Preparation and optical resolution of a new helical lactone carrying the 2,8-dioxabicyclo[3.3.0]octane ring system

Heterocycles

Volumn 63, Issue 1, 2004, Pages 137-143

  Yamaye, Makoto ^a   Ikeda, Yusuke ^a   Cho, Namiko ^a   Miura, Yoshinori ^b   Yoshinaga, Tetsutaro ^c   Mukae, Katsuya ^d   Tsuru, Toshiaki ^d  

^a KYUSHU KYORITSU UNIVERSITY   (Japan)

^b KYUSHU UNIVERSITY   (Japan)

^c KYUSHU INSTITUTE OF TECHNOLOGY   (Japan)

^d KYUSHU SANGYO UNIVERSITY   (Japan)

Author keywords

[No Author keywords available]

Indexed keywords

2,7 DIHYDRONAPHTHALENE; 2,8 DIOXABICYCLO[3.3.0]OCTANE; 3,5 XYLENOL; GLYOXAL DERIVATIVE; LACTONE DERIVATIVE; NAPHTHALENE DERIVATIVE; OCTANE; UNCLASSIFIED DRUG; XYLENE;

ARTICLE; CHEMICAL STRUCTURE; ENANTIOMER; OPTICAL RESOLUTION; REACTION ANALYSIS; ROTATION; STRUCTURE ANALYSIS; SYNTHESIS;

EID: 0347654896     PISSN: 03855414     EISSN: None     Source Type: Journal    
DOI: 10.3987/COM-03-9919     Document Type: Article

References (7)

1. (a) T. Kito, K. Yoshinaga, M. Yamaye, and H. Mizobe, J. Org. Chem., 1991, 56, 3336.
2. (b) X. Fan, M. Yamaye, Y. Kosugi, H. Okazaki, H. Mizobe, T. Yanai, and T. Kito, J. Chem. Soc., Perkin Trans. 2, 1994, 2001.
3. (c) X. Fan, T. Yanai, H. Okazaki, M. Yamaye, H. Mizobe, Y. Kosugi, and T. Kito, J. Org. Chem., 1995, 60, 5407.
4. 4: C, 76.73; H, 4.68; Found: C, 76.46; H, 4.75. The rest of new compounds prepared were also characterized by spectroscopic methods, and gave the correct elemental analyses.
5. -3.
6. 20 +719° (c 0.1, 1,4-dioxane).
7. ext (Δε) 214 (8), 223 (1), 248 nm (36).