Product Diversity in the Reactions of Tp*W(S 2CNEt 2)(CO) 2 with Alkynes: Novel η 2-Alkyne and Tungstathiaenone Complexes

Organometallics

Volumn 22, Issue 24, 2003, Pages 4853-4860

  Lim, Patrick J ^a,c   Slizys, Damian A ^a   White, Jonathan M ^a   Young, Charles G ^a   Tiekink, Edward R T ^b  

^a UNIVERSITY OF MELBOURNE   (Australia)

^b NATIONAL UNIVERSITY OF SINGAPORE   (Singapore)

^c UNIVERSITY OF SAN CARLOS   (Philippines)

Author keywords

[No Author keywords available]

Indexed keywords

LIGANDS; METAL COMPLEXES;

CHEMICAL BONDS; CORRELATION METHODS; DESULFURIZATION; MASS SPECTROMETRY; MOLECULAR STRUCTURE; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; PHOTOCHEMICAL REACTIONS; TUNGSTEN COMPOUNDS; ULTRAVIOLET RADIATION; X RAY DIFFRACTION ANALYSIS;

ORGANOMETALLICS;

EID: 0344875529     PISSN: 02767333     EISSN: None     Source Type: Journal    
DOI: 10.1021/om030416w     Document Type: Article

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62. Many stable alkyne W-Tp* complexes have been prepared by Templeton and co-workers. Selected reports include: (a) Feng, S. G.; Philipp, C. C.; Gamble, A. S.; White, P. S.; Templeton, J. L. Organometallics 1991, 10, 3504-3512. (b) Feng, S. G.; White, P. S.; Templeton, J. L. J. Am. Chem. Soc. 1992, 114, 2951-2960. (c) Collins, M. A.; Feng, S. G.; White, P. A.; Templeton, J. L. J. Am. Chem. Soc. 1992, 114, 3771-3775. (d) Caldarelli, J. L.; White, P. S.; Templeton, J. L. J. Am. Chem. Soc. 1992, 114, 10097-10103. (e) Feng, S. G.; White, P. S.; Templeton, J. L. Organometallics 1993, 12, 1765-1774. (f) Feng, S. G.; White, P. S.; Templeton, J. L. Organometallics 1993, 12, 2131-2139. (g) Caldarelli, J. L.; Wagner, L. E.; White, P. S.; Templeton, J. L. J. Am. Chem. Soc. 1994, 116, 2878-2888. (h) Gunnoe. T. B.; White, P. S.; Templeton, J. L. J. Am. Chem. Soc. 1996, 118, 6916-6923. (i) Francisco, L. W.; White, P. S.; Templeton, J. L. Organometallics 1996, 15, 5127-5136. (j) Gunnoe, T. B.; White, P. S.; Templeton, J. L.; Casarrubios, L. J. Am. Chem. Soc. 1997, 119, 3171-3172. (k) Wells, M. B.; White, P. S.; Templeton, J. L. Organometallics 1997, 16, 1857-1864. (l) Francisco, L. W.; White, P. S.; Templeton, J. L. Organometallics 1997, 16, 2547-2555. (m) Frohnapfel, D. S.; Reinartz, S.; White, P. S.; Templeton, J. L. Organometallics 1998, 17, 8759-3769. (n) Schuster, D. M.; White, P. S.; Templeton, J. L. Organometallics 2000, 19, 1540-1548.
63. Many stable alkyne W-Tp* complexes have been prepared by Templeton and co-workers. Selected reports include: (a) Feng, S. G.; Philipp, C. C.; Gamble, A. S.; White, P. S.; Templeton, J. L. Organometallics 1991, 10, 3504-3512. (b) Feng, S. G.; White, P. S.; Templeton, J. L. J. Am. Chem. Soc. 1992, 114, 2951-2960. (c) Collins, M. A.; Feng, S. G.; White, P. A.; Templeton, J. L. J. Am. Chem. Soc. 1992, 114, 3771-3775. (d) Caldarelli, J. L.; White, P. S.; Templeton, J. L. J. Am. Chem. Soc. 