Synthesis and X-ray crystal structure of PhC(CF3)(OH)CONEt2, and CH3C(CF3)(OH)CON[CH2CH(CH3) 2]2

Journal of Fluorine Chemistry

Volumn 98, Issue 2, 1999, Pages 127-132

  Singh, Rajendra P ^a   Vij, Ashwani ^a   Kirchmeier, Robert L ^a   Shreeve, Jean'ne M ^a  

^a UNIVERSITY OF IDAHO   (United States)

Author keywords

CH3C(CF3)(OH)CON CH2CH(CH3) 2 2; Crystal structure; Intermolecular hydrogen bonding; PhC(CF3)(OH)CONEt2

Indexed keywords

EID: 0346786733     PISSN: 00221139     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0022-1139(99)00093-7     Document Type: Article

References (22)

1. McClinton M.A., McClinton D.A. Tetrahedron. 82:1992;6555.
2. Lal G.C., Pez G.P., Syvret R.G. Chem. Rev. 96:1996;1737.
3. Prakash G.K.S., Yudin A.K. Chem. Rev. 97:1997;757.
4. Kobayashi Y., Kumadaki I. Acc. Chem. Res. 11:1978;197.
5. C. Hansch, A. Leo, (Eds.), Substituent Constants for Correlation Analysis in Chemistry and Biology, Wiley, New York, 1997.
6. R.K. Filler, Y. Kobayashi, Biomedical Aspects of Fluorine Chemistry, Kodansha, Tokyo, 1982.
7. R.E. Banks, B.E. Smart, J.C. Tatlow, Organofluorine Chemistry, Plenum Press, New York, 1994.
8. G.A. Olah, R.D. Chambers, G.K.S. Prakash, Synthetic Fluorine Chemistry, Wiley, New York, 1992.
9. R.A. Darral, F. Smith, M. Stacey, J.C. Tatlow, J. Chem. Soc. (1951) 2329.
10. E.C. Tongco, G.K.S. Prakash, G.A. Olah, Synlett. (1997) 1193.
11. Rasmusson G.H. Ann. Rep. Med. Chem. 21:1986;179.
12. Katchen B., Buxbaum S. J. Clin. Endocrinol. 41:1975;373.
13. Glen A.T., Hughes L.R., Morris J.J., Taylor P.J. SCI-RSSC Med. Chem. Symp. 3:1987;345.
14. Morris J.J., Hughes L.R., Glen A.T., Taylor P.J. J. Med. Chem. 34:1991;447.
15. Singh R.P., Kirchmeier R.L., Shreeve J.M. J. Org. Chem. 64:1999;2579.
16. Nelson D.W., O'Reilly N.J., Speier J., Gassman P.G. J. Org. Chem. 59:1994;8157.
17. Ottenheijm H.C.J., Tijhuis M.W. Org. Synth. 61:1983;1.
18. SMART V 4.043 Software for the CCD Detector System, Siemens Analytical Instruments Division, Madison, WI, 1995.
19. SAINT V 4.035 Software for the CCD Detector System, Siemens Analytical Instruments Division, Madison, WI, 1995.
20. SADABS, Siemens Area Detector Absorption Correction Program, Siemens Analytical Instruments Division, Madison, WI, 1995.
21. G.M. Sheldrick, SHELXS-97, Program for the Solution of Crystal Structure, University of Gottingen, Germany, 1997.
22. SHELXTL 5.10, Program Library for Structure Solution and Molecular Graphics, Bruker AXS, WI, 1997.