A simple one pot synthesis of 1-chlorophospholes

Phosphorus, Sulfur and Silicon and Related Elements

Volumn 118, Issue 1-4, 1996, Pages 309-312

  Teunissen, Herman T ^a   Hansen, Carola B ^b   Bickelhaupt, Friedrich ^a  

^a VU UNIVERSITY AMSTERDAM   (Netherlands)

^b DSM RESEARCH   (Netherlands)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0345106885     PISSN: 10426507     EISSN: None     Source Type: Journal    
DOI: 10.1080/10426509608038822     Document Type: Article

References (15)

1. F. Mathey, Chem. Rev., 88, 429 (1988).
2. A.N. Hughes, in Handbook of Organophosphorus Chemistry, R. Engel (Ed) (M. Dekker Inc., New York 1992), Chap. 10, pp. 483-558.
3. (a) F. Nief and L. Ricard, J. Organomet. Chem., 464, 149 (1994).
4. (b) T. Douglas and K.H. Theopold, Angew. Chem., 101, 1394 (1988).
5. (c) C. Charrier, H. Bonnard, F. Mathey and D. Neibecker, J. Organomet. Chem., 231, 361 (1982).
6. (d) E.W. Abel and C. Towers, J. Chem. Soc. Dalton Trans., 814 (1979).
7. (e) G.O. Doak, L.D. Freedman and J.B. Levy, J. Org. Chem. 29, 2382 (1964).
8. A. Sekiguchi, S.S. Zigler, K.J. Haller and R. West, Recl. Trav. Chim. Pays-Bas 107, 197 (1988).
9. 2P 456.0601, found 456.0598.
10. (a) J.J. Eisch, Organometallic Synthesis (Academic Press, New York, 1981), Vol. 2, pp. 99-100.
11. (b) W. Schlenk and E. Bergmann, Justus Liebigs Ann. Chem., 463, 1 (1928).
12. (c) E. Bergmann and O. Zwecker, Justus Liebigs Ann. Chem., 487, 155 (1931).
13. H. Gilman and B.J. Gaj, J. Org. Chem., 22, 447 (1957).
14. 3e 6 is described as yellow crystals of mp. 53-56°C; apparently this sample was not quite pure.
15. 1H NMR spectrum of 5-phenyldibenzophosphole: J.H. Nelson, S. Affandi, G.A. Gray and E.C. Alyea, Magn. Res. Chem., 25, 774 (1987).