1992, 114, 10097-10103. (e) Feng, S. G.; White, P. S.; Templeton, J. L. Organometallics 1993, 12, 1765-1774. (f) Feng, S. G.; White, P. S.; Templeton, J. L. Organometallics 1993, 12, 2131-2139. (g) Caldarelli, J. L.; Wagner, L. E.; White, P. S.; Templeton, J. L. J. Am. Chem. Soc. 1994, 116, 2878-2888. (h) Gunnoe. T. B.; White, P. S.; Templeton, J. L. J. Am. Chem. Soc. 1996, 118, 6916-6923. (i) Francisco, L. W.; White, P. S.; Templeton, J. L. Organometallics 1996, 15, 5127-5136. (j) Gunnoe, T. B.; White, P. S.; Templeton, J. L.; Casarrubios, L. J. Am. Chem. Soc. 1997, 119, 3171-3172. (k) Wells, M. B.; White, P. S.; Templeton, J. L. Organometallics 1997, 16, 1857-1864. (l) Francisco, L. W.; White, P. S.; Templeton, J. L. Organometallics 1997, 16, 2547-2555. (m) Frohnapfel, D. S.; Reinartz, S.; White, P. S.; Templeton, J. L. Organometallics 1998, 17, 8759-3769. (n) Schuster, D. M.; White, P. S.; Templeton, J. L. Organometallics 2000, 19, 1540-1548.
64. Many stable alkyne W-Tp* complexes have been prepared by Templeton and co-workers. Selected reports include: (a) Feng, S. G.; Philipp, C. C.; Gamble, A. S.; White, P. S.; Templeton, J. L. Organometallics 1991, 10, 3504-3512. (b) Feng, S. G.; White, P. S.; Templeton, J. L. J. Am. Chem. Soc. 1992, 114, 2951-2960. (c) Collins, M. A.; Feng, S. G.; White, P. A.; Templeton, J. L. J. Am. Chem. Soc. 1992, 114, 3771-3775. (d) Caldarelli, J. L.; White, P. S.; Templeton, J. L. J. Am. Chem. Soc. 1992, 114, 10097-10103. (e) Feng, S. G.; White, P. S.; Templeton, J. L. Organometallics 1993, 12, 1765-1774. (f) Feng, S. G.; White, P. S.; Templeton, J. L. Organometallics 1993, 12, 2131-2139. (g) Caldarelli, J. L.; Wagner, L. E.; White, P. S.; Templeton, J. L. J. Am. Chem. Soc. 1994, 116, 2878-2888. (h) Gunnoe. T. B.; White, P. S.; Templeton, J. L. J. Am. Chem. Soc. 1996, 118, 6916-6923. (i) Francisco, L. W.; White, P. S.; Templeton, J. L. Organometallics 1996, 15, 5127-5136. (j) Gunnoe, T. B.; White, P. S.; Templeton, J. L.; Casarrubios, L. J. Am. Chem. Soc. 1997, 119, 3171-3172. (k) Wells, M. B.; White, P. S.; Templeton, J. L. Organometallics 1997, 16, 1857-1864. (l) Francisco, L. W.; White, P. S.; Templeton, J. L. Organometallics 1997, 16, 2547-2555. (m) Frohnapfel, D. S.; Reinartz, S.; White, P. S.; Templeton, J. L. Organometallics 1998, 17, 8759-3769. (n) Schuster, D. M.; White, P. S.; Templeton, J. L. Organometallics 2000, 19, 1540-1548.
65. Many stable alkyne W-Tp* complexes have been prepared by Templeton and co-workers. Selected reports include: (a) Feng, S. G.; Philipp, C. C.; Gamble, A. S.; White, P. S.; Templeton, J. L. Organometallics 1991, 10, 3504-3512. (b) Feng, S. G.; White, P. S.; Templeton, J. L. J. Am. Chem. Soc. 1992, 114, 2951-2960. (c) Collins, M. A.; Feng, S. G.; White, P. A.; Templeton, J. L. J. Am. Chem. Soc. 1992, 114, 3771-3775. (d) Caldarelli, J. L.; White, P. S.; Templeton, J. L. J. Am. Chem. Soc. 