Selective Reduction of an Aromatic Nitro Group to an Azoxy Unit in the Presence of an Aliphatic Nitro Group

Monatshefte fur Chemie

Volumn 134, Issue 3, 2003, Pages 419-423

  Siemeling, Ulrich ^a   Türk, Thomas ^a   Vorfeld, Udo ^a   Fink, Heinrich ^a  

^a UNIVERSITY OF KASSEL   (Germany)

Author keywords

Azoxybenzene; Bismuth; Nitro compounds; Reductions; X ray structure determination

Indexed keywords

1 AMINO 2 (2 AMINO 2 METHYLPROPYL)BENZENE; 1 NITRO 2 (2 NITRO 2 METHYLPROPYL)BENZENE; 2,2' BIS(2 NITRO 2 METHOXYPROPYL)AZOXYBENZENE; 3,3 DIMETHYL 3,4 DIHYDROCINNOLINE; ALIPHATIC COMPOUND; AROMATIC NITRO COMPOUND; AZOXY DERIVATIVE; BENZENE DERIVATIVE; FUNCTIONAL GROUP; HYDROCHLORIC ACID; UNCLASSIFIED DRUG; ZINC;

ARTICLE; CHEMICAL BOND; CRYSTAL STRUCTURE; REDUCTION; REPRODUCIBILITY; STRUCTURE ANALYSIS; X RAY DIFFRACTION;

EID: 0346250079     PISSN: 00269247     EISSN: None     Source Type: Journal    
DOI: 10.1007/s00706-002-0549-9     Document Type: Article

References (11)

1. Kabalka GW, Varma RS (1991) Reduction of Nitro and Nitroso Compounds. In: Trost BM, Fleming I (eds) Comprehensive Organic Synthesis, vol 8, Pergamon, Oxford, p 363
2. Lang-Fuhrmann S, Pawlenko S (1992) Diazen-N-oxide (Azoxy-Verbindungen). In: Klamann D (ed) Methoden der organischen Chemie (Houben-Weyl), Bd E16d, Organische Stickstoff-Verbindungen IV, Teil I, Thieme, Stuttgart, p 119
3. Smith MB, March J (2001) March's advanced organic chemistry, 5th ed, Wiley, New York
4. Ren P, Pan S, Dong T, Wu S (1996) Synth Commun 26: 3903, and references cited therein
5. Clark, JH, Miller JM, So K-H (1978) J Chem Soc, Perkin I: 941
6. Siemeling U, Türk T, Schoeller WW, Redshaw C, Gibson VC (1998) Inorg Chem 37: 4738
7. This compound has been previously prepared by a different route; however, spectroscopic data have been unavailable: Wang SF, Mathew L, Warkentin J (1988) J Am Chem Soc 110: 7235
8. Tsuji T, Takashima H, Takeuchi H, Egawa T, Konaka S (2000) J Mol Struct 554: 203
9. Chebli C, Brisse F (1995) Acta Crystallogr C51: 1164
10. Ibers JA, Hamilton WC (eds) (1974) International Tables for X-ray Crystallography, vol IV, Kynoch Press, Birmingham
11. Sheldrick GM (1997) SHELXL 97, University of Göttingen, Germany