The Crystal Structure of [Na4(OSiPh3)4(H2O)3];Die Kristallstruktur von [Na4(OSiPh3)4(H2O)3]

Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences

Volumn 51, Issue 11, 1996, Pages 1583-1586

  Mommertz, A ^a   Dehnicke, K ^a   Magull, J ^b  

^a PHILIPPS UNIVERSITY MARBURG   (Germany)

^b UNIVERSITY OF KARLSRUHE   (Germany)

Author keywords

Crystal Structure; Sodium Triphenylsilanolate Hydrate; Synthesis

Indexed keywords

CRYSTAL STRUCTURE; HYDRATION; SILICON; SODIUM COMPOUNDS; SYNTHESIS (CHEMICAL);

COORDINATION NUMBER; CRYSTAL STRUCTURE DETERMINATION; HUMID ATMOSPHERES; LATTICE DIMENSIONS; SATURATED SOLUTIONS; SODIUM ATOM; SPACE GROUPS; TITLE COMPOUNDS;

CRYSTAL ATOMIC STRUCTURE;

EID: 0345984351     PISSN: 09320776     EISSN: None     Source Type: Journal    
DOI: 10.1515/znb-1996-1109     Document Type: Article

References (28)

1. O. Graalmann, U. Klingebiel, W. Clegg, M. Haase, G. M. Sheldrick, Angew. Chem. 96, 904 (1984); Angew. Chem. Int. Ed. Engl. 23, 891 (1984).
2. O. Graalmann, U. Klingebiel, W. Clegg, M. Haase, G. M. Sheldrick, Angew. Chem. 96, 904 (1984); Angew. Chem. Int. Ed. Engl. 23, 891 (1984).
3. K. Dippel, N. K. Keweloh, P. G. Jones, U. Klingebiel, D. Schmidt, Z. Naturforsch. 42b, 1253 (1987).
4. D. Schmidt-Bäse, U. Klingebiel, Chem. Ber. 122, 815 (1989).
5. S. Schütte, C. Freire-Erdbrugger, U. Klingebiel, G. M. Sheldrick, Phosphorus, Sulfur, Silicon 78, 75 (1993).
6. S. Schütte, U. Pieper, U. Klingebiel, D. Stalke, J. Organomet. Chem. 446, 45 (1993).
7. [61 P. B. Hitchcock, N. H. Buttus, A. C. Sullivan, J. Organomet. Chem. 303, 321 (1986).
8. M. J. McGeary, K. Folting, W. E. Streib, J. C. Huffman, K. G. Caulton, Polyhedron 10, 2699 (1991).
9. G. Boche, A. Opel, M. Marsch, K. Harms, F. Haller. J. C. W. Lohrenz, C. Tümmler, W. Koch, Chem. Ber. 125, 2265 (1992).
10. [91 G. R. Fuentes, P. S. Coan, W. E. Streib, K. G. Caulton, Polyhedron 10, 2371 (1991).
11. F. Pauer, G. M. Sheldrick, Acta Crystallogr. C49, 1283 (1993).
12. K. B. Renkema, R. J. Matthews, T. L. Bush, S. K. Hendges, R. N. Redding, F. W. Vance, M. E. Silver, S. A. Snow, J. C. Huffman, Inorg. Chim. Acta 244, 185 (1996).
13. O. V. Kononov, V. D. Lobkov, V. A. Igonin, S. V. Lindeman, V. E. Shklover, Yu. T. Struchkov, Metalloorg. Khim. 4, 784 (1991).
14. I. L. Dubchak, V. E. Shklover, M. Yu. Antipin, Yu. T. Struchkov, V. M. Kopylov, A. M. Muzafarov, P. L. Prikhod'ko, A. A. Zhdanov, Zh. Strukt. Khim. 23, 63 (1982).
15. I. L. Dubchak, V. E. Shklover, Yu. T. Struchkov, V. M. Kopylov, P. L. Prikhod'ko, Zh. Strukt. Khim. 24, 59 (1983).
16. R. J. H. Voorhoeve, Organohalosilanes: Precursors to Silicones, Elsevier, Amsterdam (1967); W. Noll, Chemistry and Technology of Silicones, Academic Press, New York (1968); H. A. Liebhafsky, Silicones under the Monogram, Wiley, New York (1978); J. Saam, Silicon Based Polymer Science, Advances in Chemistry Series No. 224, American Chemical Society, Washington, D. C. (1990), p. 145; C. S. Elsbernd, M. Spinu, V. J. Krukonis, P. M. Gallagher, D. K. Mohanty, J. E. McGrath, Silicon Based Polymer Science, Advances in Chemistry Series No. 224, American Chemical Society, Washington, D. C. (1990), p. 245.