1992, 114, 10097-10103. (e) Feng, S. G.; White, P. S.; Templeton, J. L. Organometallics 1993, 12, 1765-1774. (f) Feng, S. G.; White, P. S.; Templeton, J. L. Organometallics 1993, 12, 2131-2139. (g) Caldarelli, J. L.; Wagner, L. E.; White, P. S.; Templeton, J. L. J. Am. Chem. Soc. 1994, 116, 2878-2888. (h) Gunnoe. T. B.; White, P. S.; Templeton, J. L. J. Am. Chem. Soc. 1996, 118, 6916-6923. (i) Francisco, L. W.; White, P. S.; Templeton, J. L. Organometallics 1996, 15, 5127-5136. (j) Gunnoe, T. B.; White, P. S.; Templeton, J. L.; Casarrubios, L. J. Am. Chem. Soc. 1997, 119, 3171-3172. (k) Wells, M. B.; White, P. S.; Templeton, J. L. Organometallics 1997, 16, 1857-1864. (l) Francisco, L. W.; White, P. S.; Templeton, J. L. Organometallics 1997, 16, 2547-2555. (m) Frohnapfel, D. S.; Reinartz, S.; White, P. S.; Templeton, J. L. Organometallics 1998, 17, 8759-3769. (n) Schuster, D. M.; White, P. S.; Templeton, J. L. Organometallics 2000, 19, 1540-1548.
66. Many stable alkyne W-Tp* complexes have been prepared by Templeton and co-workers. Selected reports include: (a) Feng, S. G.; Philipp, C. C.; Gamble, A. S.; White, P. S.; Templeton, J. L. Organometallics 1991, 10, 3504-3512. (b) Feng, S. G.; White, P. S.; Templeton, J. L. J. Am. Chem. Soc. 1992, 114, 2951-2960. (c) Collins, M. A.; Feng, S. G.; White, P. A.; Templeton, J. L. J. Am. Chem. Soc. 1992, 114, 3771-3775. (d) Caldarelli, J. L.; White, P. S.; Templeton, J. L. J. Am. Chem. Soc. 1992, 114, 10097-10103. (e) Feng, S. G.; White, P. S.; Templeton, J. L. Organometallics 1993, 12, 1765-1774. (f) Feng, S. G.; White, P. S.; Templeton, J. L. Organometallics 1993, 12, 2131-2139. (g) Caldarelli, J. L.; Wagner, L. E.; White, P. S.; Templeton, J. L. J. Am. Chem. Soc. 1994, 116, 2878-2888. (h) Gunnoe. T. B.; White, P. S.; Templeton, J. L. J. Am. Chem. Soc. 1996, 118, 6916-6923. (i) Francisco, L. W.; White, P. S.; Templeton, J. L. Organometallics 1996, 15, 5127-5136. (j) Gunnoe, T. B.; White, P. S.; Templeton, J. L.; Casarrubios, L. J. Am. Chem. Soc. 1997, 119, 3171-3172. (k) Wells, M. B.; White, P. S.; Templeton, J. L. Organometallics 1997, 16, 1857-1864. (l) Francisco, L. W.; White, P. S.; Templeton, J. L. Organometallics 1997, 16, 2547-2555. (m) Frohnapfel, D. S.; Reinartz, S.; White, P. S.; Templeton, J. L. Organometallics 1998, 17, 8759-3769. (n) Schuster, D. M.; White, P. S.; Templeton, J. L. Organometallics 2000, 19, 1540-1548.
67. Many stable alkyne W-Tp* complexes have been prepared by Templeton and co-workers. Selected reports include: (a) Feng, S. G.; Philipp, C. C.; Gamble, A. S.; White, P. S.; Templeton, J. L. Organometallics 1991, 10, 3504-3512. (b) Feng, S. G.; White, P. S.; Templeton, J. L. J. Am. Chem. Soc. 1992, 114, 2951-2960. (c) Collins, M. A.; Feng, S. G.; White, P. A.; Templeton, J. L. J. Am. Chem. Soc. 1992, 114, 3771-3775. (d) Caldarelli, J. L.; White, P. S.; Templeton, J. L. J. Am. Chem. Soc. 