Crystal structure of "[Li(Et2O)]4[FePh4]": Corrigendum and reformulation. A remarkable example of a false solution in a wrong space group

Organometallics

Volumn 17, Issue 16, 1998, Pages 3630-3632

  Jefferis, Jesse M ^a   Girolami, Gregory S ^a  

^a UNIVERSITY OF ILLINOIS AT URBANA CHAMPAIGN   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0347266352     PISSN: 02767333     EISSN: None     Source Type: Journal    
DOI: 10.1021/om980186z     Document Type: Article

References (27)

1. Morse, P. M.; Wilson, S. R.; Girolami, G. S. J. Am. Chem. Soc. 1989, 111, 4114-4116.
2. Nelsen, M. J. Ph.D. Thesis, University of Illinois at Urbana-Champaign, 1996.
3. Bazhenova, T. A.; Lobkovskaya, R. M.; Shibaeva, R. P.; Shilov, A. E.; Shilova, A. K.; Gruselle, M.; Leny, G.; Tchoubar, B. J. Organomet. Chem. 1983, 244, 265-272.
4. Kerber, R. C. J. Organomet. Chem. 1984, 278, 205-254. Hubberstey, P. Coord. Chem. Rev. 1985, 66, 1-92. Bartlett, R. A.; Power, P. P.; Shoner, S. C. J. Am. Chem. Soc. 1988, 110, 1966-1968. Olmstead, M. M.; Power, P. P.; Shoner, S. C. Organometallics 1988, 7, 1380-1385. Taube, R.; Steinborn, D.; Drevs, H.; Chuong, P. N.; Stransky, N.; Langlotz, J. Z. Chem. 1988, 28, 381-396. Koschmieder, S. U.; Wilkinson, G. Polyhedron 1991, 10, 135-173. Shilov, A. E. New J. Chem. 1992, 16, 213-218. Müller, H.; Seidel, W.; Görls, H. J. Organomet. Chem. 1993, 445, 133-136. Poli, R. Chem. Rev. 1996, 96, 2135-2204. Kerber, R. C. In Comprehensive Organometallic Chemistry II; Abel, E. W., Stone, F. G. A., Wilkinson, G., Eds.; Pergamon: New York, 1995; Vol. 7, Chapter 2.
5. Kerber, R. C. J. Organomet. Chem. 1984, 278, 205-254. Hubberstey, P. Coord. Chem. Rev. 1985, 66, 1-92. Bartlett, R. A.; Power, P. P.; Shoner, S. C. J. Am. Chem. Soc. 1988, 110, 1966-1968. Olmstead, M. M.; Power, P. P.; Shoner, S. C. Organometallics 1988, 7, 1380-1385. Taube, R.; Steinborn, D.; Drevs, H.; Chuong, P. N.; Stransky, N.; Langlotz, J. Z. Chem. 1988, 28, 381-396. Koschmieder, S. U.; Wilkinson, G. Polyhedron 1991, 10, 135-173. Shilov, A. E. New J. Chem. 1992, 16, 213-218. Müller, H.; Seidel, W.; Görls, H. J. Organomet. Chem. 1993, 445, 133-136. Poli, R. Chem. Rev. 1996, 96, 2135-2204. Kerber, R. C. In Comprehensive Organometallic Chemistry II; Abel, E. W., Stone, F. G. A., Wilkinson, G., Eds.; Pergamon: New York, 1995; Vol. 7, Chapter 2.
6. Kerber, R. C. J. Organomet. Chem. 1984, 278, 205-254. Hubberstey, P. Coord. Chem. Rev. 1985, 66, 1-92. Bartlett, R. A.; Power, P. P.; Shoner, S. C. J. Am. Chem. Soc. 1988, 110, 1966-1968. Olmstead, M. M.; Power, P. P.; Shoner, S. C. Organometallics 1988, 7, 1380-1385. Taube, R.; Steinborn, D.; Drevs, H.; Chuong, P. N.; Stransky, N.; Langlotz, J. Z. Chem. 1988, 28, 381-396. Koschmieder, S. U.; Wilkinson, G. Polyhedron 1991, 10, 135-173. Shilov, A. E. New J. Chem. 1992, 16, 213-218. Müller, H.; Seidel, W.; Görls, H. J. Organomet. Chem. 1993, 445, 133-136. Poli, R. Chem. Rev. 1996, 96, 2135-2204. Kerber, R. C. In Comprehensive Organometallic Chemistry II; Abel, E. W., Stone, F. G. A., Wilkinson, G., Eds.; Pergamon: New York, 1995; Vol. 7, Chapter 2.
