volume injection
    • Mol, H. G.; Staniewski, J.; Janssen, H. G.; Cramers, C. A.; Ghijsen, R. T.; Brinkman, U. A. Th. Trace level analysis of micropollutants in aqueous samples using gas chromatography with on-line sample enrichment and large volume injection. J. Chromatogr. 1993, 630, 201-12.
    • (1993) J. Chromatogr. , vol.630 , pp. 201-212
    • Mol, H.G.1    Staniewski, J.2    Janssen, H.G.3    Cramers, C.A.4    Ghijsen, R.T.5    Brinkman, U.A.Th.6
  • 16
    • 0002001441 scopus 로고
    • Large volume sample introduction using temperature programmable injectors: Implications of liner diameter
    • Mol, H. G. J.; Janssen, H. G.; Cramers, C. A.; Brinkman, U. A. Th. Large volume sample introduction using temperature programmable injectors: Implications of liner diameter. J. High Resolut. Chromatogr. 1995a, 18, 19-27.
    • (1995) J. High Resolut. Chromatogr. , vol.18 , pp. 19-27
    • Mol, H.G.J.1    Janssen, H.G.2    Cramers, C.A.3    Brinkman, U.A.Th.4
  • 17
  • 18
    • 84986773244 scopus 로고
    • Automated LC-GC: A powerful method for essential oils analysis. Part IV. Coupled LC-GC-MS (ITD) for bergamot oil analysis
    • Mondello, L.; Bartle, K. D.; Dugo, P.; Gans, P..; Dugo, G. Automated LC-GC: A powerful method for essential oils analysis. Part IV. Coupled LC-GC-MS (ITD) for bergamot oil analysis. J. Microcolumn Sep. 1994, 6, 237-44.
    • (1994) J. Microcolumn Sep. , vol.6 , pp. 237-244
    • Mondello, L.1    Bartle, K.D.2    Dugo, P.3    Gans, P.4    Dugo, G.5
  • 19
    • 0001083047 scopus 로고    scopus 로고
    • On-line microbore high performance liquid chromatography-capillary gas chromatography for food and water analysis. A review
    • Mondello, L.; Dugo, G.; Bartle, K. D. On-line microbore high performance liquid chromatography-capillary gas chromatography for food and water analysis. A review. J. Microcolumn Sep. 1996a, 8, 275-310.
    • (1996) J. Microcolumn Sep. , vol.8 , pp. 275-310
    • Mondello, L.1    Dugo, G.2    Bartle, K.D.3
  • 20
    • 0001106162 scopus 로고    scopus 로고
    • On-line HPLC-HRGC-MS for the analysis of natural complex mixtures
    • Mondello, L.; Dugo, P.; Dugo, G.; Bartle, K. D. On-line HPLC-HRGC-MS for the analysis of natural complex mixtures. J. Chromatogr. Sci. 1996b, 34, 174-81.
    • (1996) J. Chromatogr. Sci. , vol.34 , pp. 174-181
    • Mondello, L.1    Dugo, P.2    Dugo, G.3    Bartle, K.D.4
  • 21
    • 0000238336 scopus 로고
    • A simplex method for function minimization
    • Nedler, J. A.; Mead, R. A simplex method for function minimization. Comput. J. 1965, 7, 308-13.
    • (1965) Comput. J. , vol.7 , pp. 308-313
    • Nedler, J.A.1    Mead, R.2
  • 22
    • 85034473890 scopus 로고
    • Jan 29, EEC Regulation 183/ 93 of Jan 29, 1993
    • Official Journal of the European Communities, Off. J. Eur. Communities 1988 (Jan 29), L22, 58 (EEC Regulation 183/ 93 of Jan 29, 1993).
    • (1988) Off. J. Eur. Communities , vol.L22 , pp. 58
  • 23
    • 0030144453 scopus 로고    scopus 로고
    • Kinetic evaluation of 3,β-hidroxychoIest-5-en-7-one (7-Ketocholesterol) stability during saponification
    • Park, P. W.; Guardiola, F.; Park, S. H.; Addis, P. B. Kinetic evaluation of 3,β-hidroxychoIest-5-en-7-one (7-Ketocholesterol) stability during saponification. J. Am. Oil Chem. Soc. 1996, 73, 623-29.
    • (1996) J. Am. Oil Chem. Soc. , vol.73 , pp. 623-629
    • Park, P.W.1    Guardiola, F.2    Park, S.H.3    Addis, P.B.4
  • 25
    • 0003157443 scopus 로고
    • Automatic injection in high-resolution gas chromatography. A programmed temperature vaporizer as a general purpose injection system
    • Poy, F.; Visani, S.; Terrosi, F. Automatic injection in high-resolution gas chromatography. A programmed temperature vaporizer as a general purpose injection system. J. Chromatogr. 1981, 217, 81-90.
    • (1981) J. Chromatogr. , vol.217 , pp. 81-90
    • Poy, F.1    Visani, S.2    Terrosi, F.3
  • 27
    • 0027361324 scopus 로고
    • Variables affecting the introduction of large sample volumes in capillary gas chromatography using a programmed-temperature vaporizer
    • Señoráns, F. J.; Tabera, J.; Villén, J.; Herraiz, M.; Reglero, G. Variables affecting the introduction of large sample volumes in capillary gas chromatography using a programmed-temperature vaporizer. J. Chromatogr. 1993, 648, 407-14.