1992, 114, 10097-10103. (e) Feng, S. G.; White, P. S.; Templeton, J. L. Organometallics 1993, 12, 1765-1774. (f) Feng, S. G.; White, P. S.; Templeton, J. L. Organometallics 1993, 12, 2131-2139. (g) Caldarelli, J. L.; Wagner, L. E.; White, P. S.; Templeton, J. L. J. Am. Chem. Soc. 1994, 116, 2878-2888. (h) Gunnoe. T. B.; White, P. S.; Templeton, J. L. J. Am. Chem. Soc. 1996, 118, 6916-6923. (i) Francisco, L. W.; White, P. S.; Templeton, J. L. Organometallics 1996, 15, 5127-5136. (j) Gunnoe, T. B.; White, P. S.; Templeton, J. L.; Casarrubios, L. J. Am. Chem. Soc. 1997, 119, 3171-3172. (k) Wells, M. B.; White, P. S.; Templeton, J. L. Organometallics 1997, 16, 1857-1864. (l) Francisco, L. W.; White, P. S.; Templeton, J. L. Organometallics 1997, 16, 2547-2555. (m) Frohnapfel, D. S.; Reinartz, S.; White, P. S.; Templeton, J. L. Organometallics 1998, 17, 8759-3769. (n) Schuster, D. M.; White, P. S.; Templeton, J. L. Organometallics 2000, 19, 1540-1548.
68. Many stable alkyne W-Tp* complexes have been prepared by Templeton and co-workers. Selected reports include: (a) Feng, S. G.; Philipp, C. C.; Gamble, A. S.; White, P. S.; Templeton, J. L. Organometallics 1991, 10, 3504-3512. (b) Feng, S. G.; White, P. S.; Templeton, J. L. J. Am. Chem. Soc. 1992, 114, 2951-2960. (c) Collins, M. A.; Feng, S. G.; White, P. A.; Templeton, J. L. J. Am. Chem. Soc. 1992, 114, 3771-3775. (d) Caldarelli, J. L.; White, P. S.; Templeton, J. L. J. Am. Chem. Soc. 1992, 114, 10097-10103. (e) Feng, S. G.; White, P. S.; Templeton, J. L. Organometallics 1993, 12, 1765-1774. (f) Feng, S. G.; White, P. S.; Templeton, J. L. Organometallics 1993, 12, 2131-2139. (g) Caldarelli, J. L.; Wagner, L. E.; White, P. S.; Templeton, J. L. J. Am. Chem. Soc. 1994, 116, 2878-2888. (h) Gunnoe. T. B.; White, P. S.; Templeton, J. L. J. Am. Chem. Soc. 1996, 118, 6916-6923. (i) Francisco, L. W.; White, P. S.; Templeton, J. L. Organometallics 1996, 15, 5127-5136. (j) Gunnoe, T. B.; White, P. S.; Templeton, J. L.; Casarrubios, L. J. Am. Chem. Soc. 1997, 119, 3171-3172. (k) Wells, M. B.; White, P. S.; Templeton, J. L. Organometallics 1997, 16, 1857-1864. (l) Francisco, L. W.; White, P. S.; Templeton, J. L. Organometallics 1997, 16, 2547-2555. (m) Frohnapfel, D. S.; Reinartz, S.; White, P. S.; Templeton, J. L. Organometallics 1998, 17, 8759-3769. (n) Schuster, D. M.; White, P. S.; Templeton, J. L. Organometallics 2000, 19, 1540-1548.
69. Many stable alkyne W-Tp* complexes have been prepared by Templeton and co-workers. Selected reports include: (a) Feng, S. G.; Philipp, C. C.; Gamble, A. S.; White, P. S.; Templeton, J. L. Organometallics 1991, 10, 3504-3512. (b) Feng, S. G.; White, P. S.; Templeton, J. L. J. Am. Chem. Soc. 1992, 114, 2951-2960. (c) Collins, M. A.; Feng, S. G.; White, P. A.; Templeton, J. L. J. Am. Chem. Soc. 1992, 114, 3771-3775. (d) Caldarelli, J. L.; White, P. S.; Templeton, J. L. J. Am. Chem. Soc. 