Allylmagnesium-initiated Oligomerization of α,β-Unsaturated Aldehyde Aziridinylhydrazones

Synlett

Volumn 1997, Issue 2, 1997, Pages 191-192

  Oishi, Masataka ^a   Yamamoto, Hisashi ^a  

^a NAGOYA UNIVERSITY   (Japan)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0344724167     PISSN: 09365214     EISSN: None     Source Type: Journal    
DOI: 10.1055/s-1997-731     Document Type: Article

References (14)

1. (a) Vedejs, E.; Stolle, W. T. Tetrahedron Lett. 1977, 135.
2. (b) Bertz, S. Tetrahedron Lett. 1980, 21, 3151.
3. (c) Kabalka, G. W.; Maddox, J. T.; Bogas, E. J. Org. Chem. 1994, 59, 5530.
4. Maruoka, K.; Oishi, M.; Yamamoto, H. Macromolecules 1996, 29, 3328.
5. Kleinman, E. F.; Volkmann, R. A. In Comprehensive Organic Synthesis; Trost, B. M., Fleming, I., Eds.; Pergamon Press: New York, 1991; Vol. 2, 975-1006.
6. (a) Alexakis, A.; Lensen, N.; Tranchier, J-P.; Mangeney, P.; Feneau-Dupont, J.; Declercq, J. P. Synthesis, 1995, 1038.
7. (b) Denmark, S. E.; Edwards, J. P.; Nicaise, O. J. Org. Chem. 1993, 58, 569.
8. 3).
9. -1.
10. Regioselective reactions of 3-trimethylsilylpropargyl and/or 1-trimethylsilylallenyl anion: (a) Ishiguro, M.; Ikeda, N.; Yamamoto, H. J. Org. Chem. 1982, 47, 2225. (b) Yamamoto, Y.; Ito, W.; Maruyama, K. J. Chem. Soc., Chem. Commun. 1984, 1004.
11. Regioselective reactions of 3-trimethylsilylpropargyl and/or 1-trimethylsilylallenyl anion: (a) Ishiguro, M.; Ikeda, N.; Yamamoto, H. J. Org. Chem. 1982, 47, 2225. (b) Yamamoto, Y.; Ito, W.; Maruyama, K. J. Chem. Soc., Chem. Commun. 1984, 1004.
12. 2Si: C, 75.42; H, 6.96; N, 8.80. Found: C, 75.44; H, 7.05; N, 8.75.
13. -1.
14. n = 1.13.