Evaluation and Optimisation of the Reagent Addition Sequence during the Synthesis of Atrazine (6-Chloro-N2-ethyl-N4-isopropyl-1,3, 5-triazine-2,4-diamine) Using Reaction Calorimetry

Organic Process Research and Development

Volumn 7, Issue 6, 2003, Pages 1071-1076

  Barton, Benita ^a   Gouws, Shawn ^a   Schaefer, Melissa C ^a   Zeelie, Bernard ^a  

^a NELSON MANDELA METROPOLITAN UNIVERSITY   (South Africa)

Author keywords

[No Author keywords available]

Indexed keywords

6 CHLORO N2 ETHYL N4 ISOPROPYL 1,3,5 TRIAZONE 2,4 DIAMINE; AMINE; ATRAZINE; CHLORIDE; CYANURIC ACID; ETHYLAMINE; HERBICIDE; PROPYLAMINE; REAGENT; SODIUM HYDROXIDE; UNCLASSIFIED DRUG;

ADDITION REACTION; ARTICLE; CALORIMETRY; CHEMICAL REACTION; HEAT; REACTION OPTIMIZATION; REACTOR; SAFETY; SYNTHESIS;

EID: 0347365738     PISSN: 10836160     EISSN: None     Source Type: Journal    
DOI: 10.1021/op0340715     Document Type: Article

References (10)

1. See: http://www.pan-uk.org/pestnews/Actives/atrazine.htm.
2. See: http://www.lenjohnson.com/atrazine.html.
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4. Singh, J. Process Saf. Prog. 1997, 16, 43.
5. Ullman's Encyclopedia of Industrial Chemistry, 6th ed.; Wiley-VCH: Weinheim, 2001; electronic release: http://www.wiley-vch.de/vch/software/ ullmann/.
6. Messori, V.; Francese, R.; Esposito, R. U.S. Patent 4,275,204, 1981.
7. Haschke, H.; Schreyer, G.; Schwarze, W.; Suchsland, H. U.S. Patent 4,058,662, 1977.
8. Baldi, L.; Ferrari, C.; Francese, R. U.S. Patent 4,099,006, 1978.
9. Singh, J. Process Saf. Prog. 1997, 16, 225.
10. See: http://physchem.ox.ac.uk/MSDS/AT/atrazine.html.