1992, 114, 10097-10103. (e) Feng, S. G.; White, P. S.; Templeton, J. L. Organometallics 1993, 12, 1765-1774. (f) Feng, S. G.; White, P. S.; Templeton, J. L. Organometallics 1993, 12, 2131-2139. (g) Caldarelli, J. L.; Wagner, L. E.; White, P. S.; Templeton, J. L. J. Am. Chem. Soc. 1994, 116, 2878-2888. (h) Gunnoe. T. B.; White, P. S.; Templeton, J. L. J. Am. Chem. Soc. 1996, 118, 6916-6923. (i) Francisco, L. W.; White, P. S.; Templeton, J. L. Organometallics 1996, 15, 5127-5136. (j) Gunnoe, T. B.; White, P. S.; Templeton, J. L.; Casarrubios, L. J. Am. Chem. Soc. 1997, 119, 3171-3172. (k) Wells, M. B.; White, P. S.; Templeton, J. L. Organometallics 1997, 16, 1857-1864. (l) Francisco, L. W.; White, P. S.; Templeton, J. L. Organometallics 1997, 16, 2547-2555. (m) Frohnapfel, D. S.; Reinartz, S.; White, P. S.; Templeton, J. L. Organometallics 1998, 17, 8759-3769. (n) Schuster, D. M.; White, P. S.; Templeton, J. L. Organometallics 2000, 19, 1540-1548.
70. Many stable alkyne W-Tp* complexes have been prepared by Templeton and co-workers. Selected reports include: (a) Feng, S. G.; Philipp, C. C.; Gamble, A. S.; White, P. S.; Templeton, J. L. Organometallics 1991, 10, 3504-3512. (b) Feng, S. G.; White, P. S.; Templeton, J. L. J. Am. Chem. Soc. 1992, 114, 2951-2960. (c) Collins, M. A.; Feng, S. G.; White, P. A.; Templeton, J. L. J. Am. Chem. Soc. 1992, 114, 3771-3775. (d) Caldarelli, J. L.; White, P. S.; Templeton, J. L. J. Am. Chem. Soc. 1992, 114, 10097-10103. (e) Feng, S. G.; White, P. S.; Templeton, J. L. Organometallics 1993, 12, 1765-1774. (f) Feng, S. G.; White, P. S.; Templeton, J. L. Organometallics 1993, 12, 2131-2139. (g) Caldarelli, J. L.; Wagner, L. E.; White, P. S.; Templeton, J. L. J. Am. Chem. Soc. 1994, 116, 2878-2888. (h) Gunnoe. T. B.; White, P. S.; Templeton, J. L. J. Am. Chem. Soc. 1996, 118, 6916-6923. (i) Francisco, L. W.; White, P. S.; Templeton, J. L. Organometallics 1996, 15, 5127-5136. (j) Gunnoe, T. B.; White, P. S.; Templeton, J. L.; Casarrubios, L. J. Am. Chem. Soc. 1997, 119, 3171-3172. (k) Wells, M. B.; White, P. S.; Templeton, J. L. Organometallics 1997, 16, 1857-1864. (l) Francisco, L. W.; White, P. S.; Templeton, J. L. Organometallics 1997, 16, 2547-2555. (m) Frohnapfel, D. S.; Reinartz, S.; White, P. S.; Templeton, J. L. Organometallics 1998, 17, 8759-3769. (n) Schuster, D. M.; White, P. S.; Templeton, J. L. Organometallics 2000, 19, 1540-1548.
71. Many stable alkyne W-Tp* complexes have been prepared by Templeton and co-workers. Selected reports include: (a) Feng, S. G.; Philipp, C. C.; Gamble, A. S.; White, P. S.; Templeton, J. L. Organometallics 1991, 10, 3504-3512. (b) Feng, S. G.; White, P. S.; Templeton, J. L. J. Am. Chem. Soc. 1992, 114, 2951-2960. (c) Collins, M. A.; Feng, S. G.; White, P. A.; Templeton, J. L. J. Am. Chem. Soc. 1992, 114, 3771-3775. (d) Caldarelli, J. L.; White, P. S.; Templeton, J. L. J. Am. Chem. Soc. 1992, 