Reaction of Borane in Tetrahydrofuran with 1,1,3,3-Tetramethyldisilazane and Cyclic Disilazanes - Competition between N-Si and N-H Bond Cleavage

Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences

Volumn 51, Issue 12, 1996, Pages 1707-1715

  Wrackmeyer, Bernd ^a   Schwarze, Bernd ^a  

^a UNIVERSITY OF BAYREUTH   (Germany)

Author keywords

Aminoboranes; Borane THF Adduct; Borazines; Disilazanes

Indexed keywords

NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; ORGANIC SOLVENTS; SILICON;

AMINOBORANES; BORANE-THF ADDUCT; BORAZINES; DISILAZANES; H FUNCTION; HEXAMETHYLDISILAZANE; REACTION CONDITIONS; TETRA-HYDROFURAN;

SILICON COMPOUNDS;

EID: 0346616696     PISSN: 09320776     EISSN: None     Source Type: Journal    
DOI: 10.1515/znb-1996-1207     Document Type: Article

References (31)

1. a) R. Köster, I. Iwasaki, Adv. Chem. Ser. 42, 148 (1964);
2. b) B. M. Mikhailov, V. A. Dorokhov, N. V. Mostovoi, Izv. Akad. Nauk SSSR, 199 (1964);
3. c) A.B. Burg, J. Banus, J. Am. Chem. Soc. 76, 3903 (1954);
4. d) R. Köster, Angew. Chem. 75, 730 (1963);
5. e) H. Bellut, R. Köster, Justus Liebigs Ann. Chem. 738, 86 (1970);
6. f) R. Köster, H. Bellut, S. Hattori, Justus Liebigs Ann. Chem. 720, 1 (1968);
7. g) R. Köster, G. Seidel, Liebigs Ann. Chem. 1837 (1977).
8. B. Wrackmeyer, B. Schwarze, W. Milius, J. Organomet. Chem. 489, 201 (1995).
9. H. Nöth, Z. Naturforsch. 16b, 618 (1961).
10. W. R. Nutt, R. L. Wells, Inorg. Chem. 21, 2649 (1982).
11. B. Wrackmeyer, B. Schwarze, Z. Anorg. Allg. Chem. (1996) in press.
12. a) J. H. Smalley, S. F. Stafiej, J. Am. Chem. Soc. 81, 852 (1959);
13. b) A. Grace, P. Powell, J. Chem. Soc. A. 673 (1966);
14. c) A. Meller, M. Wechsberg, V. Gutmann, Monatsh. Chem. 97, 1163 (1966);
15. d) C. S. G. Phillips, P. Powell, J.A. Semlyen, P.L. Timms, Fres. J. Anal. Chem. 197, 202 (1963).
16. a) J. F. Harrod, A. J. Chalk, J. Am. Chem. Soc. 87, 1133 (1965);
17. b) N. Chatani, S. Fuji, Y. Ynasaki, S. Murai, N. Sonoda, J. Am. Chem. Soc. 108, 7361 (1966).
18. a) H. Nöth, B. Wrackmeyer, Nuclear Magnetic Resonance Spectroscopy of Boron Compounds, in P. Diehl, E. Fluck and R. Kosfeld (eds.) NMR Basic Principles and Progress, Vol. 14, Springer, Berlin (1978);
19. b) B. Wrackmeyer, R. Kösten, in R. Köster (ed.) Houben-Weyl, Methoden der Organischen Chemie, Vol. 13/3c, pp. 377-611, Thieme, Stuttgart (1984).
20. a) H. Nöth, W. Tinhof, B. Wrackmeyer, Chem. Ber. 107, 518 (1974);
21. 14N-NMR-Spektren von Bor-Stickstoff-Verbindungen mit dreifach koordiniertem Bor, in K. Niedenzu (ed.) Gmelin, 8. Aufl., Vol. 23/5, pp. 197-277, Springer, Berlin (1975).
22. a) G. A. Morris, J. Am. Chem. Soc. 102, 428 (1980);
23. b) D. P. Burum, R. R. Ernst, J. Magn. Reson 39, 163 (1980).
24. a) B. Wrackmeyer, S. Kerschl, C. Stader, K. Horchler, Spectrochim. Acta 42A, 1113 (1986);
25. b) B. Wrackmeyer, C. Stader, H. Zhou, Spectrochim. Acta 45A, 1101 (1989).
26. B. Wrackmeyer, B. Schwarze, D. M. Durran, G. A. Webb, Magn. Reson. Chem. 33, 557 (1995).
27. B. Wrackmeyer, Ē. Kupče, R. Köster, G. Seidel, Magn. Reson. Chem. 33, 812 (1995).
28. B. Wrackmeyer, Ē. Kupče, in M. Gielen (ed.) Topics of Physical Organometallic Chemistry, Vol. 4, pp. 289-352, Freund Publishing House, Tel Aviv (1992).
29. H. C. Brown, R. L. Sharp, J. Am. Chem. Soc. 90, 2915 (1968).
30. a) R. H. Baney, G. G. Haberland, J. Organomet. Chem. 5, 320 (1966);
31. b) D. Seyferth, J. Robison, Macromolecules 26, 407 (1993).