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0345348477
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note
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2, 5% ether/hexane to 25% ether/hcxane) to give 1 (11.39 g, 22.3 mmol) in 76% yield and the bis-coupled product 5 (1.07 g, 1.9 mmol) in 7% yield.
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14
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0004055425
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Pergamon: Oxford
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Perrin, D.W.1
Armarego, W.L.F.2
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15
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0000311719
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Angelici, R. J., Ed.; Wiley; New York
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nd ed.; Pergamon: Oxford, 1980; p 547 and use of freshly prepared tetrakis(triphenylphosphine)palladium(0), Coulson, D. R. in Inorganic Syntheses; Vol. 28; Angelici, R. J., Ed.; Wiley; New York, 1990; p 107. rather than the use of commercially available sources were necessary for satisfactory and reproducible results.
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Coulson, D.R.1
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17
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33748664603
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21
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0345348476
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note
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4: C, 53.92; H, 6.41; N, 15.72. Found: C, 53.54; H, 6.39; N, 15.63.
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22
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0030814505
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Breipohl, G.; Will, D. W.; Peyman, A.; Uhlmann, E. Tetrahedron 1997, 53, 14671.
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Uhlmann, E.4
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