7. Kerber, R. C. J. Organomet. Chem. 1984, 278, 205-254. Hubberstey, P. Coord. Chem. Rev. 1985, 66, 1-92. Bartlett, R. A.; Power, P. P.; Shoner, S. C. J. Am. Chem. Soc. 1988, 110, 1966-1968. Olmstead, M. M.; Power, P. P.; Shoner, S. C. Organometallics 1988, 7, 1380-1385. Taube, R.; Steinborn, D.; Drevs, H.; Chuong, P. N.; Stransky, N.; Langlotz, J. Z. Chem. 1988, 28, 381-396. Koschmieder, S. U.; Wilkinson, G. Polyhedron 1991, 10, 135-173. Shilov, A. E. New J. Chem. 1992, 16, 213-218. Müller, H.; Seidel, W.; Görls, H. J. Organomet. Chem. 1993, 445, 133-136. Poli, R. Chem. Rev. 1996, 96, 2135-2204. Kerber, R. C. In Comprehensive Organometallic Chemistry II; Abel, E. W., Stone, F. G. A., Wilkinson, G., Eds.; Pergamon: New York, 1995; Vol. 7, Chapter 2.
8. Kerber, R. C. J. Organomet. Chem. 1984, 278, 205-254. Hubberstey, P. Coord. Chem. Rev. 1985, 66, 1-92. Bartlett, R. A.; Power, P. P.; Shoner, S. C. J. Am. Chem. Soc. 1988, 110, 1966-1968. Olmstead, M. M.; Power, P. P.; Shoner, S. C. Organometallics 1988, 7, 1380-1385. Taube, R.; Steinborn, D.; Drevs, H.; Chuong, P. N.; Stransky, N.; Langlotz, J. Z. Chem. 1988, 28, 381-396. Koschmieder, S. U.; Wilkinson, G. Polyhedron 1991, 10, 135-173. Shilov, A. E. New J. Chem. 1992, 16, 213-218. Müller, H.; Seidel, W.; Görls, H. J. Organomet. Chem. 1993, 445, 133-136. Poli, R. Chem. Rev. 1996, 96, 2135-2204. Kerber, R. C. In Comprehensive Organometallic Chemistry II; Abel, E. W., Stone, F. G. A., Wilkinson, G., Eds.; Pergamon: New York, 1995; Vol. 7, Chapter 2.
9. Kerber, R. C. J. Organomet. Chem. 1984, 278, 205-254. Hubberstey, P. Coord. Chem. Rev. 1985, 66, 1-92. Bartlett, R. A.; Power, P. P.; Shoner, S. C. J. Am. Chem. Soc. 1988, 110, 1966-1968. Olmstead, M. M.; Power, P. P.; Shoner, S. C. Organometallics 1988, 7, 1380-1385. Taube, R.; Steinborn, D.; Drevs, H.; Chuong, P. N.; Stransky, N.; Langlotz, J. Z. Chem. 1988, 28, 381-396. Koschmieder, S. U.; Wilkinson, G. Polyhedron 1991, 10, 135-173. Shilov, A. E. New J. Chem. 1992, 16, 213-218. Müller, H.; Seidel, W.; Görls, H. J. Organomet. Chem. 1993, 445, 133-136. Poli, R. Chem. Rev. 1996, 96, 2135-2204. Kerber, R. C. In Comprehensive Organometallic Chemistry II; Abel, E. W., Stone, F. G. A., Wilkinson, G., Eds.; Pergamon: New York, 1995; Vol. 7, Chapter 2.
10. Kerber, R. C. J. Organomet. Chem. 1984, 278, 205-254. Hubberstey, P. Coord. Chem. Rev. 1985, 66, 1-92. Bartlett, R. A.; Power, P. P.; Shoner, S. C. J. Am. Chem. Soc. 1988, 110, 1966-1968. Olmstead, M. M.; Power, P. P.; Shoner, S. C. Organometallics 1988, 7, 1380-1385. Taube, R.; Steinborn, D.; Drevs, H.; Chuong, P. N.; Stransky, N.; Langlotz, J. Z. Chem. 1988, 28, 381-396. Koschmieder, S. U.; Wilkinson, G. Polyhedron 1991, 10, 135-173. Shilov, A. E. New J. Chem. 1992, 16, 213-218. Müller, H.; Seidel, W.; Görls, H. J. Organomet. Chem. 1993, 445, 133-136. Poli, R. Chem. Rev. 1996, 96, 2135-2204. Kerber, R. C. In Comprehensive Organometallic Chemistry II; Abel, E. W., Stone, F. G. A., Wilkinson, G., Eds.; Pergamon: New York, 1995; Vol. 7, Chapter 2.