114, 10097-10103. (e) Feng, S. G.; White, P. S.; Templeton, J. L. Organometallics 1993, 12, 1765-1774. (f) Feng, S. G.; White, P. S.; Templeton, J. L. Organometallics 1993, 12, 2131-2139. (g) Caldarelli, J. L.; Wagner, L. E.; White, P. S.; Templeton, J. L. J. Am. Chem. Soc. 1994, 116, 2878-2888. (h) Gunnoe. T. B.; White, P. S.; Templeton, J. L. J. Am. Chem. Soc. 1996, 118, 6916-6923. (i) Francisco, L. W.; White, P. S.; Templeton, J. L. Organometallics 1996, 15, 5127-5136. (j) Gunnoe, T. B.; White, P. S.; Templeton, J. L.; Casarrubios, L. J. Am. Chem. Soc. 1997, 119, 3171-3172. (k) Wells, M. B.; White, P. S.; Templeton, J. L. Organometallics 1997, 16, 1857-1864. (l) Francisco, L. W.; White, P. S.; Templeton, J. L. Organometallics 1997, 16, 2547-2555. (m) Frohnapfel, D. S.; Reinartz, S.; White, P. S.; Templeton, J. L. Organometallics 1998, 17, 8759-3769. (n) Schuster, D. M.; White, P. S.; Templeton, J. L. Organometallics 2000, 19, 1540-1548.
72. Many stable alkyne W-Tp* complexes have been prepared by Templeton and co-workers. Selected reports include: (a) Feng, S. G.; Philipp, C. C.; Gamble, A. S.; White, P. S.; Templeton, J. L. Organometallics 1991, 10, 3504-3512. (b) Feng, S. G.; White, P. S.; Templeton, J. L. J. Am. Chem. Soc. 1992, 114, 2951-2960. (c) Collins, M. A.; Feng, S. G.; White, P. A.; Templeton, J. L. J. Am. Chem. Soc. 1992, 114, 3771-3775. (d) Caldarelli, J. L.; White, P. S.; Templeton, J. L. J. Am. Chem. Soc. 1992, 114, 10097-10103. (e) Feng, S. G.; White, P. S.; Templeton, J. L. Organometallics 1993, 12, 1765-1774. (f) Feng, S. G.; White, P. S.; Templeton, J. L. Organometallics 1993, 12, 2131-2139. (g) Caldarelli, J. L.; Wagner, L. E.; White, P. S.; Templeton, J. L. J. Am. Chem. Soc. 1994, 116, 2878-2888. (h) Gunnoe. T. B.; White, P. S.; Templeton, J. L. J. Am. Chem. Soc. 1996, 118, 6916-6923. (i) Francisco, L. W.; White, P. S.; Templeton, J. L. Organometallics 1996, 15, 5127-5136. (j) Gunnoe, T. B.; White, P. S.; Templeton, J. L.; Casarrubios, L. J. Am. Chem. Soc. 1997, 119, 3171-3172. (k) Wells, M. B.; White, P. S.; Templeton, J. L. Organometallics 1997, 16, 1857-1864. (l) Francisco, L. W.; White, P. S.; Templeton, J. L. Organometallics 1997, 16, 2547-2555. (m) Frohnapfel, D. S.; Reinartz, S.; White, P. S.; Templeton, J. L. Organometallics 1998, 17, 8759-3769. (n) Schuster, D. M.; White, P. S.; Templeton, J. L. Organometallics 2000, 19, 1540-1548.
73. Many stable alkyne W-Tp* complexes have been prepared by Templeton and co-workers. Selected reports include: (a) Feng, S. G.; Philipp, C. C.; Gamble, A. S.; White, P. S.; Templeton, J. L. Organometallics 1991, 10, 3504-3512. (b) Feng, S. G.; White, P. S.; Templeton, J. L. J. Am. Chem. Soc. 1992, 114, 2951-2960. (c) Collins, M. A.; Feng, S. G.; White, P. A.; Templeton, J. L. J. Am. Chem. Soc. 1992, 114, 3771-3775. (d) Caldarelli, J. L.; White, P. S.; Templeton, J. L. J. Am. Chem. Soc. 1992, 114, 