Determination of Vitamin E Acid Succinate in Biodegradable Microspheres by Reversed-Phase High-Performance Liquid Chromatography

Journal of Chromatographic Science

Volumn 42, Issue 1, 2004, Pages 43-48

  Martinez Sancho C ^a   Herrero Vanrell, R ^a   Negro, S ^a  

^a UNIVERSIDAD COMPLUTENSE DE MADRID   (Spain)

Author keywords

[No Author keywords available]

Indexed keywords

ALPHA TOCOPHEROL ACID SUCCINATE; ALPHA TOCOPHEROL DERIVATIVE; MICROSPHERE; POLYGLACTIN; UNCLASSIFIED DRUG;

ACCURACY; ARTICLE; BIODEGRADABILITY; CONCENTRATION (PARAMETERS); DRUG DEGRADATION; DRUG DETERMINATION; DRUG FORMULATION; DRUG STABILITY; REVERSED PHASE HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; SEPARATION TECHNIQUE; TEMPERATURE DEPENDENCE; ULTRAVIOLET RADIATION;

EID: 0346967175     PISSN: 00219665     EISSN: None     Source Type: Journal    
DOI: 10.1093/chromsci/42.1.43     Document Type: Article

References (29)

1. J.M. Larrosa, A.S. Veloso, F.-L. Leong, and M.F. Refojo. Antiproliferative effect of intravitreal alpha-tocopherol and alpha-tocopheryl-acid-succinate in a rabbit model of PVR. Curr. Eye Res. 16: 1030-35 (1997).
2. T. Sakamoto, D.R. Hinton, H. Kimura, C. Spee, R. Gopalakrishna, and S.J. Ryan. Vitamin E succinate inhibits proliferation and migration of retinal pigment epithelial cells in vitro: therapeutic implication for proliferative vitreoretinopathy. Graefe's Arch. Clin. Exp. Ophthalmol. 234; 186-92 (1996).
3. S. Cohen, T. Yoshiaka, and M. Lucarelli. Controlled delivery system for proteins based on poly (lactic/glycolic acid) microspheres. Pharm. Res. 8: 713-20 (1991).
4. D.K. Gilding and A.M. Reed. Biodegradable polymers for use in surgery. Poly(glycolic)/poli (lactic acid) homo and copolymers. Polymer 20: 1459-64 (1979).
5. D.W. Nierenberg, D.C. Lester, and T.A. Colacchio. Determination of tocopherol and tocopherol acetate concentrations in human feces using high-performance liquid chromatography. J. Chromatogr. 413: 79-89 (1987).
6. A. Celardo and A. Bortolotti. Measurement of vitamin E in premature infants by reversed-phase high-performance liquid chromatography. J. Chromatogr. 490: 432-38 (1989).
7. J.P. Koskas, J. Cillard, and P. Cillard. Separation of α-tocopherol, α-tocopherol quinone and α-tocopherol-dimer by reversed-phase high performance liquid chromatography. J. Chromatogr. 287: 442-46(1984).
8. J. Vigo, M.J. Lucero, and M.J. Leon. Determination of α-tocopherol in semisolid gelled preparations by reversed phase HPLC. Boll. Chim. Farm. 11: 415-18 (1992).
9. A.P. de Leenheer, H.J. Nelis, and W.E. Lambert. Chromatography of fat-soluble vitamins in clinical chemistry. J. Chromatogr. 429: 3-58 (1988).
10. P.C.H. Hollman, J.H. Slangen, P.J, Wagstaffe, U. Faure, D.A.T. Southgate, and P.M. Finglas. Intercomparison of methods for the determination of vitamins in foods. Part 1. Fat-soluble vitamins. Analyst 118: 475-80 (1993).
11. S. Gueguen, B. Herbeth, G. Siest, and P. Leroy. An isocratic liquid chromatographic method with diode-array detection for the simultaneous determination of α-tocopherol, retinol, and five carotenoids in human serum. J. Chromatogr. Sci. 40: 69-76 (2002).
12. S. Torrado, E. Jiménez-CabaIIero, R. Cadórniga, and J. Torrado. A selective liquid chromatography assay for the determination of dlα-tocopherol acetate in plasma samples. J. Liq. Chromatogr. 18: 1251-64(1995).
