Column Switching Technique, Assisted on-Line Matrix Elimination, and Chiral Analysis of R- and S-1-Phenyl-1-butanol in Biphasic Saccharomyces cerevisiae Mediated Culture

Journal of Liquid Chromatography and Related Technologies

Volumn 26, Issue 19, 2003, Pages 3249-3264

  Tsai, Shiang Rong ^a   Cheng, Cheanyeh ^a  

^a CHUNG YUAN CHRISTIAN UNIVERSITY   (Taiwan)

Author keywords

Chiral; Column switching; Matrix elimination; Saccharomyces cerevisiae

Indexed keywords

CELL CULTURE; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; KETONES; YEAST;

CHIRAL PRODUCTS; COUPLED COLUMN SYSTEMS;

ALCOHOLS;

1 PHENYLBUTAN 1 OL; BUTANOL; KETONE DERIVATIVE; PHENYL N PROPYLKETONE; UNCLASSIFIED DRUG;

ACCURACY; ARTICLE; CHEMICAL ANALYSIS; CHIRAL CHROMATOGRAPHY; CHIRALITY; DEVICE; FUNGUS CULTURE; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; ONLINE ANALYSIS; SACCHAROMYCES CEREVISIAE; STANDARD; TECHNIQUE; TIME;

FUNGI; SACCHAROMYCES; SACCHAROMYCES CEREVISIAE;

EID: 0345256290     PISSN: 10826076     EISSN: None     Source Type: Journal    
DOI: 10.1081/JLC-120025521     Document Type: Article

References (15)

1. Cherrak, D.E.; Khattabi, S.; Guiochon, G. Adsorption behavior and prediction of the enantiomers of 3-chloro-1-phenyl-1-propanol influence of the mass transfer kinetics. J. Chromatogr. A 2000, 877, 109-122.
2. Cheng, C.; Ma, J.H. Enantioselective synthesis of S-(-)-1-phenylethanol in candida utilis semi-fed-batch cultures. Proc. Biochem. 1996, 31, 119-124.
3. Kartozia, I.; Kanyonyo, M.; Happaerts, T.; Lambert, D.M.; Scriba, G.K.E. ; Chankvetadze, B. Comparative HPLC enantioseparation of new chiral hydantoin derivatives on three different polysaccharide type chiral stationary phases. J. Pharm. Biomed. Anal. 2002, 27, 457-465.
4. Ning, J.G. Direct chiral separation with Chiralpak AD converted to the reversed phase mode. J. Chromatogr. A 1998, 805, 309-314.
5. Campins-Falcó, P.; Herráez-Hernández, R.; Sevillano-Cabeza, A. Column-switching techniques for high-performance liquid chromatography of drugs in biological samples. J. Chromatogr. 1993, 619, 177-190.
6. Fujitomo, H.; Nagaoka, T.; Nishino, I.; Umeda, T. Determination of a new oral cephalosporin, s-1090, in human plasma and urine by direct injection high-performance liquid chromatography with ultraviolet detection and column switching. J. Chromatogr. B 1999, 728, 125-131.
7. Lamprecht, G.; Kraushofer, T.; Stoschitzky, K.; Lindner, W. Enantio-selective analysis of (R)- and (S)-atenolol in urine samples by a high-performance liquid chromatography column-switching setup. J. Chromatogr. B 2000, 740, 219-226.
8. Murahashi, T.; Hayakawa, K. A sensitive method for the determination of 6-nitrochrysene, 2-nitro-fluoranthene and 1-, 2- and 4-nitropyrenes in airborne particulates using high-performance liquid chromatography with chemiluminescence detection. Anal. Chim. Acta. 1997, 343, 251-257.
9. Huang, Y.; Mou, S.F.; Riviello, J.M. Determination of ammonium in seawater by column-switching ion chromatography. J. Chromatogr. A 2000, 868, 209-216.
10. Blahová, E.; Bovanová, L.; Brandšteterová, E. Direct HPLC analysis of trimethoprim in milk. J. Liq. Chrom. & Rel. Technol. 2001, 24 (19), 3027-3035.
11. Wang, H.; Xu, H.; Guan, Y. Column switching-back flushing technique for the analysis of aromatic compounds in gasoline. J. Chromatogr. A 2002, 972, 253-258.
12. Cheng, C.; Wu, S.C. Analysis of the enzymatic racemization of D-aspartic acid to L-aspartic acid by the on-line coupling of a solid-phase extraction column and a ligand-exchange high-performance liquid chromatography column. J. Chromatogr. A 2000, 896, 299-310.
13. Oertel, R.; Richter, K.; Fauler, J.; Kirch, W. Increasing sample throughput in pharmacological studies by using dual-column liquid chromatography with tandem mass spectrometry. J. Chromatogr. A 2002, 948, 187-192.
14. Zeng, H.; Wu, J.T.; Unger, S.E. The investigation and the use of high flow column-switching LC/MS/MS as a high-throughput approach for direct plasma sample analysis of single and multiple components in pharmacokinetic studies. J. Pharm. Biomed. Anal. 2002, 27, 967-982.
15. Mathews, C.K.; van Holde, K.E.; Ahem, K.G. Enzymes: biological catalysts. In Biochemistry, 3rd Ed.; Addison Wesley Longman, Inc.: San Francisco, CA, 2000; 391 pp.