X-Ray Structure of Keggin-type Peroxo Polyoxometalate A- α-[Si(NbO2)3W9O37] 7-

Bulletin of the Korean Chemical Society

Volumn 24, Issue 7, 2003, Pages 1005-1008

  Kim, Gyu Shik ^a   Zeng, Huadong ^b   Hill, Craig L ^b  

^a Kangwon National University   (South Korea)

^b EMORY UNIVERSITY   (United States)

Author keywords

Keggin; Niobium; Peroxo; Polyoxometalates; Tungsten

Indexed keywords

NIOBIUM; SILICON DERIVATIVE; TUNGSTEN DERIVATIVE;

AQUEOUS SOLUTION; ARTICLE; CRYSTAL STRUCTURE; MOLECULAR SIZE; MOLECULAR STABILITY; STRUCTURE ANALYSIS; SUPRAMOLECULAR CHEMISTRY; SYNTHESIS; X RAY CRYSTALLOGRAPHY; X RAY DIFFRACTION;

EID: 0344876454     PISSN: 02532964     EISSN: None     Source Type: Journal    
DOI: 10.5012/bkcs.2003.24.7.1005     Document Type: Article

References (21)

1. For the first synthesis of tetrabutylammonium salt of this peroxniobium anion, see Droege, M. W.; Finke, R. G. J. Mol. Catal. 1991, 69, 323.
2. Kim, G.-S.; Judd, D. A.; Hill, C. L.; Schinazi, R. F. J. Med. Chem. 1994, 37, 816.
3. Rhule, J. T.; Hill, C. L.; Judd, D. A.; Schinazi, R. F. Chem. Rev. 1998, 98, 327.
4. Kim, G.-S.; Zeng, H.; VanDerveer, D.; Hill, C. L. Angew. Chem. Int. Ed. 1999, 30, 3205.
5. Kim, G.-S; Zeng, H.; Weinstock, I. A.; Rhule, J. T.; VanDerveer, D.; Hill, C. L. Inorg. Chem., in submission.
6. See also Kim, G.-S; Zeng, H.; Rhule, J. T.; Weinstock, I. A.; Hill, C. L. J. Chem. Soc., Chem. Commun. 1999, 17, 1651.
7. Judd, D. A.; Chen, Q.; Campana, C. F.; Hill, C. L. J. Am. Chem. Soc. 1997, 119, 5461.
8. Klemperer, W. G. In Inorganic Syntheses; John Wiley and Sons, Inc.: New York, 1990; Vol. 27, p 71.
9. Dabbabi, M.; Boyer, M. J. Inorg. Nucl. Chem. 1976, 38, 1011.
10. SMART, version 4.05; Siemens Analytical X-ray Systems, Inc.: Madison, WI, 1995.
11. SAINT, version 4.05; Siemens Analytical X-ray Systems. Inc.: Madison, WI, 1995.
12. SADABS: Siemens area detector absorption correction program; Siemens Analytical X-ray Systems, Inc.: Madison, WI, 1995.
13. Sheldrick, G. M. SHELX-97 program package for structure solution and refinement; University Goettingen: Germany, 1997.
14. 2-) are low nuclearity polyanions and are better regarded as class of complexes distinct from conventional POMs.
15. Dickman, M. H.; Pope, M. T. Chem. Rev. 1994, 94, 569.
16. Bas-Serra, J.; Todorut, I.; Jameson, G. B.; Acerete, R.; Baker, L. C. W. Abstract of Paper No. 77b Presented at the Intl. Chem. Congress of Pacific Basin Societies, Honolulu, 1989.
17. Server-Carrió, J.; Bas-Serra, J.; González-Núñ ez, M. E.; García-Gastaldi, A.; Jameson, G. B.; Baker, L. C. W.; Acerete, R. J. Am. Chem. Soc. 1999, 121, 911.
18. Harrup, M. K.; Kim, G.-S.; Zeng, H.; Johnson, R. P.; VanDerveer, D.; Hill, C. L. Inorg. Chem. 1998, 37, 5550.
19. Vaska, L. Acc. Chem. Res. 1976, 9, 175.
20. Mathern, G.; Weiss, R. Acta Cryst. 1971, B27, 1598.
21. Roch, M.; Weber, J.; Williams, A. F. Inorg. Chem. 1984, 23, 4572.