11. Kerber, R. C. J. Organomet. Chem. 1984, 278, 205-254. Hubberstey, P. Coord. Chem. Rev. 1985, 66, 1-92. Bartlett, R. A.; Power, P. P.; Shoner, S. C. J. Am. Chem. Soc. 1988, 110, 1966-1968. Olmstead, M. M.; Power, P. P.; Shoner, S. C. Organometallics 1988, 7, 1380-1385. Taube, R.; Steinborn, D.; Drevs, H.; Chuong, P. N.; Stransky, N.; Langlotz, J. Z. Chem. 1988, 28, 381-396. Koschmieder, S. U.; Wilkinson, G. Polyhedron 1991, 10, 135-173. Shilov, A. E. New J. Chem. 1992, 16, 213-218. Müller, H.; Seidel, W.; Görls, H. J. Organomet. Chem. 1993, 445, 133-136. Poli, R. Chem. Rev. 1996, 96, 2135-2204. Kerber, R. C. In Comprehensive Organometallic Chemistry II; Abel, E. W., Stone, F. G. A., Wilkinson, G., Eds.; Pergamon: New York, 1995; Vol. 7, Chapter 2.
12. Kerber, R. C. J. Organomet. Chem. 1984, 278, 205-254. Hubberstey, P. Coord. Chem. Rev. 1985, 66, 1-92. Bartlett, R. A.; Power, P. P.; Shoner, S. C. J. Am. Chem. Soc. 1988, 110, 1966-1968. Olmstead, M. M.; Power, P. P.; Shoner, S. C. Organometallics 1988, 7, 1380-1385. Taube, R.; Steinborn, D.; Drevs, H.; Chuong, P. N.; Stransky, N.; Langlotz, J. Z. Chem. 1988, 28, 381-396. Koschmieder, S. U.; Wilkinson, G. Polyhedron 1991, 10, 135-173. Shilov, A. E. New J. Chem. 1992, 16, 213-218. Müller, H.; Seidel, W.; Görls, H. J. Organomet. Chem. 1993, 445, 133-136. Poli, R. Chem. Rev. 1996, 96, 2135-2204. Kerber, R. C. In Comprehensive Organometallic Chemistry II; Abel, E. W., Stone, F. G. A., Wilkinson, G., Eds.; Pergamon: New York, 1995; Vol. 7, Chapter 2.
13. Kerber, R. C. J. Organomet. Chem. 1984, 278, 205-254. Hubberstey, P. Coord. Chem. Rev. 1985, 66, 1-92. Bartlett, R. A.; Power, P. P.; Shoner, S. C. J. Am. Chem. Soc. 1988, 110, 1966-1968. Olmstead, M. M.; Power, P. P.; Shoner, S. C. Organometallics 1988, 7, 1380-1385. Taube, R.; Steinborn, D.; Drevs, H.; Chuong, P. N.; Stransky, N.; Langlotz, J. Z. Chem. 1988, 28, 381-396. Koschmieder, S. U.; Wilkinson, G. Polyhedron 1991, 10, 135-173. Shilov, A. E. New J. Chem. 1992, 16, 213-218. Müller, H.; Seidel, W.; Görls, H. J. Organomet. Chem. 1993, 445, 133-136. Poli, R. Chem. Rev. 1996, 96, 2135-2204. Kerber, R. C. In Comprehensive Organometallic Chemistry II; Abel, E. W., Stone, F. G. A., Wilkinson, G., Eds.; Pergamon: New York, 1995; Vol. 7, Chapter 2.
14. 2) was approximately the same (∼500) as reported by Shilov et al.
15. -3).