10097-10103. (e) Feng, S. G.; White, P. S.; Templeton, J. L. Organometallics 1993, 12, 1765-1774. (f) Feng, S. G.; White, P. S.; Templeton, J. L. Organometallics 1993, 12, 2131-2139. (g) Caldarelli, J. L.; Wagner, L. E.; White, P. S.; Templeton, J. L. J. Am. Chem. Soc. 1994, 116, 2878-2888. (h) Gunnoe. T. B.; White, P. S.; Templeton, J. L. J. Am. Chem. Soc. 1996, 118, 6916-6923. (i) Francisco, L. W.; White, P. S.; Templeton, J. L. Organometallics 1996, 15, 5127-5136. (j) Gunnoe, T. B.; White, P. S.; Templeton, J. L.; Casarrubios, L. J. Am. Chem. Soc. 1997, 119, 3171-3172. (k) Wells, M. B.; White, P. S.; Templeton, J. L. Organometallics 1997, 16, 1857-1864. (l) Francisco, L. W.; White, P. S.; Templeton, J. L. Organometallics 1997, 16, 2547-2555. (m) Frohnapfel, D. S.; Reinartz, S.; White, P. S.; Templeton, J. L. Organometallics 1998, 17, 3759-3769. (n) Schuster, D. M.; White, P. S.; Templeton, J. L. Organometallics 2000, 19, 1540-1548.
74. Many stable alkyne W-Tp* complexes have been prepared by Templeton and co-workers. Selected reports include: (a) Feng, S. G.; Philipp, C. C.; Gamble, A. S.; White, P. S.; Templeton, J. L. Organometallics 1991, 10, 3504-3512. (b) Feng, S. G.; White, P. S.; Templeton, J. L. J. Am. Chem. Soc. 1992, 114, 2951-2960. (c) Collins, M. A.; Feng, S. G.; White, P. A.; Templeton, J. L. J. Am. Chem. Soc. 1992, 114, 3771-3775. (d) Caldarelli, J. L.; White, P. S.; Templeton, J. L. J. Am. Chem. Soc. 1992, 114, 10097-10103. (e) Feng, S. G.; White, P. S.; Templeton, J. L. Organometallics 1993, 12, 1765-1774. (f) Feng, S. G.; White, P. S.; Templeton, J. L. Organometallics 1993, 12, 2131-2139. (g) Caldarelli, J. L.; Wagner, L. E.; White, P. S.; Templeton, J. L. J. Am. Chem. Soc. 1994, 116, 2878-2888. (h) Gunnoe. T. B.; White, P. S.; Templeton, J. L. J. Am. Chem. Soc. 1996, 118, 6916-6923. (i) Francisco, L. W.; White, P. S.; Templeton, J. L. Organometallics 1996, 15, 5127-5136. (j) Gunnoe, T. B.; White, P. S.; Templeton, J. L.; Casarrubios, L. J. Am. Chem. Soc. 1997, 119, 3171-3172. (k) Wells, M. B.; White, P. S.; Templeton, J. L. Organometallics 1997, 16, 1857-1864. (l) Francisco, L. W.; White, P. S.; Templeton, J. L. Organometallics 1997, 16, 2547-2555. (m) Frohnapfel, D. S.; Reinartz, S.; White, P. S.; Templeton, J. L. Organometallics 1998, 17, 8759-3769. (n) Schuster, D. M.; White, P. S.; Templeton, J. L. Organometallics 2000, 19, 1540-1548.
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82. For known monomeric group 6 thiocarboxamido complexes see ref 6a (and references therein) and: (a) Desmond, T.; Lalor, F. J.; O'Sullivan, B.; Ferguson, G. J. Organomet. Chem. 1990, 381, C33-C37. (b) Ogric, C.; Lehotkay, T.; Wurst, K.; Jaitner, P.; Kriessl, F. R. J. Organomet. Chem. 1997, 541, 71-75. (c) Luo, X.-L.; Kubas, G. J.; Burns, C. J.; Butcher, R. J. Organometallics 1995, 14, 3370-3376.
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