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3-O group. For this reason, we decided to perform the reversible water loss experiment at 135-140°C, so that the iron-coordinated water is retained. In this temperature range complete loss of four lattice waters takes 5 hours because this process is kinetically slow at relatively lower temperature, as evidenced by the TGA plot of 1 taken after eight months from its preparation which shows gradual water loss even under ambient conditions.
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2O vapor is not ruled out.
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