메뉴 건너뛰기
Tetrahedron Letters
Volumn 13, Issue 19, 1972, Pages 1853-1856
A synthetic precursor of (±)-trichodermin
Author keywords

[No Author keywords available]
Indexed keywords

EID: 0346866664     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0040-4039(01)84734-1     Document Type: Article
Times cited : (20)
References (17)
  • 8
    • 37049142186 scopus 로고
    • The total synthesis of (�)-trichodermin
    • During the course of these laboratory investigations an elegant total synthesis of (±)-trichodermin (1) via (±)-lactone 2 was reported;, Although the overall synthetic goal of our scheme is the same as that reported, our choice of starting material and synthetic route to both (±)-lactone and (±)-trichodermin are different.
    • (1971) Journal of the Chemical Society D: Chemical Communications , pp. 858
    • Colvin1    Raphael2    Roberts3
  • 9
    • 84918196881 scopus 로고    scopus 로고
    • All new compounds reported, herein, gave satisfactory elemental analyses. All structures, except (−)-trichodermin (1) that are represented as one enantiomer are, in fact, racemic.
  • 10
    • 37049170442 scopus 로고
    • 540. Reactions of ??-unsaturated cyclic aldehydes and ketones. Part IX. (?)-cis- and (+)-trans-Piperitol from (?)-piperitone
    • Reduction of piperitone with lithium aluminum hydride produces a 64%:36% ratio of trans- to cis-piperitol respectively as reported by, and, therefore, the preferential reduction of enone-acid 8 was not expected to occur stereoselectively.
    • (1952) Journal of the Chemical Society (Resumed) , pp. 2852
    • Macbeth1    Shannon2
  • 11
    • 84918196880 scopus 로고
    • For two excellent reviews on alkylation of unsymmetrical ketones of this type, see:
    • (1963) Rec. of Chem. Prog. , vol.24 , pp. 42
    • Conia1
  • 13
    • 84918196879 scopus 로고    scopus 로고
    • glc analyses were conducted using 1/8 in.x 6 ft., stainless steel columns, with (a) 3% SE-30 on Vapaport 30, 100/120 mesh; (b) 5% FFAP on Varaport 30, 80/100 mesh; (c) 5% OV-17 on Varaport 30, 80/100 mesh.
  • 17
    • 84918196878 scopus 로고    scopus 로고
    • We would like to thank Dr. S.C. Watson of Texas Alkyls, Inc., Deer Park, Texas 77536 for the gracious gift of diisobutylaluminum hydride in benzene.

* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.