17. R. J. H. Voorhoeve, Organohalosilanes: Precursors to Silicones, Elsevier, Amsterdam (1967); W. Noll, Chemistry and Technology of Silicones, Academic Press, New York (1968); H. A. Liebhafsky, Silicones under the Monogram, Wiley, New York (1978); J. Saam, Silicon Based Polymer Science, Advances in Chemistry Series No. 224, American Chemical Society, Washington, D. C. (1990), p. 145; C. S. Elsbernd, M. Spinu, V. J. Krukonis, P. M. Gallagher, D. K. Mohanty, J. E. McGrath, Silicon Based Polymer Science, Advances in Chemistry Series No. 224, American Chemical Society, Washington, D. C. (1990), p. 245.
18. R. J. H. Voorhoeve, Organohalosilanes: Precursors to Silicones, Elsevier, Amsterdam (1967); W. Noll, Chemistry and Technology of Silicones, Academic Press, New York (1968); H. A. Liebhafsky, Silicones under the Monogram, Wiley, New York (1978); J. Saam, Silicon Based Polymer Science, Advances in Chemistry Series No. 224, American Chemical Society, Washington, D. C. (1990), p. 145; C. S. Elsbernd, M. Spinu, V. J. Krukonis, P. M. Gallagher, D. K. Mohanty, J. E. McGrath, Silicon Based Polymer Science, Advances in Chemistry Series No. 224, American Chemical Society, Washington, D. C. (1990), p. 245.
19. R. J. H. Voorhoeve, Organohalosilanes: Precursors to Silicones, Elsevier, Amsterdam (1967); W. Noll, Chemistry and Technology of Silicones, Academic Press, New York (1968); H. A. Liebhafsky, Silicones under the Monogram, Wiley, New York (1978); J. Saam, Silicon Based Polymer Science, Advances in Chemistry Series No. 224, American Chemical Society, Washington, D. C. (1990), p. 145; C. S. Elsbernd, M. Spinu, V. J. Krukonis, P. M. Gallagher, D. K. Mohanty, J. E. McGrath, Silicon Based Polymer Science, Advances in Chemistry Series No. 224, American Chemical Society, Washington, D. C. (1990), p. 245.
20. R. J. H. Voorhoeve, Organohalosilanes: Precursors to Silicones, Elsevier, Amsterdam (1967); W. Noll, Chemistry and Technology of Silicones, Academic Press, New York (1968); H. A. Liebhafsky, Silicones under the Monogram, Wiley, New York (1978); J. Saam, Silicon Based Polymer Science, Advances in Chemistry Series No. 224, American Chemical Society, Washington, D. C. (1990), p. 145; C. S. Elsbernd, M. Spinu, V. J. Krukonis, P. M. Gallagher, D. K. Mohanty, J. E. McGrath, Silicon Based Polymer Science, Advances in Chemistry Series No. 224, American Chemical Society, Washington, D. C. (1990), p. 245.
21. K. Dehnicke, F. Weller, Coord. Chem. Rev., im Druck.
22. J. F. Hyde, O. K. Johannson, W. H. Daudt, R. F. Fleming, H. B. Laudenslager, M. P. Roche, J. Am. Chem. Soc. 75, 5615 (1953).
23. A. Mommertz, Diplomarbeit, Universität Marburg (1995).
24. J. Weidlein, U. Müller, K. Dehnicke, Schwingungsspektroskopie, G. Thieme-Verlag, Stuttgart - New York, 2. Aufl. (1988).
25. W. A. Bueno, Spectrochim. Acta 36A, 1059 (1980).
26. K. Licht, H. Kriegsmann, Z. Anorg. Allg. Chem. 323, 190 (1963).
27. H. Puff, K. Braun, H. Reuter, J. Organomet. Chem. 409, 119 (1991).
28. G. M. Sheldrick, SHEEXS-86, SHELXL-93, Programme zur Verfeinerung von Kristallstrukturen, Göttingen (1986), (1993).