13. D.T. Burns and C. Mackay. Comparison of reversed-phase and adsorption modes of high-performance liquid chromatography for the assay of fat soluble vitamins in multivitamin tablets. J. Chromatogr. 200: 300-304 (1980).
14. M. Eriksson, T. Eriksson, and B. Sörensen. Simultaneous determination of vitamin A, D and E in multivitamin tablets by HPLC. Acta Pharm. Suec. 15: 274-81 (1978).
15. K.E. Savolainen, K.M. Pynnönen, S.P. Lapinjoki, and M.T. Vidgren. Determination of fat-soluble vitamins in a pharmaceutical dosage form by solid-phase extraction and reversed-phase liquid chromatography. J. Pharm. Sci. 77: 802-803 (1989).
16. W.O. Landen. Application of gel permeation chromatography and nonaqueous reverse phase chromatography to high performance liquid chromatographic determination of retinyl palmitate and α-tocopheryl acetate in infant formulas. J. Assoc. Off. Anal. Chem. 65: 810-16 (1982).
17. S. Scalia, A. Renda, G. Ruberto, F. Bonina, and E. Menegatti. Assay of vitamin A palmitate and vitamin E acetate in cosmetic creams and lotions by supercritical fluid extraction and HPLC. J. Pharm. Biomed. Anal. 13: 273-77 (1995).
18. T. Ijitsu and M. Ueno. Two-dimensional high-performance liquid chromatographic system for the direct determination of tocopherol derivatives in plasma. J. Chromatogr. 427: 29-39 (1988).
19. B.L. Lee, S.C. Chua, H.Y. Ong, and C.N. Ong. High-performance liquid chromatographic method for routine determination of vitamins A and E and β-carotene in plasma. J. Chromatogr. 581: 41-47 (1992).
20. L.R. Beck, D.R. Cowsar, D.H. Lewis, R.J. Cosgrove, C.T. Riddle, S.L. Lowry, and T. Epperly. A new long-acting injectable microcapsule system for the administration of progesterone. Fertil. Steril. 31: 545-48(1979).
21. C. Alvarez, R. Herrero-Vanrell, S. Negro, I.T. Molina, M.T. Hernández, P. Pastoriza, and E. Barcia. Dexametasone microspheres for intravitreal administration. Abstract. III. Spanish Portuguese Conference on Controlled Drug Delivery, Lisben, Portugal, 1998, p. 83.
22. S. Benita, J.P. Benoit, F. Puisieux, and C. Thies. Characterization of drug-loaded poly(D,L-lactide) microspheres. J. Pharm. Sci. 73: 1721-24 (1984).
23. J. Caporal-Gautier and J.M. Nivet. Rapport d'une commission SFSTP I. Méthodologie. S.T.P. Pharma 2: 205-26 (1992).
24. J. Caporal-Gautier and J.M. Nivet. Guide de validation analytique. Rapport d'une commission SFSTP II. Exemples d'application. S.T.P. Pharma 2: 227-39 (1992).
25. R.C. Causon. Validation of chromatographic methods in biomedical analysis. Viewpoint and discussion. J. Chromatogr. B 689: 175-80 (1997).
26. ICH Expert Working Group. Validation of analytical procedures: methodology (Q2B) International Conference on Harmonization. http://fda.gov/cder/guidance (accessed May 1999).
27. F. Brellose, M. Bromet-Petit, and M. Audran. Validation of liquid chromatographic and gas chromatographic methods. Applications to pharmacokinetics. J. Chromatogr. B 686: 3-10 (1996).
28. L. Oppenheimer, T.P. Capizzi, R.M. Weppelman, and H. Mehta. Determining the lowest limit of reliable assay measurement. Anal. Chem. 55: 638-43 (1983).
29. K. Paffitt, Ed. Martindale, 32nd ed. Pharmaceutical Press, London, U.K., 1999, pp. 1369-70.