    • (1993) J. Chromatogr. , vol.648 , pp. 407-414
    • Señoráns, F.J.1    Tabera, J.2    Villén, J.3    Herraiz, M.4    Reglero, G.5
  • 28
    • 0010650427 scopus 로고
    • Use of a programmed temperature injector for on-line reversed phase liquid chromatography-capillary gas chromatography
    • Señoráns, F. J.; Reglero, G.; Herraiz, M. Use of a programmed temperature injector for on-line reversed phase liquid chromatography-capillary gas chromatography. J. Chromatogr. Sci. 1995a, 33, 446-50.
    • (1995) J. Chromatogr. Sci. , vol.33 , pp. 446-450
    • Señoráns, F.J.1    Reglero, G.2    Herraiz, M.3
  • 29
    • 84988099685 scopus 로고
    • On-line reversed phase liquid chromatography-capillary gas chromatography using a programmed temperature vaporizer as interface
    • Señoráns, F. J.; Herraiz, M.; Tabera, J. On-line reversed phase liquid chromatography-capillary gas chromatography using a programmed temperature vaporizer as interface. J. High Resolut. Chromatogr. 1995b, 18, 433-38.
    • (1995) J. High Resolut. Chromatogr. , vol.18 , pp. 433-438
    • Señoráns, F.J.1    Herraiz, M.2    Tabera, J.3
  • 30
    • 0040022062 scopus 로고    scopus 로고
    • Rapid separation of free sterols in edible oils by on-line coupled reversed phase liquid chromatography-gas chromatography
    • Señoráns, F. J.; Tabera, J.; Herraiz, M. Rapid separation of free sterols in edible oils by on-line coupled reversed phase liquid chromatography-gas chromatography. J. Agric. Food Chem. 1996, 44, 3189-92.
    • (1996) J. Agric. Food Chem. , vol.44 , pp. 3189-3192
    • Señoráns, F.J.1    Tabera, J.2    Herraiz, M.3
  • 31
    • 84946640734 scopus 로고
    • Sequential application of simplex design in optimization and evolutionary operation
    • Spendley, W.; Hext, G. R.; Himsworth, F. R. Sequential application of simplex design in optimization and evolutionary operation. Technometrics 1962, 4, 441.
    • (1962) Technometrics , vol.4 , pp. 441
    • Spendley, W.1    Hext, G.R.2    Himsworth, F.R.3
  • 32
    • 84988057751 scopus 로고
    • Potential and limitations of differently designed programmed temperature injector liners for large volume sample introduction in capillary GC
    • Staniewski, J.; Rijks, J. A. Potential and limitations of differently designed programmed temperature injector liners for large volume sample introduction in capillary GC. J. High Resolut. Chromatogr. 1993, 16, 182-7.
    • (1993) J. High Resolut. Chromatogr. , vol.16 , pp. 182-187
    • Staniewski, J.1    Rijks, J.A.2
  • 33
    • 84986765094 scopus 로고
    • Programmed-temperature injector for large-volume sample introduction in capillary gas chromatography and for liquid chromatography-gas chromatography interfacing
    • Staniewski, J.; Janssen, H. G.; Cramers, C. A..; Rijks, J. A. Programmed-temperature injector for large-volume sample introduction in capillary gas chromatography and for liquid chromatography-gas chromatography interfacing. J. Microcolumn Sep. 1992, 4, 331-8.
    • (1992) J. Microcolumn Sep. , vol.4 , pp. 331-338
    • Staniewski, J.1    Janssen, H.G.2    Cramers, C.A.3    Rijks, J.A.4
  • 35
    • 0026897512 scopus 로고
    • Experimental design optimization of large volume sampling in a programmed temperature vaporizer
    • Villén, J.; Señoráns, F. J.; Herraiz, M.; Reglero, G.; Tabera, J. Experimental design optimization of large volume sampling in a programmed temperature vaporizer. J. Chromatogr. Sci. 1992, 30, 261-6.
    • (1992) J. Chromatogr. Sci. , vol.30 , pp. 261-266
    • Villén, J.1    Señoráns, F.J.2    Herraiz, M.3    Reglero, G.4    Tabera, J.5
  • 36
    • 0000152897 scopus 로고
    • Capillary gas Chromatographic injection system for large sample volumes
    • Vogt, W.; Jacob, K; Ohnesorge, A.; Obwexer, H. W. Capillary gas Chromatographic injection system for large sample volumes. J. Chromatogr. 1979, 186, 197-205.
    • (1979) J. Chromatogr. , vol.186 , pp. 197-205
    • Vogt, W.1    Jacob, K.2    Ohnesorge, A.3    Obwexer, H.W.4
  • 37
    • 84985225002 scopus 로고
    • On-line solid-phase extraction-thermal desorption for introduction of large volumes of aqueous samples into a gas Chromatograph
    • Vreuls, J. J.; Brinkman, U. A. Th.; de Jong, G. J.; Grob, K.; Artho, A. On-line solid-phase extraction-thermal desorption for introduction of large volumes of aqueous samples into a gas Chromatograph. J. High Resolut. Chromatogr. 1991, 14, 455-9.
    • (1991) J. High Resolut. Chromatogr. , vol.14 , pp. 455-459
    • Vreuls, J.J.1    Brinkman, U.A.Th.2    De Jong, G.J.3    Grob, K.4    Artho, A.5
  • 38
    • 0000970556 scopus 로고
    • Liquid chromatography coupled on-line with gas chromatography: State of the art
    • Vreuls, J. J.; de Jong, G. J.; Ghijsen, R. T.; Brinkman, U. A. Th. Liquid chromatography coupled on-line with gas chromatography: State of the art. J. AOAC Int. 1994, 77, 306-27.
    • (1994) J. AOAC Int. , vol.77 , pp. 306-327
    • Vreuls, J.J.1    De Jong, G.J.2    Ghijsen, R.T.3    Brinkman, U.A.Th.4


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.