Validation of a U.S. EPA method for the ion Chromatographic determination of perchlorate in fertilizers using a polyvinyl alcohol gel resin

American Laboratory

Volumn 34, Issue 15, 2002, Pages 14-16

  De Borba, Brian M ^a   Urbansky, Edward Todd ^b  

^a Metrohm Peak Inc   (United States)

^b U S ENVIRONMENTAL PROTECTION AGENCY   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

CHLORINE COMPOUNDS; CHROMATOGRAPHIC ANALYSIS; GELS; LEACHING; POLYVINYL ALCOHOLS; POTABLE WATER; PURIFICATION; REGULATORY COMPLIANCE; RESINS; SALTS; SOLUBILITY; STANDARDS;

GEL REINS; RESIDUAL METAL CATIONS; THYROID GLANDS; WRIST-ACTION SHAKER;

FERTILIZERS;

FERTILIZERS; ION CHROMATOGRAPHY; PERCHLORATES; POLYVINYL ALCOHOL;

EID: 0348085869     PISSN: 00447749     EISSN: None     Source Type: Trade Journal    
DOI: None     Document Type: Article

References (13)

1. Urbansky ET. Perchlorate chemistry: implications for analysis and remediation. Bioremed J 1998; 2:81-95.
2. Urbansky ET, Schock MR. Issues associated with managing the risks of perchlorate in drinking water. J Environ Manag 1999; 56:79-95.
3. Gullick RW, LeChevallier MW, Barhorst TW. Occurrence of perchlorate in drinking water sources. J Am Water Works Assoc 2001; 93(1):66-77.
4. Urbansky ET, Brown SK, Magnuson ML, Kelty CA. Perchlorate levels in samples of sodium nitrate fertilizers derived from Chilean caliche. Environ Pollut 2001; 112:299-302.
5. Susarla S, Collette TW, Garrison AW, Wolfe NL, McCutcheon SC. Perchlorate identification in fertilizers. Environ Sci Technol 1999; 33: 3469-72; see also erratum: Susarla S, Collette TW, Garrison AW, Wolfe NL, McCutcheon SC. Environ Sci Technol 2000; 34:224.
6. Susarla S, Collette TW, Garrison AW, Wolfe NL, McCutcheon SC. Perchlorate identification in fertilizers. Environ Sci Technol 1999; 33: 3469-72; see also erratum: Susarla S, Collette TW, Garrison AW, Wolfe NL, McCutcheon SC. Environ Sci Technol 2000; 34:224.
7. -): final report. Cincinnati, OH: U.S. Environmental Protection Agency, 2001, doc. no. EPA/600/R-01/049.
8. Urbansky ET, Collette TW. Comparison and evaluation of laboratory performance on a method for the determination of perchlorate in fertilizers. J Environ Monit 2001; 3(5):454-62.
9. Hautman DP, Munch DJ, Eaton AD, Haghani AW. Determination of perchlorate in drinking water using ion chromatography, Method 314.0, rev. 1.0. Cincinnati, OH: U.S. Environmental Protection Agency, 1999, doc. no. EPA/814/B-99/003.
10. Collette TW, Robarge WP, Urbansky ET. Ion Chromatographic determination of perchlorate: analysis of fertilizers and related materials. Cincinnati, OH: U.S. En-vironmental Protection Agency, 2001, doc. no. EPA/ 600/R-01/026.
11. Urbansky ET. Quantification of perchlorate ion: practices and advances applied to the analysis of common matrices. Crit Rev Anal Chem 2000; 30(5):311-43.
12. De Borba BM, Rowe DW. Determination of trace-level perchlorate according to U.S. EPA Method 314.0 using a polyvinyl alcohol gel resin. Am Lab 2001; 33(9):22-4.
13. De Borba BM, Urbansky ET. Performance of poly(vinyl alcohol) gel columns on the ion Chromatographic determination of perchlorate in fertilizers. J Environ Monit 2002; 4:149-55.