16. Marsh, R. E. Acta Crystallogr. 1995, B51, 897-907.
17. Baur, W. H.; Tillmanns, E. Acta Crystallogr. 1986, B42, 95-111.
18. Stout, G. H.; Turley, S.; Sieker, L. C.; Jensen, L. H. Proc. Natl. Acad. Sci. U.S.A. 1988, 85, 1020-1022.
19. Burrell, A. K.; Cotton, F. A.; Daniels, L. M.; Petricek, V. Inorg. Chem. 1995, 34, 4253-4255.
20. Donohue, J.; Goodman, S. H. Acta Crystallogr. 1967, 22, 352-354. Cowie, M.; Haymore, B. L.; Ibers, J. A. J. Am. Chem. Soc. 1976, 98, 7608-7617. Cotton, F. A.; Rice, G. W. Inorg. Chem. 1978, 17, 688-692. Lock, C. J. L.; Speranzini, R. A.; Zvagulis, M. Acta Crystallogr. 1980, B36, 1789-1793 and references therein. Murphy, V. J.; Rabinovich, D.; Parkin, G. J. Am. Chem. Soc. 1995, 117, 9762-9763.
21. Donohue, J.; Goodman, S. H. Acta Crystallogr. 1967, 22, 352-354. Cowie, M.; Haymore, B. L.; Ibers, J. A. J. Am. Chem. Soc. 1976, 98, 7608-7617. Cotton, F. A.; Rice, G. W. Inorg. Chem. 1978, 17, 688-692. Lock, C. J. L.; Speranzini, R. A.; Zvagulis, M. Acta Crystallogr. 1980, B36, 1789-1793 and references therein. Murphy, V. J.; Rabinovich, D.; Parkin, G. J. Am. Chem. Soc. 1995, 117, 9762-9763.
22. Donohue, J.; Goodman, S. H. Acta Crystallogr. 1967, 22, 352-354. Cowie, M.; Haymore, B. L.; Ibers, J. A. J. Am. Chem. Soc. 1976, 98, 7608-7617. Cotton, F. A.; Rice, G. W. Inorg. Chem. 1978, 17, 688-692. Lock, C. J. L.; Speranzini, R. A.; Zvagulis, M. Acta Crystallogr. 1980, B36, 1789-1793 and references therein. Murphy, V. J.; Rabinovich, D.; Parkin, G. J. Am. Chem. Soc. 1995, 117, 9762-9763.
23. Donohue, J.; Goodman, S. H. Acta Crystallogr. 1967, 22, 352-354. Cowie, M.; Haymore, B. L.; Ibers, J. A. J. Am. Chem. Soc. 1976, 98, 7608-7617. Cotton, F. A.; Rice, G. W. Inorg. Chem. 1978, 17, 688-692. Lock, C. J. L.; Speranzini, R. A.; Zvagulis, M. Acta Crystallogr. 1980, B36, 1789-1793 and references therein. Murphy, V. J.; Rabinovich, D.; Parkin, G. J. Am. Chem. Soc. 1995, 117, 9762-9763.
24. Donohue, J.; Goodman, S. H. Acta Crystallogr. 1967, 22, 352-354. Cowie, M.; Haymore, B. L.; Ibers, J. A. J. Am. Chem. Soc. 1976, 98, 7608-7617. Cotton, F. A.; Rice, G. W. Inorg. Chem. 1978, 17, 688-692. Lock, C. J. L.; Speranzini, R. A.; Zvagulis, M. Acta Crystallogr. 1980, B36, 1789-1793 and references therein. Murphy, V. J.; Rabinovich, D.; Parkin, G. J. Am. Chem. Soc. 1995, 117, 9762-9763.
25. Bazhenova, T. A.; Kachapina, L. M.; Shilov, A. E.; Antipin, M. Yu.; Struchkov, Yu. T. J. Organomet. Chem. 1992, 428, 107-123.
26. 3 (1.0 g, 6.2 mmol) in diethyl ether (75 mL). The mixture was stirred for 1 h at -78°C and then for 3 h at room temperature. The dark red solution was filtered, cooled to -78°C, and treated with n-butyllithium (6.2 mL of a 2.5 M solution in hexane, 15.4 mmol). The mixture was warmed ; to room temperature and allowed to stand for 12 h. The resulting black crystals were collected and then dried in a vacuum. Yield: 0.80 g (19%). The identity of the product was confirmed from its IR spectrum and unit cell parameters, which agree with those reported for 2.
27. Bazhenova, T. A.; Ivleva, I. N.; Kachapina, L. M.; Shilova, A. K.; Shilov, A. E.; Tchoubar, B. J. Organomet. Chem. 1985, 296, 95-101.